• 대한치과기공학회지
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• 제26권1호
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• pp.89-96
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• 2004

Hydroxyapatite powder were synthesized by precipitation method, varying pH, and reaction temperature. The powders were heated at 1,200$^{\circ}{\cdots}$ and 1,300$^{\circ}{\cdots}$ for fabrication of dental prosthesis. The results are as follows: Synthesized powder showed the smallest particle in size, under the conditions of pH 11 and reaction temperature 37$^{\circ}{\cdots}$. The hydroxyapatite was partially converted to $\alpha,\;\beta$-TCP at 1,200$^{\circ}{\cdots}$ and 1,300$^{\circ}{\cdots}$. Mechanical strength of sample was affected by such powder preparation conditions as pH and reaction temperature and sintering temperature. The mechanical strength of sample prepared under the same conditions was increased with increasing pH, reaction temperature and sintering temperature.

• 호남수학학술지
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• 제42권1호
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• pp.139-150
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• 2020

Let p be a prime number with p > 3, p ≡ 3 (mod 4) and let n be a positive integer. In this paper, we prove that the Diophantine equation (5pn² - 1)^x + (p(p - 5)n² + 1)^y = (pn)^z has only the positive integer solution (x, y, z) = (1, 1, 2) where pn ≡ ±1 (mod 5). As an another result, we show that the Diophantine equation (35n² - 1)^x + (14n² + 1)^y = (7n)^z has only the positive integer solution (x, y, z) = (1, 1, 2) where n ≡ ±3 (mod 5) or 5 | n. On the proofs, we use the properties of Jacobi symbol and Baker's method.

• 한국지반환경공학회 논문집
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• 제13권2호
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• pp.95-102
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• 2012

본 연구에서는 기존 C.I.P 공법의 개선사항을 보완하여 벽체 강성 및 차수성을 증진시킨 개량형 C.I.P 공법을 개발하고 이에 대한 현장 적용성을 검토하였다. 개량형 C.I.P 공법의 특징은 원형케이싱의 내부 양쪽에 삼각형 형태의 조인트를 설치하여 연직연속천공을 위한 가이드로 이용하고 연속천공 이후에는 조인트와 조인트를 소형 H형강으로 연결하여 개별말뚝들이 연결된 벽체를 형성함과 동시에 H형강 외의 내부는 그라우팅으로 충진되어 벽체 전체가 차수성을 확보하도록 고안된 점이다. 이러한 특성에 대한 현장 적용성을 검토하기 위해 모형 토조실험을 수행하여 차수성을 검토하였으며 벽체 강성의 증진에 대한 사항은 케이싱의 두께를 2mm와 3mm로 변화를 둔 실물크기의 시험체를 대상으로 강도실험과 수치해석이 병행되었다. 수치해석의 경우, 강도실험에 대한 시뮬레이션을 통해 사용프로그램의 타당성을 우선 검토한 후, 케이싱의 두께 변화에 따른 영향을 비교분석하였다. 연구결과, 차수성 시험은 정수압 300KPa의 가압상태에서도 이음부의 누수가 발생하지 않았다. 휨강도 실험결과, 개량형 흙막이 벽체의 강성이 기존 C.I.P 벽체의 강성보다 4배 정도 큰 것으로 나타났으며 압축강도 또한 콘크리트의 압축강도보다 큰 것으로 나타났다. 이상의 결과로부터 제안된 개량형 C.I.P 공법은 기존의 C.I.P 공법의 차수공정의 생략뿐만 아니라, 연결부 차수성 확보, 연직연속천공, 그리고 상대적으로 우수한 강성등의 장점을 보유한 것으로 나타나 향후 주열식 흙막이 시공에 일조할 수 있을 것으로 판단된다.

• 한국세라믹학회지
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• 제26권2호
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• pp.157-166
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• 1989

The effect of pH variation in starting solution on the characteristics of hydroxyapatite precipitates and powder prepared by the wet method was investigated. Hydroxyapatite precipitates was agglomerated, the average agglomerated particle size was decreased in the range from 2 to 6${\mu}{\textrm}{m}$ with increasing pH values in starting solution. The aspect ratio of rod-shaped hydroxyapatite particle was rapidly increased at pH 11 and 11.5. The maximum specific surface area, 91.1$m^2$/g, was at pH 10.5. Dried powder prepared at high pH values contained more minutes CO2 than that prepared at low pH values. The poor crystallinity was maintained up to $600^{\circ}C$ regardless of the pH values in starting solutions. However, the second phase or high crsytalline hydroxypatite phase appeared above 80$0^{\circ}C$. In pH 9.5 and pH 10, $\beta$-whitlockite transformed to $\alpha$-whitlockite at 120$0^{\circ}C$, while in pH 10.5-11.5, hydroxyapatite phase was maintained up to 120$0^{\circ}C$.

• Journal of Pharmaceutical Investigation
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• 제20권3호
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• pp.115-119
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• 1990

The reaction rates, duration times and neutralizing capacities of the antacids which are frequently used in Korean market and three different commercial combination products were evaluated in vitro by Fuchs method and Johnson-duncan method, respectively. In vivo tests of combination products were determined in the fasted state of rat by Aspiration method. Comparing the result of in vitro test with that of in vivo test, the maximal pH was lowered by 2-3 value and the durational time increased by two folds in vivo test. Each antacid composition and combination products from three phamaceutical companies (A, B, and C) were studied, respectively. The duration times measured by Fuchs method were double compared to those by Johnson-Duncan method. A and C preparation maintained the pH range from 3 to 7 for 60 min by Fuchs method. In vovo test, maximum pH of A, B and C preparation was 6.50, 3.65, 2.65 and duration time of those was 200, 500, 0 min, respectively.

• Asian-Australasian Journal of Animal Sciences
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• 제31권2호
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• pp.293-300
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• 2018

Objective: This study observed the effects of cooking method and final core temperature on cooking loss, lipid oxidation, aroma volatiles, nucleotide-related compounds and aroma volatiles of Hanwoo brisket (deep pectoralis). Methods: Deep pectoralis muscles (8.65% of crude fat) were obtained from three Hanwoo steer carcasses with $1^+$ quality grade. Samples were either oven-roasted at $180^{\circ}C$ (dry heat) or cooked in boiling water (moist heat) to final core temperature of $70^{\circ}C$ (medium) or $77^{\circ}C$ (well-done). Results: Boiling method reduced more fat but retained more moisture than did the oven roasting method (p<0.001), thus no significant differences were found on cooking loss. However, samples lost more weight as final core temperature increased (p<0.01). Further, total saturated fatty acid increased (p = 0.02) while total monounsaturated fatty acid decreased (p = 0.03) as final core temperature increased. Regardless the method used for cooking, malondialdehyde (p<0.01) and free iron contents (p<0.001) were observed higher in samples cooked to $77^{\circ}C$. Oven roasting retained more inosinic acid, inosine and hypoxanthine in samples than did the boiling method (p<0.001), of which the concentration decreased as final core temperature increased except for hypoxanthine. Samples cooked to $77^{\circ}C$ using oven roasting method released more intense aroma than did the others and the aroma pattern was discriminated based on the intensity. Most of aldehydes and pyrazines were more abundant in oven-roasted samples than in boiled samples. Among identified volatiles, hexanal had the highest area unit in both boiled and oven-roasted samples, of which the abundance increased as the final core temperature increased. Conclusion: The boiling method extracted inosinic acid and rendered fat from beef brisket, whereas oven roasting intensified aroma derived from aldehydes and pyrazines and prevented the extreme loss of inosinic acid.

• 한국환경보건학회지
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• 제28권2호
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• pp.109-116
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• 2002

The purpose of this study was to evaluate a new sampling and analytical method for the determination of airborne hexavalent chromium, Cr(Ⅵ), in a field plating operation. The procedures of this new method (Shin & Paik's Method) are as the following: Airborne hexavalent chromium is collected on polyvinyl chloride (PVC) filter according to the National Institute iota Occupational Safety and Health (NIOSH) Method 7600, and the filler sample is placed in a screw-capped vial and soaked with 2% NaOH/3% Na₂CO₃ solution immediately after sampling. The Cr(Ⅵ) sample is analyzed by ion chromatography/visible spectrophotometry (IC/VS) according to the U.S. Environmental Protection Agency (EPA) Method 218.6. The airborne Cr(Ⅵ) concentrations measured by this method were compared with those determined by three reference methods: One (NIOSH/EPA Method) consisted of sampling airborne Cr(Ⅵ) on PVC filters and storing the sample filters in strew-capped vials according to the NIOSH method, and analyzing Cr(Ⅵ) in samples using IC/VS according to the EPA method. The second method (Impinger Method/NaHCO₃) consisted of absorbing airborne Cr(Ⅵ) into 0.02 M NaHCO₃ solution in midget impinger, and analyzing the Cr(Ⅵ) in samples using IC/VS. The third method was the OSHA Method ID-215. Using these four different methods, lour replicates of air samples were collected at an electroplating process and analyzed simultaneously. Two-way ANOVA and paired t-test were used to test difference among values determined by the methods. There was no significant difference and a strong correlation (r²:0.99) between Cr(Ⅵ) concentrations measured by the Shin & Paik's Method and an impinger method (p>0.05). However, Cr(Ⅵ) concentrations determined by Shin & Paik's Method were significant1y different from those by the NIOSH/EPA Method (p<0.05) or the OSHA method (p<0.05). The Cr(Ⅵ) concentrations of Shin & Paik's Method were significantly higher than those of the NIOSH/EPA Method or the OSHA method. This result indicated that the Shin & Paik's Method may prevent Cr(Ⅵ) losses caused by reduction and give more reliable results of airborne Cr(Ⅵ) concentrations in work environments.

• 기본간호학회지
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• 제3권2호
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• pp.273-283
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• 1996

Effectiveness of the video-record learning method in teaching bowel elimination nursing skill was investigated using an experimental research methodology. Data was collected from 63 female students attending Fundamental Nursing class from a nursing college in Seoul. The subjects were randomly assigned to two groups, one is the experimental group of 29 and the other the control group of 34. The independent variable was video-record learning method and the dependent variable were the degree of knowledge achivement, nursing skill achivement, competence on practicing elimination skill, and satisfaction about the learning method. The hypotheses of the study were as following. 1) There will be significant difference between the experimental group and the control group in dependent variables. 2) There will be significant positive correlations between nursing skill achievement and other three dependent variables-interest in nursing, adaptation in nursing, and preference of nursing job. Data was analyzed using descriptive statistics, chi-square test, t-test, and Pearson's correlation coefficient with SPSS $PC^+$ program. Findings of the study are : 1) There was no significant difference between the experimental group and the control group in knowledge achievement using P<.05. 2) There was significant difference between the experimental group and the control group in nursing skill achievement using P<.05. 3) There was no significant difference between the experimental group and the control group in competence on practicing elimination skill using P<.05. 4) There was no significant difference between the experimental group and the control group in satisfaction about learning method using P<.05. 5) There was positive correlation between nursing skill achievement and the other variables but no significant difference was shown. 6) This study suggests that video-record learning method is an effective learning method for achiving basic nursing skills but is not effective in other areas such as knowledge achivement, competence in performing nursing practice, and satis-faction about the learning method. Further study with more developed research design and statistical analysis should be done to investigate the effectivenes of video-record learning method in learning basic nursing skill more accurately.

• 생약학회지
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• 제47권2호
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• pp.186-191
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• 2016

A new UPLC-DAD method for simultaneous determination of p-coumaric acid and trans-cinnamic acid in propolis was developed using Halo-C18 column and step gradient elution of MeCN and $0.1%H_3PO_4$ in 8 min. The method was validated by specificity, linearity, limit of detection, limit of quantification, precision(intra- and inter-day variability) and recovery tests. The validated method was sufficiently applicable for quantitative analysis of propolis products as well as propolis collected from different regions in Korea. The established method is simple, appropriate and efficient, and can be used for quality assessment of Korean propolis.

• 한국통신학회논문지
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• 제36권3C호
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• pp.149-156
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• 2011

차세대 무선 이동통신 시스템의 높은 서비스 품질을 위한 방법으로 MIMO-OFDM(Multiple Input Multiple Output-Orthogonal Frequency Division Multiplexing)방식이 주목받고 있다. 그러나 OFDM 시스템에서와 같이 큰 PAPR(Peak-to-Average Power Ratio)이 중요한 문제이다. 본 논문에서는 PAPR의 감소를 위해, 새로운 위상시퀀스를 기반으로 한 적응형 P-SLM(Partitioned-SeLective Mapping) 기법을 제안한다. 제안된 기법은 새로운위상 시퀀스를 주기적으로 곱하고, 일정한 PAPR 임계치를 이용한 적응성으로 인해 PAPR성능 향상뿐만 아니라 복잡도 또한 감소한다. 모의 실험 결과 제안된 기법이 기존의 기법보다 PAPR 성능 뿐만 아니라 복잡도 또한 감소한 것을 확인 할 수 있었다.