• Title/Summary/Keyword: Over-firing

Search Result 112, Processing Time 0.028 seconds

Effects of Glass Particle Size on Sintering Behaviors of the Glass-Alumina Composites for Low Firing Temperature (저온 소성용 유리-알루미나 복합체에서 유리 입자크기에 따른 소결거동)

  • 박덕훈;김봉철;김정주;박이순
    • Journal of the Korean Ceramic Society
    • /
    • v.37 no.6
    • /
    • pp.545-551
    • /
    • 2000
  • Sintering behaviors of the glass-alumina composites for low firing temperature were investigated as a function of the particle size of glass frit. The system of glass frit was Pb-B-Si-Al-O. The median particle sizes of the glass frits were 2.72$\mu\textrm{m}$, 2.67$\mu\textrm{m}$ and 1.33$\mu\textrm{m}$, which were prepared with changing ball-milling times as 24 h, 48 h and 96 h. The glass-alumina composites showed maximum density at certain temperature, and further heating led to dedensification behaviors, so called over-firing. The sintering temperature, which showed maximum density, raised from 425$^{\circ}C$ to 475$^{\circ}C$ with increase of particle size of glass frit from 1.33$\mu\textrm{m}$ to 2.72$\mu\textrm{m}$. Especially, the over firing behaviors, which were occurred at high sintering temperatures, were greatly increased with decrease of particle size of glass frit.

  • PDF

Effects of Volume Fraction & Particle Size of Alumina on Sintering Behaviors of the Glass-Alumina Composites for Low Firing Temperature (저온 소성용 유리-알루미나 복합체에서 알루미나의 부피분율과 입자크기에 따른 소결 거동)

  • 박덕훈;김봉철;김정주;박이순
    • Journal of the Korean Ceramic Society
    • /
    • v.37 no.7
    • /
    • pp.638-644
    • /
    • 2000
  • The sintering behaviors of the glass-alumina composites for low firing temperature were investigated as functiions of the volume fraction of alumina powder and the particle size with respect to porosity and pore shape. As the volume fraction of alumina powder was increased or the particle size of it was decreased, the sintering temperature of open pore-closing was raised. When the volume fractions of alumina which had 2.19$\mu\textrm{m}$ median diameter were increased with 20, 30, 40, and 50%, the sintering temperatures of open pore-closing were 425, 450, 475, and 500$^{\circ}C$. And when the median particle size of alumina was diminished from 2.19$\mu\textrm{m}$ to 0.38$\mu\textrm{m}$, the sintering temperature of open pore-closing was increased from 450$^{\circ}C$ to 475$^{\circ}C$. Especially, the sintering temperature, which showed maximum density, was corresponded with the stage of open pore-closing and after achieving maximum density over heating resulted in dedensification of specimen, so called, over-firing behavior.

  • PDF

On the Reachability Set of Petri Net under the Earliest Firing Rule

  • Ohta, Atsushi;Seto, Hiroaki;Tsuji, Kohkichi
    • Proceedings of the IEEK Conference
    • /
    • 2000.07b
    • /
    • pp.641-644
    • /
    • 2000
  • This paper studies coverability tree and reach-ability set of Petri net under the earliest filing rule. Conventional algorithm for coverability tree for ‘normal’ Petri net is not good for Petri net under the earliest firing rule. More over, it is shown that there exists no coverability graph for general class of earliest firing Petri net. Some subclasses are studied where coverability graph can be constructed.

  • PDF

Investigation of Firing Conditions for Optimizing Aluminum-Doped p+-layer of Crystalline Silicon Solar Cells

  • Lee, Sang Hee;Lee, Doo Won;Shin, Eun Gu;Lee, Soo Hong
    • Current Photovoltaic Research
    • /
    • v.4 no.1
    • /
    • pp.12-15
    • /
    • 2016
  • Screen printing technique followed by firing has commonly been used as metallization for both laboratory and industrial based solar cells. In the solar cell industry, the firing process is usually conducted in a belt furnace and needs to be optimized for fabricating high efficiency solar cells. The printed-Al layer on the silicon is rapidly heated at over $800^{\circ}C$ which forms a layer of back surface field (BSF) between Si-Al interfaces. The BSF layer forms $p-p^+$ structure on the rear side of cells and lower rear surface recombination velocity (SRV). To have low SRV, deep $p^+$ layer and uniform junction formation are required. In this experiment, firing process was carried out by using conventional tube furnace with $N_2$ gas atmosphere to optimize $V_{oc}$ of laboratory cells. To measure the thickness of BSF layer, selective etching was conducted by using a solution composed of hydrogen fluoride, nitric acid and acetic acid. The $V_{oc}$ and pseudo efficiency were measured by Suns-$V_{oc}$ to compare cell properties with varied firing condition.

Regional difference in spontaneous firing inhibition by GABAA and GABAB receptors in nigral dopamine neurons

  • Kim, Yumi;Jang, Jinyoung;Kim, Hyun Jin;Park, Myoung Kyu
    • The Korean Journal of Physiology and Pharmacology
    • /
    • v.22 no.6
    • /
    • pp.721-729
    • /
    • 2018
  • GABAergic control over dopamine (DA) neurons in the substantia nigra is crucial for determining firing rates and patterns. Although GABA activates both $GABA_A$ and $GABA_B$ receptors distributed throughout the somatodendritic tree, it is currently unclear how regional GABA receptors in the soma and dendritic compartments regulate spontaneous firing. Therefore, the objective of this study was to determine actions of regional GABA receptors on spontaneous firing in acutely dissociated DA neurons from the rat using patch-clamp and local GABA-uncaging techniques. Agonists and antagonists experiments showed that activation of either $GABA_A$ receptors or $GABA_B$ receptors in DA neurons is enough to completely abolish spontaneous firing. Local GABA-uncaging along the somatodendritic tree revealed that activation of regional GABA receptors limited within the soma, proximal, or distal dendritic region, can completely suppress spontaneous firing. However, activation of either $GABA_A$ or $GABA_B$ receptor equally suppressed spontaneous firing in the soma, whereas $GABA_B$ receptor inhibited spontaneous firing more strongly than $GABA_A$ receptor in the proximal and distal dendrites. These regional differences of GABA signals between the soma and dendritic compartments could contribute to our understanding of many diverse and complex actions of GABA in midbrain DA neurons.

Development of Heterojunction Electric Shock Protector Device by Co-firing (동시소성형 감전소자의 개발)

  • Lee, Jung-soo;Oh, Sung-yeop;Ryu, Jae-su;Yoo, Jun-seo
    • Korean Journal of Materials Research
    • /
    • v.29 no.2
    • /
    • pp.106-115
    • /
    • 2019
  • Recently, metal cases are widely used in smart phones for their luxurious color and texture. However, when a metal case is used, electric shock may occur during charging. Chip capacitors of various values are used to prevent the electric shock. However, chip capacitors are vulnerable to electrostatic discharge(ESD) generated by the human body, which often causes insulation breakdown during use. This breakdown can be eliminated with a high-voltage chip varistor over 340V, but when the varistor voltage is high, the capacitance is limited to about 2pF. If a chip capacitor with a high dielectric constant and a chip varistor with a high voltage can be combined, it is possible to obtain a new device capable of coping with electric shock and ESD with various capacitive values. Usually, varistors and capacitors differ in composition, which causes different shrinkage during co-firing, and therefore camber, internal crack, delamination and separation may occur after sintering. In addition, varistor characteristics may not be realized due to the diffusion of unwanted elements into the varistor during firing. Various elements are added to control shrinkage. In addition, a buffer layer is inserted in the middle of the varistor-capacitor junction to prevent diffusion during firing, thereby developing a co-fired product with desirable characteristics.

Effect of $CaSO_4$ and $BaSO_4$ on the Formation of Portland Cement Clinker (Portland Cement Clinker 생성반응에 미치는 $CaSO_4$$BaSO_4$의 영향)

  • 서일영;최상흘
    • Journal of the Korean Ceramic Society
    • /
    • v.11 no.1
    • /
    • pp.29-35
    • /
    • 1974
  • Effect of calcium sulfate and barium sulfate on the formation of portland cement clinker was studied by means of chemical analysis. DTA and X-ray diffraction analysis. In the presence of liquid phase, effect of the additives on the formation of tricalcium silicate was examined according to the reaction, 2CaO.$SiO_3$+CaO$\longrightarrow$3CaO.$SiO_3$, which is the principal reaction in portland cement clinkerization, and optimum conditions in firing clinker concerning amount of additive, firing time and temperature were determined, and its kinetics was referred to. The experimental results are summerized as follow: (1) Appropriate burning temperature range of cement clinker is more limited as the content of calcium sulfate in clinker is increased. Amount of calcium sulfate, firing time and temperature in proper condition of clinkerization is related to each others. Being added suitable quantity of calcium sulfate, firing temperature of clinker can be lowered about $100^{\circ}C$. (2) When 3-5 mole% of calcium sulfate is added, firing time of 15-30 minutes at about $1380^{\circ}C$ is reasonable, and if the content is over7 mole %, firing for 1 hr. or more at $1350^{\circ}C$ is anticipated to be optimum condition. (3) In the reaction of tricalcium silicate formation, the role of barium sulfate as a mineralizer is similar to that of calcium sulfate, but the optimum firing temperature of cement clinker containing barium sulfate tends to be 20-$30^{\circ}C$ higher than that of clinker containing calcium sulfate. (4) When barium sulfate is used as mineralizer, 2-3 mole % of it to tricalcium silicate is recommended and if it is added more than this amount, free CaO is increased rapidly in clinker and alite formation is inhibited.

  • PDF

Powder Synthesis and Sintering Behavior of Hydroxyapatite by Citrate Method (Citrate법을 이용한 수산화아파타이트 분말합성 및 소결특성)

  • 임병일;최세영;정형진;정형진;오영제
    • Journal of the Korean Ceramic Society
    • /
    • v.33 no.9
    • /
    • pp.1003-1011
    • /
    • 1996
  • Hydroxyapatite powder was synthesized by a citrate method, . Char-like precursor composed of Ca8(HPO4)2(PO4)4.5H2O (OCP) and CaCo3 was found via viscous resin-like intermediate by heating the mixed aqueous solution of Ca(NO3)2.4H2O(NH4)2HPO4 and citric acid. Resulted powder was transformed into hydroxyapatite phase by firing over 120$0^{\circ}C$-135$0^{\circ}C$ for 4 hr using the powder calcined at 90$0^{\circ}C$ for 10 hr composed of mostly single hydroxyapatite phase. The sintered densities increased with firing temperature up to 130$0^{\circ}C$ but the highest relative density was about 94% of theoritical value. indicating the presence of closed pores. The maximum 96 MPa of flexural strength was obtained at 120$0^{\circ}C$ firing but the flexural strength showed lower values over the above sintering condition. Vitro test was performed by immersing of two jointed specimens in SBF for seven days and adhesion was observed between two specimens.

  • PDF

Customer Selection in CRM implementation: Firms′strategies in the competitive market with network externality

  • Kim Eun-Jin;Lee Byeong-Tae
    • Proceedings of the Korean Operations and Management Science Society Conference
    • /
    • 2003.11a
    • /
    • pp.183-186
    • /
    • 2003
  • Customer profitability recognition is easier with CRM enabling technologies and the strategy of firing unprofitable customers prevails in the market. However, in the digital and Internet age, network externality is becoming more important. Therefore, the concern over firing unprofitable customers has increased. Our research is intended to develop strategic guidance for customer selection when firms implement CRM in the market with network externality.

  • PDF

Study on Operating Limits of 5.56mm Rifle Overheat - Focusing on Human Engineering (5.56mm 소총 과열에 의한 운용한계 분석 - 인간공학 중심으로)

  • Lee, Ho-Jun;Choi, Si-Young;Shin, Tae-Sung
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.21 no.9
    • /
    • pp.49-56
    • /
    • 2020
  • High temperature heat generated during rifle firing not only degrades the performance of the weapon, but also limits the user's operation. In this study, temperature change of handguard according to firing was measured with reference to Human Engineering criteria and the operability according to material was examined. Accordingly, for the firing test, three types of Korean rifle and one overseas model were selected for each material of handguard, and firing test was conducted using a contact type temperature meter. The test result shows that using a plastic handguard with low thermal conductivity and aluminum handguard with high thermal conductivity enabled the rifles to be operated with bare hands even when firing at more than 100 rounds at low atmospheric temperature. However, when firing more than 60 rounds at over 20℃ atmospheric temperature, aluminum handguard use is limited. When firing quickly over 100 rounds, handguard use is restricted regardless of its fabrication material. To eliminate operational limitations by overheating, it is necessary to eliminate direct contact with skin using gloves, vertical grips, etc. This study examined the operability of rifles in terms of thermal risk, and the resulting study results are expected to be used as basic data for Human Engineering of other rifles and munitions.