• 한국세라믹학회지
• /
• 제39권8호
• /
• pp.758-763
• /
• 2002

초음파 에너지(28 kHz, 40 kHz, 70 kHz)를 사용하여 수직자기기록용 Ba-ferrite의 자기적 특성 향상에 대하여 조사하였다. 한편, 분산된 Ba-ferrite를 sheet에 수직으로 배향시키기 위해 다양한 형태의 배향기들을 사용하여 실험을 행하였다. Ba-ferrite가 도포된 sheet 중 초음파 에너지가 40 kHz이고 초음파 처리 시간이 2시간에서 자기적 특성인 S. Q. (Squareness Ratio)와 O. R. (Orientation Ratio)값이 각각 0.7831과 2.87로 비교적 좋은 값을 얻을 수 있었다. 이때 얻어진 sheet의 표면 형상을 SEM(Scanning Electron Microscopy)으로 분석한 결과 Ba-ferrite가 자화용이축인 c 축에 수직방향으로 배향되어 수직자기기록용으로서의 응용에 가능성을 보였다. 또한, VSM(Vibrating Sample Magnetometer)으로 자기장의 각도변화에 따른 S. Q.의 측정시, 자기장의 각도가 증가함에 따라 S. Q. 값이 감소하였고 이는 수직자기기록용으로써 가능성을 재확인 시켜주었다.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2003년도 추계학술대회논문집
• /
• pp.281-284
• /
• 2003

The microstructural changes of Al-Zn-Mg-Cu alloy containing Sc during hot extrusion and post heat treatment is investigated. Two kinds of Al-Sc alloys with different alloying elements (B1, B2) are hot extruded to make I-shape bars at 380$^{\circ}C$, then the bars are solution treated at 480$^{\circ}C$ for 2hrs followed by artificial aging at 120$^{\circ}C$ for 24hrs. The interior microstructure of as extruded bar consists of elongated grains, however, fine equiaxed grains are mainly observed around surface. The microstructural gradient suggests that different restoration process can proceed during the hot extrusion. For B1 and B2, different grain growth behaviors are found around the surface during the post heat treatment. Rapid grain growth behavior around the surface is discussed related with the crystallographic orientation of the grain.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2003년도 춘계학술대회논문집
• /
• pp.120-126
• /
• 2003

Finite element analysis model is suggested for analysis of milli-forming process, which forms milli-size products. Since the size of workpiece in a milli-forming process ranges from a few hundred micrometers to a few millimeters, microstructural changes such as the growth of micro-voids and the development of preferred orientation in a grain become crucial factors for the success of milli-forming. This analysis model incorporates anisotropy from deformation torture and deterioration of mechanical properties due to the growth of micro-voids. Applications of the proposed modeling to milli-forming are given and the results are carefully examined to understand the deformation characteristics such as texture development and damage evolution during extrusion/drawing of a milli-bar.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2001년도 춘계학술대회 논문집
• /
• pp.245-249
• /
• 2001

This paper is concerned with numerical analyses for bulk forming of a single crystal milli-product, whose typical size ranges from a few hundreds ${\mu}m$ to a few mm. The numerical formulation invoked in this paper combines the crystal plasticity theory considering texture development and the ductile damage mechanics for growth of micro voids, since orientation development and growth of micro voids become the primary factors for bulk forming of milli-size products. As applications, milli-extrusion of a single crystal round bar and milli-rolling of a single crystal plate are simulated and the results are discussed in detail.

• 한국공작기계학회논문집
• /
• 제17권4호
• /
• pp.133-139
• /
• 2008

With the increasing demand for higher production quality and growing competition in the global market, coordinate measuring machine(CMM) has been widely used in industry to improve the efficiency and effectiveness of measurement. In this paper the performance evaluation of coordinate measuring machine is proposed using design of experiments. A factorial design is applied to carry out the performance test proposed by ISO 10360 with a length bar and to investigate CMM measurement errors associated to orientation and length in the work volume. The determination of the significance of effects in an experiment is made through the analysis of variance(ANOVA). The results show that the proposed method is suitable to analyze the factors which affect the CMM measurement performance.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2009년도 하계학술대회 논문집
• /
• pp.235-235
• /
• 2009

This paper describes the influence of a polycrystalline (poly) 3C-SiC buffer layer on the surface acoustic wave (SAW) properties of poly aluminum nitride (AlN) thin films by comparing the center frequency, insertion loss, the electromechanical coupling coefficient ($k^2$), andthetemperaturecoefficientoffrequency(TCF) of an IDT/AlN/3C-SiC structure with those of an IDT/AlN/Si structure, The poly-AlN thin films with an (0002)-preferred orientation were deposited on a silicon (Si) substrate using a pulsed reactive magnetron sputtering system. Results show that the insertion loss (21.92 dB) and TCF (-18 ppm/$^{\circ}C$) of the IDT/AlN/3C-SiC structure were improved by a closely matched coefficient of thermal expansion (CTE) and small lattice mismatch (1 %) between the AlN and 3C-SiC. However, a drawback is that the $k^2(0.79%)$ and SAW velocity(5020m/s) of the AlN/3C-SiC SAW device were reduced by appearing in some non-(0002)AlN planes such as the (10 $\bar{1}$ 2) and (10 $\bar{1}$ 3) AlN planes in the AlN/SiC film. Although disadvantages were shown to exist, the use of the AlN/3C-SiC structure for SAW applications at high temperatures is possible. The characteristics of the AlN thin films were also evaluated using FT-IR spectra, XRD, and AFM images.

• 공업화학
• /
• 제7권1호
• /
• pp.34-42
• /
• 1996

합성에메랄드[$(BeO)_3(Al_{2-x}Cr_xO_3)(SiO_2)_6$]단결정을 flux법에 의하여 육성하였다. 출발물질로 BeO, $Al_2O_3$와 $SiO_2$ 시약을 화학양론비로 혼합하여 사용하였다. 에메랄드 단결정의 성장 조건은 다음과 같다. 온도범위 ; $1150{\sim}900^{\circ}C$, 냉각속도 ; 2, 4, $10^{\circ}C/hr$, 융제 : $Li_2CO_3$, $V_2O_5$, 첨가제 ; $Cr_2O_3$. 에메랄드 단결정의 크기는 2, 4, $10^{\circ}C/hr$의 냉각속도에 의존하였다. 얻어진 에메랄드 단결정을 동정하였고, 그 결과는 다음과 같다. 즉, 결정계 ; 육방정계, 격자상수 ; a=0.921nm, c=0.917nm, 결정의 크기 ; 최대 $0.80{\times}0.95mm^2(c{\times}m)$, 방위 ; c(1000), $m(10{\bar{1}}0)$.

• 한국산림과학회지
• /
• 제82권1호
• /
• pp.7-11
• /
• 1993

상해(傷害)에 기인하여 양버즘나무(Platanus occidentalis L.) 수간에 형성된 팽창조직(膨脹組織)의 해부학적(解剖學的) 특성(特性)을 조직학적(組織學的) 및 수량적(數量的) 측면(側面)네서 정상조직(正常組織)과 비교(比較) 고찰(考察)하였다. 팽창조직은 정상조직에 비하여 세포배열이 불규칙적이고 도관요소내 타일로시스가 현저하게 발달되어 있으며, 후벽화(厚壁化)된 목섬유가 흔히 관찰된다는 점, 복합관공이 덜 나타난다는 점에서 차이를 나타내었고, 관공의 직경이 작고 도관요소와 목섬유의 길이가 짧으며 도관빈도(vessel frequency)는 작은 반면, 도관요소내 계단상 천공관의 bar 수(數)가 많으며, 방사조직 빈도(ray frequency)가 크고 방사조직의 폭이 넓으나 높이가 작은 특성(特性)을 나타내었다.

• 한국정밀공학회지
• /
• 제26권4호
• /
• pp.91-99
• /
• 2009

Because of both precise measurement and efficient quality control, coordinate measuring machines(CMMs) have been widely used in the industry. The purpose of this paper is to present a method to estimate the CMM measurement uncertainty using design of experiments. A factorial design is applied to carry out the performance test proposed by ISO 10360 and to investigate CMM measurement errors associated to orientation and length of the length bar. In order to assess the measurement uncertainty for the performance test, an analysis of the uncertainty components that make up the uncertainty budget has been carried out. The procedure for evaluating the uncertainty of it follows GUM ("Guide to the expression of uncertainty in measurement"). The results show that the proposed method is suitable to investigate CMM performance and determine the contribution of machine variables to measurement uncertainty.

• 한국주조공학회지
• /
• 제15권3호
• /
• pp.283-290
• /
• 1995

Molybdenum ingot of 50mm in diameter were obtained from sintered Mo bars by EB drip melting technique. Macroscopic observation of EB remelted ingot indicates that coarse and columnar grains grow in the direction parallel to ingot pulling direction. This can be explained by slow solidification (3mm/min), large temperature gradient and heat flow to this direction. The orientation of columnar structure was found to be <110>, <200> and <211> by the analysis of X-ray diffraction patterns. The contents of typical metallic impurities in Mo sintered bar are 1.2ppm Cr, 3ppm Fe, 44ppm Zr, 150ppm W. Most of metallic impurities were reduced below the order of ppm except zirconium and tungsten by the selective evaporation. In the removal of nonmetallic impurities, oxygen and carbon impurities were lowered from 120 to 6ppm and from 157 to 106ppm, respectively, after first melting. Although the purification effect was not significant with the number of remelting, Vickers hardness was reduced from 217 to 195 and 184 in sequence with increasing the number of remelting.