• Title/Summary/Keyword: Optimum treatment condition

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Phosphate Removal from Aqueous Solution according to Activation Methods of Red Mud (알루미늄 제련 폐기물(Red Mud)의 활성화 방법에 따른 수용상의 인산염 제거특성)

  • Kim, I-Tae;Bae, Woo-keun;Kim, Woo-jeong
    • Journal of Korean Society on Water Environment
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    • v.20 no.5
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    • pp.466-472
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    • 2004
  • Red mud is formed as a waste during bauxite refining known as Bayer's process. Its main constituents are iron, aluminium, sodium and silica. The disposal of large quantities of wasted red mud causes a serious ecological problem. In this study, the red mud wasted from the bauxite refinery was studied for phosphate removal from aqueous solution according to activation methods. The influence of heat treatment, and neutralization with sea water and acid treatment level for the optimum conditions for phosphate removal have been determined. Heat treatment combined with acid treatment is most suitable for the removal of phosphate from aqueous solution. The optimal condition was activated with 1 N HCl solution after heating in $600^{\circ}C$ during 4 hours. Acid and heat treatment causes sodalite compounds which hinder the phosphate adsorption to leach out. The adsorption data obtained followed a first-order rate expression and fitted well with the Freundlich Isotherm well.

Characteristics of Surface Hardening by Laser Power Control in Real Time of Spheroidal Graphite Cast Iron (실시간 출력 제어를 통한 구상흑연 주철의 레이저 표면경화 특성)

  • Kim, Jongdo;Song, Mookeun
    • Laser Solutions
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    • v.18 no.2
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    • pp.1-4
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    • 2015
  • This study is related to the surface hardening treatment to spheroidal graphite cast iron for die by using high power diode laser. Laser device used in this experiment is capable of real-time laser power control. This is because the infrared temperature sensor (two color pyrometer) attached to the optical system measures the surface temperature of specimen and adjusts the laser power in real time. The surface treatment was carried out with the change of heat treatment temperature at the beam travel speed 3 mm/sec. Hardened width and depth was measured and hardened zone was analyzed by micro vickers hardness test in order to research the optimum condition of heat treatment. The changes in microstructure of the hardened zone also was examined. As a result of hardness measurement and observations on microstructure of hardened zone, hardness increased over three times as compared with base metal because the martensite was formed on the matrix structure.

Drilling Characteristics of PVC Materials (PVC 재료의 드릴링 특성)

  • Byun, J.Y.;Park, Na-Ram;Chung, S.W.;Kwon, S.H.;Kwon, S.G.;Park, J.M.;Kim, J.S.;Choi, Won-Sik
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.14 no.1
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    • pp.70-77
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    • 2015
  • This paper develops and evaluates a mechanical machining process which involves drilling on PVS material. According to the material, two treatment experiments were conducted, one involving drilling in a wet condition or using a lubricant and one involving drilling in a dry condition with no lubricant. Drilling in a dry condition showed better performance in terms of the cutting time than in the wet condition. Otherwise, the wet condition has several advantages. The lubricant influenced the burr diameter size and minimized the temperature on the surface of the work piece. During the wet condition drilling process, a smaller burr diameter size was noted as compared to the dry condition. The temperature showed a linear correlation with the drill bit size, where a least-square analysis provided an $R^2$valuewhichexceeded 0.95. The wet condition required more cutting time than the dry condition. In this condition, the water provides a lubrication effect. A thin layer between the cutting edges and the surface of the work piece is formed. The chip formation is affected by the drilling depth. The color on the tips of the chips was darker than in the initial condition. No correlation between the drilling depth and the bore roughness was noted, but the variation of the cutting speed or the RPM influenced the roughness of the bore. The optimum cutting speed ranged from 40 RPM to 45 RPM in the condition which provided the finest roughness surface.

Property Changes of Mung Bean Depending on Hydrolysis Conditions (녹두의 가수분해조건에 따른 특성 변화)

  • Gu, Young-Ah;Jang, Se-Young;Park, Nan-Young;Mun, Chae-Ryun;Kim, Ok-Mi;Jeong, Yong-Jin
    • Food Science and Preservation
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    • v.13 no.5
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    • pp.563-568
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    • 2006
  • The properties of mung bean were investigated depending on hydrolysis condition. The results showed that enzyme treatments (${\alpha}$-amylase and protease each at 0.1% (w/w)) by varying hydrolysis temperature showed better properties than non-pretense treatment (control group). The treatment with 0.08% ${\alpha}$-amylase was best for optimum hydrolysis of mung bean starch The treatment using a mixture of 0.08% (w/w) ${\alpha}$-amylase and 0.12% (w/w) protease was best for optimum hydrolysis of meg bean protein. The effects of Hydrolysis time of mung bean showed that the optimum time was 60 and 90 min and there fore the optimum time was set at 60 min. These result showed that the best hydrolysis conditions of mung bean were the treatment at $60^{\circ}C$ for 60 min using a mixture of 0.08%(w/w) ${\alpha}$-amylase and 0.12% (w/w) pretense, with the sugar level shown at $5.8^{\circ}Brix$, reducing sugar at 2,022.13 mg% and crude protein at 7,666.17 mg%.

A Study on the Post-Weld Heat Treatment Effect to Mechanical Properties and Hydrogen Embrittlement for Heating Affected Zone of a RE 36 Steel

  • Moon, Kyung-Man;Lee, Myung-Hoon;Kim, Ki-Joon;Kim, Jin-Gyeong;Kim, Seong-Jong
    • Corrosion Science and Technology
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    • v.2 no.6
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    • pp.283-288
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    • 2003
  • The cathodic protection method is being widely used in marine structural steel, however a high tensile steel like RE 36 steel for marine structural steel is easy to get hydrogen embrittlement due to over protection during cathodic protection as well as preferential corrosion of HAZ(Heating Affected Zone) part. In this paper, corrosion resistance and mechanical properties such as elongation and hydrogen embrittlement were investigated with not only in terms of electrochemical view but also SSRT(Slow Strain Rate Test) method with applied constant cathodic potential, analysis of SEM fractography in case of both As-welded and PWHT(Post-Weld Heat Treatment) of $550^{\circ}C$. The best effect for corrosion resistance was apparently indicated at PWHT of $550^{\circ}C$ and elongation was increased with PWHT of $550^{\circ}C$ than that of As-welded condition. On the other hand. Elongation was decreased with applied potential shifting to low potential direction which may be caused by hydrogen embrittlement, however the susceptibility of hydrogen embrittlement was decreased with PWHT of $550^{\circ}C$ than that of As-welded condition and Q.C(quasi cleavage) fracture mode was also observed significantly according to increasing of susceptibility of hydrogen embrittlement. Eventually it is suggested that an optimum cathodic protection potential range not causing hydrogen embrittlernent is from -770 mV(SCE) to -850 mV(SCE) in As-welded condition while is from -770 mV(SCE) to -875 mV(SCE) in PWHT of $550^{\circ}C$.

A Study on the Characteristics of Residual Stress in the Manufacturing Process of AISI 1536V and AISI A387 (제조공정에 따른 강종별 잔류응력 특성에 관한 연구; AISI 1536V, AISI A387)

  • Hwang, Sung-Kug;Moon, Jeong-Su;Kim, Han Joo
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.9
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    • pp.100-106
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    • 2020
  • This study analyzes the residual stress of AISI 1536V for an engine shaft of the shipbuilding industry and AISI A387 for a reactor shell of the chemical refining industry by the hole drilling method with a strain gauge rosette, which transforms fine mechanical changes into electrical signals. Tensile residual stress is generated in the forging and heat treatment process because specimens are affected by thermal stress and metal transformation stress. In the heat treatment process, the residual stress of AISI A387 is almost 170% the yield strength at 402 MPa. Since during the machining process, variable physical loads are applied to the material, compressive residual stress is generated. Under the same condition, the mechanical properties greatly affect the residual stress during the machining process. After the stress-relieving heat treatment process, the residual stress of AISI A387 is reduced below the yield strength at 182 MPa. Therefore, it is necessary to control the temperature, avoid rapid heat change, and select machining conditions depending on the mechanical properties of materials during manufacturing processes. In addition, to sufficiently reduce the residual stress, it is necessary to study the optimum condition of the stress-relieving heat treatment process for each material.

Development of the high elonagation and high strength steel sheets utilizing two step heat treatment (2단열처리를 이용한 고연신율 고장력 강판의 개발)

  • Kim, Y.H.;Kim, Y.H.;Kim, H.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.1
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    • pp.1-9
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    • 1997
  • The variation of the mechanical properties and the formation of retained austenite with heat treatment conditions in austempered Si bearing carbon steels has been investigated. In the case of a steel containing 0.35C-1.48Si-0.95Mn, it has been found that a feather shape bainite structure of lath are obtained under a isothermal treated condition at just below the Ms temperature, and the martensite, bainitic ferrite and retained austenite of second phase particles on the ferrite matrix for a isothermal treated steels after intercritical annealing are precipitated in a linked shape. The retained austenite with $2{\mu}m$ size induced as TRIP is found to increase with increasing the formation rate of retained austenite for the intercritical annealing and high Si containing steels. The tensile strength is increased as austempering temperature increases in all isothermal treatment temperature, whereas the elongation is shown to roughly decrease as the tensile strength increases. The values of tensile strength-elongation balance have showed a marked dependence upon the elongation rather than the tensile stregth, and their values are increased for high Si containing steels and intercritical annealing condition. The most optimum result has been shown to be the tensile stregth-elongation balance of $2882.4kgf/mm^2.%$ and the elongation of 33.3% for a "B" steel in the heat treating temperature range of $780{\sim}370^{\circ}C$.

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A Study on the Mixed Ratio and Dewaterability of Municipal Wastewater Sludge (도시하수 슬러지의 혼합비율자 탈수성에 관한 연구)

  • 이재운;김상훈
    • Journal of environmental and Sanitary engineering
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    • v.8 no.1
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    • pp.117-127
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    • 1993
  • When incineration method is utilized as a disposal process of sludge, the treatment generally consists of thickening, dewatering and incineration, implying that sludge dewaterability has a colose relationship with operating condition of a thickener. Dewatering factors should be, therefore investigated for achieving effective sludge treatment. No research on this has been performed in Korea. This study has focused on the evaluation on the effects of thickener operating variables on sludge dewatering, including sludge feed types and retention time. Mixing ratio of the first and the second sludge and operation time were varied in order to observe the change of dewaterability and optimum input of chemical conditioner.

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Fabrication and Characterization of High Purity Al2O3 by Decomposition of Selicite (세리사이드 분해에 의한 고순도 Al2O3의 제조 및 특성에 관한 연구)

  • 이경희;박한수;송명신
    • Journal of the Korean Ceramic Society
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    • v.24 no.5
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    • pp.431-436
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    • 1987
  • High purity Al2O3 has been extracted from serlcite of clayminerals, selicite was treated by H2SO4(2N∼18N) solution, NH4OH treatment(PH8.5∼10.0) and metallic impurities such as Fe were removed by NaOH treatment. The tendency of extraction yield of ${\alpha}$-Al2O3 have been investigated by relating reaction time, acid concentration. Reaction products were analyzed by DT-TGA, chemical analysis and X-ray diffractometer. Prepared ${\alpha}$-Al2O3 power is fired in air at 1400$^{\circ}C$, 1600$^{\circ}C$ 2hr. The results are as follows; 1. The most suitable extracting conditions of ${\alpha}$-Al2O3 from Selicite were N-H2SO4, 120 min acidtreating time. 2. The optimum pH condition was 9.0. 3. Physical properties of sintered Al2O3 bodies were as follows. Relative density is 99%. Water absorption is 0.26%. Rock well hardness is 89.

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Study on The Corrosion Inhibition Characteristics of Carbon Steel by Sodium Phosphate And Sodium Nitrite (삼인산 나트륨과 아질산 나트륨에 의한 탄소강 부식방지 특성 연구)

  • Moon, Jeon-Soo;Lee, Jae-Kun
    • Corrosion Science and Technology
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    • v.9 no.3
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    • pp.137-141
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    • 2010
  • Sodium nitrite is widely used as one of the popular corrosion inhibitors for the protection of ferrous metal in closed cooling water system, such as a diesel engine and a chiller. The optimum treatment conditions are studied through laboratory tests using linear polarization resistance (LPR) technique. Corrosion rate of the carbon steel electrode could be maintained less than $2.5{\times}10^{-3}$ mmpy in the test condition of 500 ppm as ${NO_2}^-$, 200 ppm as $Cl^-$, $70^{\circ}C$ and pH 6.8. The pH control is confirmed not to be an important factor in the protection of carbon steel by sodium nitrite inhibitor. The addition of tolyltriazole was needed for the protection of the copper alloy in the sodium nitrite treatment system.