• Title/Summary/Keyword: Optimum coating conditions

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Separation of Enamel from the Enamel Coated Coper Wires Via High Frequency Induction Process (에나멜코팅된 구리코일로 부터의 친환경적(親環境的) 구리선의 분리(分離))

  • Song, Yong-Ho;Kim, Jeong-Min;Park, Joon-Sik;Kong, Man-Sik;Lee, Caroline Seun-Young
    • Resources Recycling
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    • v.21 no.3
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    • pp.48-55
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    • 2012
  • Recently, the recycling with environmentally friendly method has been an issue for various fields. An effective removal method of coating layers from coated copper wires is one critical factor for recycling copper wire. We have adopted a high frequency heating routine for removing the coating layers on the coated copper wires, and attempted to find optimum conditions. The experimental results show that the copper wires should be maintained at or above $950^{\circ}C$ for rapid removal of the polyester. The simulation and experimental results are discussed with respect to the microstrucrual evolution during heating of the copper wires.

Development and Application of Anti-Corrosive Steel Using Electro-Deposition of Sea Water (1) -Development of Electro-Deposition System Using Sea Water (해수전착 코팅을 이용한 내부식성 철근의 개발 및 적용성에 대한 연구 (1) -해수전착 코팅 시스템 개발)

  • Kwon, Seung Jun;Lee, Myeong Hoon;Park, Sang Soon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.5
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    • pp.78-87
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    • 2012
  • This study is for developing a system for electro-deposition utilizing sea water containing various ions like calcium and magnesium. This is the first step research for the final goal which is a development of anti-corrosive steel for RC structure, so that this paper is mainly focused on the development for electro-deposition system. Optimum conditions for steel coating is obtained through various tests considering anode type, temperature, duration time, and current density. The composition of electro-deposition is analyzed through SEM, EDS, and XRD and it is evaluated to be $CaCO_3$ and $Mg(OH)_2$. Through measuring polarization potential and current density in the coated steel, the coating layer from the developed system is evaluated to have high resistance to steel corrosion. Additional tests and discussions on durability and structural performance in the coated steel from this work will be performed for the second step research.

Interfacial Durability and Acoustic Properties of Transparent xGnP/PVDF/xGnP Graphite Composites Film for Acoustic Actuator (음향 작동기를 위한 투명한 xGnP/PVDF/xGnP 그래핀 복합재료 필름의 계면 내구성 및 음향 특성)

  • Gu, Ga-Young;Wang, Zuo-Jia;Kwon, Dong-Jun;Park, Joung-Man
    • Composites Research
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    • v.25 no.3
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    • pp.70-75
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    • 2012
  • Interfacial durability and electrical properties of CNT, ITO or xGnP coated PVDF nanocomposites were investigated for acoustic actuator applications. The xGnP coated PVDF nanocomposite exhibited better electrical conductivity than CNT and ITO case due to the unique electrical property of xGnP, and this nanocomposite also showed good sound characteristics. Interfacial adhesion durability between either neat CNT or plasma treated CNT and plasma treated PVDF were measured by static contact angle, surface energy, work of adhesion, and spreading coefficient tests. The optimum acoustic actuation performance of xGnP coated PVDF nanocomposite was measured using sound level meter with changing radius of curvature and coating conditions. As compared to CNT and ITO, the xGnP was known as more appropriate acoustic actuator due to the characteristic electrical property. It is the most appropriate condition when the radius of curvature is 15 degree. Although sound characteristics were different with various coating thicknesses, it is possible to manufacture transparent actuator with good sound quality.

A Study on the Degradation of Isopropyl Alcohol with $TiO_{2}$-coated Metal (광촉매 코팅 금속의 IPA 분해 특성 연구)

  • Yu Dong-Sik;Park Jae-Hyeon;Ha Jin-Wook
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.6 no.5
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    • pp.418-422
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    • 2005
  • The degradation of IPA according to coating conditions was examined by $TiO_{2}$/p-25-coated aluminium metal plate. Inorganic(KR-400), inorganic$\cdot$ organic hybrid(TMOS) and organic(A-9540) resins were used as binder $TiO_{2}$ coated surface of aluminum metal plate was clear with all binders, and the adhesion of binders was good except inorganic binder. The activity for IPA degradation appeared to range in order A-9540>TMOS>KR-400. The optimum activity was obtained when the ratio of TMOS and P-25 was 1.6:10, and when the ratio of A-9540 and P-25 was 1.0:6.0, respectly.

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Optimalization of ELISA using Recombinant p27 Protein of SIV for Detection of Anti-SIV (SIV의 p27 재조합 단백질을 이용한 SIV 항체 검출을 위한 ELISA의 최적 조건)

  • Kim, Eun-ok;Kim, Eun;Oh, Yoon-i;Shin, Kwang-soon;Kim, Hyun-soo;Kim, Chul-joong
    • Korean Journal of Veterinary Research
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    • v.42 no.1
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    • pp.101-108
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    • 2002
  • The p27 coding region of the SIVmac239 isolate was amplified by PCR and cloned into an expression vector, pMAL-cri, which expressed high levels of the p27 protein from Escherichia coli. The purified p27 protein was used for detection of anti-SIV antibodies with the sera from 11 macaques and 21 marmosets by immunoblot assay of which one macaque was suspicious for the SIV infection. The optimum conditions of ELISA was studied by the check board system with the recombinant purified p27 protein. For the plate coating, 200ng/well of the purified p27 was satisfactory. The conjugate was diluted 1:1000. The sera from the 32 monkeys were negative for the anti-SIV by ELISA.

Antimicrobial Activity of Polylysine Coated Film (Polylysine 코팅 필름의 항균활성)

  • Kim Seong-Cheol;Kim Jong-Chan;Park Kee-Jai;Choi Jong-Uck;Jeong Seung-Weon
    • Food Science and Preservation
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    • v.12 no.4
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    • pp.323-328
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    • 2005
  • This study were investigated to analyzed an optimum preparation condition of coating film and its antimicrobial activity on pathogenic and deteriorative bacteria to obtain fundamental data for development of active packaging film using antimicrobial peptide, polysine. In the preparation conditions of coating film, antimicrobial activity was depending on the concentration of polylysine and polyamide respectively, and relatively high activity was obtained in the film prepared with more than $1.0\%$ (w/v) of polylysine, $40\%$ (w/v) polyamide, and more than $50\;{\mu}m$ of film thickness. Concentration of polylysine migrated from coated film to distilled water was reached at the maximum concentration, about 20 ppm after 3 days and in equilibrium after 7 days of soaking in sterilized water. An antimicrobial activity of coated film showed bactericidal effect of about $10^5\;CFU/mL$ comparing with the control against Bacillus cereus having $4.8{\times}10^5\;CFU/mL$ of initial viable cell numbers, and of about $10^2\;CFU/mL$ comparing with the control against Klebsiella pneumoniae having $6.8{\times}10^5\;CFU/mL$ of initial viable cell numbers. Consequently, it was revealed that polylysine coating film has a potential of applicable possibility as antimicrobial packaging film.

Optimization of anode and electrolyte microstructure for Solid Oxide Fuel Cells (고체산화물 연료전지 연료극 및 전해질 미세구조 최적화)

  • Noh, Jong Hyeok;Myung, Jae-ha
    • Korean Chemical Engineering Research
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    • v.57 no.4
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    • pp.525-530
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    • 2019
  • The performance and stability of solid oxide fuel cells (SOFCs) depend on the microstructure of the electrode and electrolyte. In anode, porosity and pore distribution affect the active site and fuel gas transfer. In an electrolyte, density and thickness determine the ohmic resistance. To optimizing these conditions, using costly method cannot be a suitable research plan for aiming at commercialization. To solve these drawbacks, we made high performance unit cells with low cost and highly efficient ceramic processes. We selected the NiO-YSZ cermet that is a commercial anode material and used facile methods like die pressing and dip coating process. The porosity of anode was controlled by the amount of carbon black (CB) pore former from 10 wt% to 20 wt% and final sintering temperature from $1350^{\circ}C$ to $1450^{\circ}C$. To achieve a dense thin film electrolyte, the thickness and microstructure of electrolyte were controlled by changing the YSZ loading (vol%) of the slurry from 1 vol% to 5 vol. From results, we achieved the 40% porosity that is well known as an optimum value in Ni-YSZ anode, by adding 15wt% of CB and sintering at $1350^{\circ}C$. YSZ electrolyte thickness was controllable from $2{\mu}m$ to $28{\mu}m$ and dense microstructure is formed at 3vol% of YSZ loading via dip coating process. Finally, a unit cell composed of Ni-YSZ anode with 40% porosity, YSZ electrolyte with a $22{\mu}m$ thickness and LSM-YSZ cathode had a maximum power density of $1.426Wcm^{-2}$ at $800^{\circ}C$.

Modern Paper Quality Control

  • Olavi Komppa
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2000.06a
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    • pp.16-23
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    • 2000
  • The increasing functional needs of top-quality printing papers and packaging paperboards, and especially the rapid developments in electronic printing processes and various computer printers during past few years, set new targets and requirements for modern paper quality. Most of these paper grades of today have relatively high filler content, are moderately or heavily calendered , and have many coating layers for the best appearance and performance. In practice, this means that many of the traditional quality assurance methods, mostly designed to measure papers made of pure. native pulp only, can not reliably (or at all) be used to analyze or rank the quality of modern papers. Hence, introduction of new measurement techniques is necessary to assure and further develop the paper quality today and in the future. Paper formation , i.e. small scale (millimeter scale) variation of basis weight, is the most important quality parameter of paper-making due to its influence on practically all the other quality properties of paper. The ideal paper would be completely uniform so that the basis weight of each small point (area) measured would be the same. In practice, of course, this is not possible because there always exists relatively large local variations in paper. However, these small scale basis weight variations are the major reason for many other quality problems, including calender blacking uneven coating result, uneven printing result, etc. The traditionally used visual inspection or optical measurement of the paper does not give us a reliable understanding of the material variations in the paper because in modern paper making process the optical behavior of paper is strongly affected by using e.g. fillers, dye or coating colors. Futhermore, the opacity (optical density) of the paper is changed at different process stages like wet pressing and calendering. The greatest advantage of using beta transmission method to measure paper formation is that it can be very reliably calibrated to measure true basis weight variation of all kinds of paper and board, independently on sample basis weight or paper grade. This gives us the possibility to measure, compare and judge papers made of different raw materials, different color, or even to measure heavily calendered, coated or printed papers. Scientific research of paper physics has shown that the orientation of the top layer (paper surface) fibers of the sheet paly the key role in paper curling and cockling , causing the typical practical problems (paper jam) with modern fax and copy machines, electronic printing , etc. On the other hand, the fiber orientation at the surface and middle layer of the sheet controls the bending stiffness of paperboard . Therefore, a reliable measurement of paper surface fiber orientation gives us a magnificent tool to investigate and predict paper curling and coclking tendency, and provides the necessary information to finetune, the manufacturing process for optimum quality. many papers, especially heavily calendered and coated grades, do resist liquid and gas penetration very much, bing beyond the measurement range of the traditional instruments or resulting invonveniently long measuring time per sample . The increased surface hardness and use of filler minerals and mechanical pulp make a reliable, nonleaking sample contact to the measurement head a challenge of its own. Paper surface coating causes, as expected, a layer which has completely different permeability characteristics compared to the other layer of the sheet. The latest developments in sensor technologies have made it possible to reliably measure gas flow in well controlled conditions, allowing us to investigate the gas penetration of open structures, such as cigarette paper, tissue or sack paper, and in the low permeability range analyze even fully greaseproof papers, silicon papers, heavily coated papers and boards or even detect defects in barrier coatings ! Even nitrogen or helium may be used as the gas, giving us completely new possibilities to rank the products or to find correlation to critical process or converting parameters. All the modern paper machines include many on-line measuring instruments which are used to give the necessary information for automatic process control systems. hence, the reliability of this information obtained from different sensors is vital for good optimizing and process stability. If any of these on-line sensors do not operate perfectly ass planned (having even small measurement error or malfunction ), the process control will set the machine to operate away from the optimum , resulting loss of profit or eventual problems in quality or runnability. To assure optimum operation of the paper machines, a novel quality assurance policy for the on-line measurements has been developed, including control procedures utilizing traceable, accredited standards for the best reliability and performance.

Tribological Behaviour of $WS_2$Solid Lubricant ($WS_2$ 고체윤활제의 마찰.마모 거동)

  • 신동우;김인섭;윤대현;김경도;김성진;정진수
    • Tribology and Lubricants
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    • v.14 no.2
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    • pp.35-41
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    • 1998
  • The $WS_2$ solid lubricant synthesized through the vapour phase transport method was coated on the commercial bearing steel (SUJ 2) substrate, and the tribological behaviour of the lubricant was investigated using a ball-on-disk type tester. The $WS_2$ powder was spray-coated at room temperature using compressed air, and the change of friction coefficient was examined in various conditions, i.e., specimen configuration, atmosphere (air and nitrogen), applied load and rotating speed. $WS_2$ coated ball and disk showed the optimum friction coefficient of 0.07 and wear life of 45,000 cycles in the nitrogen atmosphere under 0.3 kgf and 100 rpm, whereas relatively high coefficient of 0.13 and reduced wear life of 4,000 cycles were observed in air atmosphere. The effect of rotating speed on the friction coefficient was not observed both in nitrogen and in air atmospheres. This confirmed that the spray-coated $WS_2$ solid lubricant was effective in reducing the friction coefficient and improving wear life in nitrogen atmosphere, and the oxygen and moisture existing in air could seriously deteriorate the lubrication effect of $WS_2$ coating layer.

Fabrication of SiCN microstructures for super-high temperature MEMS using photopolymerization and its characteristics (광중합에 의한 초고온 MEMS용 SiCN 미세구조물 제작과 그 특성)

  • Chung, Gwiy-Sang
    • Journal of Sensor Science and Technology
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    • v.15 no.2
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    • pp.148-152
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    • 2006
  • This paper describes the fabrication of SiCN microstructures for super-high temperature MEMS using photopolymerization of pre-ceramic polymer. In this work, polysilazane liquide as a precursor was deposited on Si wafers by spin coating, microstructured and solidificated by UV lithography, and removed from the substrate. The resulting solid polymer microstructures were cross-linked under HIP process and pyrolyzed to form a ceramic of withstanding over $1400^{\circ}C$. Finally, the fabricated SiCN microstructures were annealed at $1400^{\circ}C$ in a nitrogen atmosphere. Mechanical characteristics of the SiCN microstructure with different fabrication process conditions were evaluated. The elastic modules, hardness and tensile strength of the SiC microstructure implemented under optimum process condtions are 94.5 GPa, 10.5 GPa and 11.7 N/min, respectively. Consequently, the SiCN microstructure proposed in this work is very suitable for super-high temperature MEMS application due to very simple fabrication process and the potential possiblity of sophisticated mulitlayer or 3D microstructures as well as its good mechanical properties.