• Food Science and Biotechnology
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• v.15 no.1
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• pp.24-27
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• 2006

A simple HPLC quantification method was developed for genistein, genistin, daidzein, and daidzin in soybeans and soybean products. The procedure used a $4.6{\times}100\;mm$ $Chromolith^{(R)}$ RP-18e column with a mobile phase of 1% HOAc in 20% MeOH to 1% HOAc in 80% MeOH for 10 min. The injection volume was $2\;{\mu}L$ at a flow rate of 2 mL/min. Detection was carried out under UV at 254 nm. Under these conditions, the major isoflavones daidzein, daidzin, genistein, and genistin in soybean and soybean pastes were eluted within 7 min with baseline separation. Optimal extraction of the above four major isoflavones was achieved when 40 g of soybean or soybean paste was refluxed in 100 mL of 95% ethanol for 2 hr. Ten different soybean cultivars and nine commercial soybean pastes were analyzed by this method. The total isoflavone content was highest in the cultivar Somyung ($2,497\;{\mu}g/g$ dry weight). The isoflavone content in soybean pastes varied widely from manufacturer to manufacturer (an almost five-fold difference between the highest and lowest values). Such variations were presumably due to differences in fermentation conditions, type of soybeans used, and levels of such additives as starch and salt.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2010.11a
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• pp.833-837
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• 2010

This study aims at finding an optimal exhaust diffuser design of a high altitude testing chamber for a low bypass turbofan engine (F404-402) with thrust pound force of 17,700 and air mass flow rate of 66kg/s ejecting at a speed of Mach 1.66. The final proposed ejector size has better pressure recovery characteristics and targets to reduce operational cost at engine performance testing. Conventional high altitude test chamber layout was adopted and first drawn in two dimensions using Autocad software so as to determine the gas path, the ejector frontal size was then determined from gas dynamics equations considering traditional gas ejection method where both the engine exhaust and cell cooling air are exhausted via the ejector. Modification to a smaller ejector with an alternative secondary cell cooling exhaust port was then performed and modelled in 3D using Solid Works software.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.26 no.12
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• pp.579-587
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• 2014

This paper deals with precise analytical state equation modeling of a variable speed refrigeration system (VSRS) for optimum control in state space. The VSRS is described as multi-input and multi-output (MIMO) system, which has two controlled variables and two control inputs. First, the Navier-Stokes equation and mass flow rate were applied to each component of the basic refrigeration cycle to build a dynamic model. The dynamic model, represented by a differential equation, was transformed into the state equation formula. Next, a full-order state observer was built to estimate all of the state variables to compose an optimum control system. Then, an optimum controller was designed to minimize an evaluation function that has input energy and control error. Finally, simulations and experiments were conducted to verify the validity of the proposed modeling and designed optimum controller to regulate target temperature and superheat in a 1RT oil cooler system. The results show that the proposed method, state equation modeling and optimum control, is efficient to ensure optimal control performance of the VSRS.

• Proceedings of the SAREK Conference
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• 2008.11a
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• pp.203-211
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• 2008

The optimal design of two stage evaporation & absorption system which is related to the large temperature difference system was investigated numerically in the absorption refrigeration system. The concentrations at inlet & oulet of absorber are 62.9% and 56.9%, but in two stage absorption system the values are 62.2% and 56.2%. Therefore strong solution & weak solution became diluted than the standard value. The amount of weak solution circulation can be reduced in absorption refrigeration system, and the sensible heat load is more reduced to enhance the COP of system. As UAR is increased, COP becomes larger, and this means the role of top section is more important than bottom section in two stage evaporation & absorption system. But the increase of COP becomes slower at 0.7 of UAR ratio. The performance of Type2 is higher than Type1 in COP with the flow direction of cooling waters. This phenomena is due to the active absorption of vapor -absorption & lower temp. cooling water is more effective. The pressure at bottom section becomes higher & that at top section becomes lower and therefore the circulation rate can be diminished more.

• YAKHAK HOEJI
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• v.52 no.6
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• pp.446-451
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• 2008

A high-performance liquid chromatography (HPLC) with diode array detector (DAD) and electrospray ionization mass spectrometry (ESI-MS) was established for the simultaneous determination of chlorogenic acid (1), sweroside (2), luteolin-7-O-glucoside (3), (E)-aldosecologanin (4) and 3,5-dicaffeoylquinic acid (5) from Lonicera joponica flower buds. The optimal chromatographic conditions were obtained on an ODS column (5 ${\mu}m$, 4.6${\times}$150 mm) with the column temperature $25^{\circ}C$. The mobile phase was composed of (A) water with 0.1% formic acid and (B) acetonitrile with 0.1% formic acid using a gradient elution, the flow rate was 0.3 ml/min. Detection wavelength was set at 250 nm. All calibration curves showed good linear regression ($r^2$>0.994) within test ranges. The developed method provided satisfactory precision and accuracy with overall intra-day and inter-day variations of 0.05${\sim}$1.95% and 0.15${\sim}$2.26%, respectively, and the overall recoveries of 97.71${\sim}$103.65% for the five compounds analyzed. The verified method was successfully applied to quantitative determination of the three types (phenolic compounds, iridoids and flavonoids) of bioactive compounds in 21 commercial L. japonica flower buds samples from different markets in Korea and China. The analytical results demonstrated that the contents of the five analytes vary significantly with sources.

• Journal of the Earthquake Engineering Society of Korea
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• v.24 no.5
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• pp.211-217
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• 2020

Earthquake preparedness has become more important with recent increase in the number of earthquakes in Korea, but many existing structures are not prepared for earthquakes. There are various types of liquefaction prevention method that can be applied, such as compaction, replacement, dewatering, and inhibition of shear strain. However, most of the liquefaction prevention methods are applied before construction, and it is important to find optimal methods that can be applied to existing structures and that have few effects on the environment, such as noise, vibration, and changes in underground water level. The purpose of this study is to estimate the correlation between the displacement of a structure and variations of pore water pressure on the ground in accordance with the depth of the sheet file when liquidation occurs. To achieve this, a shaking table test was performed for Joo-Mun-Jin standard sand and an earth pressure, accelerometer, pore water pressure transducer, and LVDT were installed in both the non-liquefiable layer and the liquefiable layer to measure the subsidence and excess pore water pressure in accordance with the time of each embedded depth. Then the results were analyzed. A comparison of the pore water pressure in accordance with Hsp/Hsl was shown to prevent lateral water flow at 1, 0.85 and confirmed that the pore water pressure increased. In addition, the relationship between Hsp/Hsl and subsidence was expressed as a trend line to calculate the expected settlement rate formula for the embedded depth ratio.

• Korean Chemical Engineering Research
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• v.56 no.2
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• pp.176-185
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• 2018

As global warming accelerates, greenhouse gas reduction becomes more important. Carbon dioxide dry reforming is a promising green-house gas reduction technology that can obtain CO and $H_2$ which are high value-added materials by utilizing $CO_2$ and $CH_4$ which are greenhouse gases. However, there is a significant coking problem during operation of the dry reforming reactor. Because the carbon dioxide dry reforming is a strong endothermic reaction, the temperature of the reactor drops near the reactor inlet and causes coke formation. To solve this problem, it is important to ensure that the reaction takes place in a temperature range where coke production is minimized. In this study, we proposed a design method that can maintain reaction temperature in the region where the coke is rarely generated by using the new catalyst configuration method. The design method also optimizes the reactor by solving the optimization problem which minimizes the reactor length for a given reaction conversion by using the fuel flow rate, catalyst density, and output temperature by section as optimization variables.

• Journal of Electrochemical Science and Technology
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• v.9 no.1
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• pp.37-43
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• 2018

In order to improve current efficiency and decrease energy consumption in the electrosynthesis of ammonium persulfate, electrolytic properties of four cation exchange membranes, namely, the $JCM-II^{(R)}$ membrane, $Nafion^{(R)}$ 324 membrane CMI-$7000^{(R)}$ membrane and a self-made perfluorosulfonic ion exchange membrane (PGN membrane) were investigated using a sintered platinized titanium anode and a Pb-Sb-Sn alloy cathode in a self-made electrolytic cell. The effect of cell voltage and electrolyte flow rate on the current efficiency and the energy consumption were investigated. The results indicated that the PGN membrane could improve current efficiency to 94.85% and decrease energy consumption to $1119kWh\;t^{-1}$ (energy consumption per ton of the ammonium persulfate generated) under the optimal operating conditions and the highest current efficiency of the $JCM-II^{(R)}$ membrane, $Nafion^{(R)}$ 324 membrane and CMI-$7000^{(R)}$ membrane were 80.73%, 77.76% and 73.22% with their lowest energy consumption of $1323kWh\;t^{-1}$, $1539kWh\;t^{-1}$ and $2256kWh\;t^{-1}$, respectively. The PGN membrane has the advantages of high current efficiency and energy power consumption and has sufficient mechanical strength with the reinforced mesh. Therefore the PGN membrane will has good value in popularization in the industrial electrosynthesis of ammonium persulfate in the future.

• Journal of Environmental Health Sciences
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• v.36 no.5
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• pp.383-390
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• 2010

Exposure to fugitive dust can contribute to several respiratory health problems, and proper sampling of fugitive dust is necessary to assess exposure. However, field sampling of soil dust encounters problems from spatial and temporal differences in soil properties, field operations, and meteorological conditions. To minimize these problems, we designed a dust generator that simulates dust generation from soil. The dust generator consisted of a rotating chamber where soil samples were loaded and tumbled, and a settling chamber, where airborne soil dust samples were collected. As standard operating conditions, we decided on 2 g soil mass, 10 min sampling time, and 20 rpm rotating speed, with a flow rate of 30 l/min, based on three common soil textures of loam, sandy loam and silt loam. To evaluate optimal operating conditions, we used mixtures of Joomoonjin silica sand and clay. Although the average $PM_{10}$ concentration of Joomoonjin silica sand was low, dust concentrations were increased by an increased content of clay. The dust concentrations were consistent across repeated experiments, and showed similar concentration profiles during the sampling time with mixtures of clay and sand (coefficient of variation was $13.6{\pm}w;7.1%$). The results demonstrated that these standard operating conditions were suitable for the dust generator, which can be used to investigate variations in soil properties that affect dust production and potential potency of fugitive dust exposure.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.17 no.1
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• pp.290-297
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• 2016

The performance of track cleaning trains to remove accumulated fine particulate matter in subway tunnels depends on the design of the suction system equipped under the train. To increase the efficiency of the suction system under the cleaning vehicle, this paper proposes a novel dust suction module equipped with both air blowing nozzles and a dust suction structure. Computational Fluid Dynamics (CFD) analysis with turbulent flow was conducted to optimize the dust suction system with a particle intake and blowing function. The optimal angle of the air blowing nozzle to maximize the dust removal rate was found to be 6 degrees. The performance of the track cleaning vehicle can be increased by at least 10 percent under an operation speed of 5km/h.