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Effect of Post-Weld Heat Treatment on the Mechanical Properties and Microstructure of P-No. 1 Carbon Steels (P-No. 1 탄소강의 기계적 특성과 미세조직에 미치는 용접후열처리의 영향)

  • Lee, Seung-Gun;Kang, Yongjoon;Kim, Gi-Dong;Kang, Sung-Sik
    • Journal of Welding and Joining
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    • v.35 no.1
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    • pp.26-33
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    • 2017
  • This study aims to investigate the suitability of requirement for post-weld heat treatment(PWHT) temperature when different P-No. materials are welded, which is defined by ASME Sec. III Code. For SA-516 Gr. 60 and SA-106 Gr. B carbon steels that are typical P-No. 1 material, simulated heat treatment were conducted for 8 h at $610^{\circ}C$, $650^{\circ}C$, $690^{\circ}C$, and $730^{\circ}C$, last two temperature falls in the temperature of PWHT for P-No. 5A low-alloy steels. Tensile and Charpy impact tests were performed for the heat-treated specimens, and then microstructure was analyzed by optical microscopy and scanning electron microscopy with energy-dispersive spectrometry. The Charpy impact properties deteriorated significantly mainly due to a large amount of cementite precipitation when the temperature of simulated heat treatment was $730^{\circ}C$. Therefore, when dissimilar metal welding is carried out for P-No. 1 carbon steel and different P-No. low alloy steel, the PWHT temperature should be carefully selected to avoid significant deterioration of impact properties for P-No. 1 carbon steel.

Correlation between Capacitance and Structure-optical Properties of Semiconductor with Zero Leakage Current (누설전류 Zero인 반도체 물질의 구조적 광학적 특성과 전도성과의 상관성)

  • Yun, Tae Hwan;Oh, Teresa
    • Journal of the Semiconductor & Display Technology
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    • v.14 no.3
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    • pp.27-31
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    • 2015
  • It was the electrical properties of ZnS treated by the annealing in a vaccum and an atmosphere conditions to reseached the leakage current effect of semiconductor devices. Most samples were shown the non-linear with unipolar properties, but the ZnS annealed at $100^{\circ}C$ in a vaccum was only observed no leakage current in a range of -20 V< voltage < 15 V. The crystallinity of ZnS with no leakage current was improved and optical property was also improved. Because the ambipolar characteristics and low leakage currents originated from the extension effect of a depletion width by electron-hole combination in the depletion layer.

Combining Conditional Generative Adversarial Network and Regression-based Calibration for Cloud Removal of Optical Imagery (광학 영상의 구름 제거를 위한 조건부 생성적 적대 신경망과 회귀 기반 보정의 결합)

  • Kwak, Geun-Ho;Park, Soyeon;Park, No-Wook
    • Korean Journal of Remote Sensing
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    • v.38 no.6_1
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    • pp.1357-1369
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    • 2022
  • Cloud removal is an essential image processing step for any task requiring time-series optical images, such as vegetation monitoring and change detection. This paper presents a two-stage cloud removal method that combines conditional generative adversarial networks (cGANs) with regression-based calibration to construct a cloud-free time-series optical image set. In the first stage, the cGANs generate initial prediction results using quantitative relationships between optical and synthetic aperture radar images. In the second stage, the relationships between the predicted results and the actual values in non-cloud areas are first quantified via random forest-based regression modeling and then used to calibrate the cGAN-based prediction results. The potential of the proposed method was evaluated from a cloud removal experiment using Sentinel-2 and COSMO-SkyMed images in the rice field cultivation area of Gimje. The cGAN model could effectively predict the reflectance values in the cloud-contaminated rice fields where severe changes in physical surface conditions happened. Moreover, the regression-based calibration in the second stage could improve the prediction accuracy, compared with a regression-based cloud removal method using a supplementary image that is temporally distant from the target image. These experimental results indicate that the proposed method can be effectively applied to restore cloud-contaminated areas when cloud-free optical images are unavailable for environmental monitoring.

Color Enhancement of the Type II and Type I aB Brown Diamonds into Colorless by HPHT Process (고온고압법에 의한 Type II, Type I aB 갈색 다이아몬드의 색향상)

  • Song, Jeong-Ho;Song, Oh-Sung
    • Journal of the Korean Ceramic Society
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    • v.49 no.3
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    • pp.221-225
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    • 2012
  • It is possible to enhance the color of the natural diamond with a high pressure high temperature(HPHT) process. We employed a pyrophyllite tube cell and cubic press apparatus for HPHT treatment on the brown colored Type II (5.6 GPa/ $1700^{\circ}C$/ 52 min), and Type I aB(5.6 GPa/ $1650^{\circ}C$/ 30 min) diamond samples. We investigated the microstructure, Types, fluorescence, properties of the diamonds with an optical microscopy, FT-IR, photoluminescence(PL) spectroscopy, Diamond-View, and micro-Raman spectroscopy. Two tinted brown diamonds changed into colorless just after the HPHT process. Optical microscopy showed that no crack and significant inclusion evolution occurred during the HPHT process except the small graphite spot appeared in Type I aB sample. FTIR spectrum confirmed that no Type, amber center, and platelet defect change with the HPHT treatment. Diamond-View could not distinguish the HPHT treated diamonds from the naturals. PL spectroscopy showed that N3 and H3 color centers remained even after HPHT process. Consequently, we successfully changed the color of diamonds into colorless by 5.6 GPa HPHT process.

Simultaneous active strain and ultrasonic measurement using fiber acoustic wave piezoelectric transducers

  • Lee, J.R.;Park, C.Y.;Kong, C.W.
    • Smart Structures and Systems
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    • v.11 no.2
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    • pp.185-197
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    • 2013
  • We developed a simultaneous strain measurement and damage detection technique using a pair of surface-mounted piezoelectric transducers and a fiber connecting them. This is a novel sensor configuration of the fiber acoustic wave (FAW) piezoelectric transducer. In this study, lead-zirconate-titanate (PZT) transducers are installed conventionally on a plate's surface, which is a technique used in many structural health monitoring studies. However, our PZTs are also connected with an optical fiber. A FAW and Lamb wave are simultaneously guided in the optical fiber and the structure, respectively. The dependency of the time-of-flight of the FAW on the applied strain is quantified for strain sensing. In our experimental results, the FAW exhibited excellent linear behavior and no hysteresis with respect to the change in strain. On the other hand, the well-known damage detection function of the surface-mounted PZT transducers was still available by monitoring the waveform change in the conventional Lamb wave ultrasonic path.

Chiral Purity Test of Metoprolol Enantiomer After Derivatization with (-)-Menthyl Chloroformate by Reversed-Phase High Performance Liquid Chromatography

  • Kim, Kyeong-Ho;Choi, Pok-Wha;Hong, Seon-Pyo;Kim, Hyun-Ju
    • Archives of Pharmacal Research
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    • v.22 no.6
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    • pp.614-618
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    • 1999
  • A reversed-phase high-performace liquid chromatographic method was developed to determine the optical purity of metoprolol enantiomers. The enantiomers were converted to diastereomeric derivatives using (-)-menthyl chloroformate reagent. Separation of the enantiomers as diastereomers was achieved by reversed-phase HPLC within 30 min using Inertsil C8 column. This method allowed determination of 0.05% of either enantiomer in the presence of its stereoisomer and method validation showed adequate linearity over the required range. Owing to the reaction condition during the derivatization with (-)-menthyl chloroformate, the possibility of racemization had to be established. Different ratios of (S)-(-)-metoprolol and (R)-(+)-metoprolol were prepared. Enantiomeric separation of these mixtures took place on a chiralcel OD column or, after derivatization with (-)-menthyl chloroformate, on a C8 column. The results form the these two independent separation systems were compared with trace racemization and were in very good agreement. No racemization was found during the experiment.

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New Compensation Method for Temperature Sensitivity of Fiber Brags Grating Using Bi-metal

  • Chung, Young-Joo;Song, Jong-Seob;Han, Won-Taek;Paek, Un-Chul
    • Journal of the Optical Society of Korea
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    • v.7 no.2
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    • pp.84-88
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    • 2003
  • A new method for temperature compensation of fiber Bragg grating (FBG) using hi-metal is proposed and experimentally demonstrated. Bi-metal bends toward the metal of low temperature expansion coefficient as the temperature increases, and this property is utilized to cancel the thermo-optic effect of the fiber. The optimum thickness of the high coefficient metal was empirically found by the trial-and-error method. The temperature sensitivities were 8.1 pm/$^{\circ}C$ and -0.018 pm/$^{\circ}C$ for the uncompensated and compensated FBGs, respectively, which indicates a reduction to a mere 0.22 % of the original sensitivity. No appreciable change in the spectral shape was observed. The packaging technique described in this paper is simple and compact, and it can be used for FBGs in WDM and DWDM communication systems that have stringent requirements on the temperature stability of the components.

$NO_x$ Sensing Characteristic of $TiO_2$ Thin Film Deposited by R.F Magnetron Sputtering (R.F 마그네트론 스퍼트링으로 작성된 $TiO_2$박막의 $NO_x$ 감지 특성)

  • 고희석;박재윤;박상현
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.51 no.12
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    • pp.567-572
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    • 2002
  • In these days, diesel vehicle or power plant emits $NO_X\; and SO_2$ which cause air pollution like acid-rain, ozone layer destroy and optical smoke, therefore there are many kinds of methods considered for removing them such as SCR, catalyst, plasma process, and plasma-catalyst hybrid process. T$TiO_2$ is commonly used as catalyst to remove $NO_X$ gas because it have very excellent chemical characteristic as photo catalyst. In this paper, $NO_X$ sensing characteristic of $TiO_2$ thin film deposited by R.F Magnetron sputtering is investigated. A finger shaped electrode on $Al_2$O$_3$ substrate is designed and $TiO_2$ is deposited on the electrode by the magnetron sputtering deposition system. Chemical composition of the deposited $TiO_2$ thin film is $TiO_{1.9}$ by RBS analysis. When the UV is irradiated on it with flowing air, capacitance of $TiO_2$ thin film increases, however, when NO gas is put into the system with air, it immediately decreases because of photo chemical reaction. and it monotonously decreases with increasing NO concentration.

An Optical Configuration for Vertical Alignment Liquid Crystal cell with Wide Viewing Angle

  • Ji, Seung-Hoon;Lee, Gi-Dong
    • Journal of Information Display
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    • v.9 no.2
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    • pp.22-27
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    • 2008
  • We propose an optical configuration of a vertical alignment (VA) liquid crystal (LC) cell to eliminate the light leakage in the diagonal direction. VA LC cell has an excellent contrast ratio in the normal direction due to the no phase-retardation. However, change of the phase-retardation occurs in all directions, which causes the light leakage and deteriorates the characteristics of the dark state. We designed the LC cell structure composed of multiple combinations with two A-plates and two C-plates in order to achieve wide viewing property on the Poincare sphere. From calculations, we show that the proposed structure can improve the viewing angle characteristics by compensating for the light leakage in all directions.

J-aggregates of Merocyanine Dye : formation and structural change on chemical and thermal treatments (메로시아닌 색소의 J-회합체 ; 형성과 열.화학적인 처리에 의한 변화)

  • Shin, Hoon-Kyu;Kwon, Young-Soo
    • Proceedings of the KIEE Conference
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    • 1998.07d
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    • pp.1398-1400
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    • 1998
  • The physical properties of the LB films with merocyanine dyes have been published and attract attention due to the possibility of molecular structure control. The evaluation of the thin films was focused for the purpose of molecular structure control. The molecular structure in the case of the thin films with dyes can be examine by optical absorption spectra measurements. In the case of optical absorption spectra of the LB films by the heat treatment at $70^{\circ}C$ in the air, both of the shifted absorption bands decay and a monomer absorption peak of about 530 nm appears instead. And, the formation and dissociation of J-aggregates, anisotropic behavior was no longer observed in the heat treated merocyanine dyes LB films. In the results, study of the merocyanine dyes LB films using optical absorption spectra would an interesting problem of absorption peak shifts and mixed components.

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