• Title/Summary/Keyword: Oil-drying

Search Result 181, Processing Time 0.027 seconds

Analysis of Binding Media Used in Mural Painting of Temple Wall by Pyrolysis/GC/MS and IR (열분해/GC/MS와 IR을 이용한 사찰 벽화 시편 교착제 분석)

  • Park, Jongseo;Lee, Jeong Won
    • Journal of Conservation Science
    • /
    • v.33 no.5
    • /
    • pp.345-354
    • /
    • 2017
  • A mural was discovered in the Ssanggyesa temple located in Jindo island, during repair of the Daeungjeon Hall. A study was conducted to determine the binding medium used for preparing the mural. Pyrolysis/GC/MS and IR spectrometry were used to analyze a painting specimen. Direct approach and on-line methylation approach were attempted for the pyrolysis/GC/MS. In IR analysis, the spectra of the specimen were found to be different from those of Asian lacquer, yellow lacquer, animal glue, and acrylic emulsion resin. They were also not identical to the standard IR spectra of drying oils such as linseed oil. Pyrolysis/GC/MS results of the specimen were different from those of Asian lacquer, yellow lacquer, animal glue, and acrylic emulsion resin. In the mean time, palmitic acid, octadecanoic acid, nonanedioic acid, and octadecenoic acid, which are characteristic pyrolysis products of dried drying oil, were detected. In addition, the pyrolysis/GC/MS chromatograms of the specimen and dried drying oil were also very similar. Therefore, it was concluded that the painting was prepared using drying oil as a binding medium.

Ultrasonic Immersion-steam Cleaning and High Temperature Drying Process for Removing Cutting Oil on Titanium Turning Scraps (타이타늄 터닝 스크랩 내 절삭유 제거를 위한 초음파 침지-스팀 및 고온 건조 공정)

  • Chae, Jikwang;Yoo, Suhwan;Oh, Jung-Min;Lim, Jae-Won
    • Resources Recycling
    • /
    • v.30 no.1
    • /
    • pp.60-65
    • /
    • 2021
  • The recycling of titanium turning scraps requires the removal of cutting oil and other contaminants remaining on the surface. In this study, an experiment was conducted in which titanium scraps were cleaned by a combination of ultrasonic immersion-steam cleaning and subsequent drying at high temperature. To determine the removal mechanism of cutting oil, the contact angle between titanium surface and cutting oil was measured. The result confirmed the optimum condition of the immersion solution of the titanium turning scraps. In the case of immersion cleaning of Na4P2O7 aqueous solution, the degree of carbon removed in the cutting oil was the highest at 50℃, and it was confirmed that the carbon content obtained from the combination of steam cleaning and ultrasonic immersion-steam cleaning was lower than that from steam cleaning after ultrasonic immersion. The oxidation and decomposition behaviors of cutting oil were investigated using Thermogravimetric analysis (TGA) and the result was applied in the high temperature drying process. From the results of the high temperature drying tests, it was concluded that 200℃ is the optimal drying temperature.

Recovery of Petroleum Hydrocarbons from Oily Sludge Landfilled Soil

  • Shin, Su-Yeon;Park, Sang-Min;Ko, Sung-Hwan;Jung, Hong-Bae;Baek, Kitae
    • Journal of Soil and Groundwater Environment
    • /
    • v.20 no.5
    • /
    • pp.41-46
    • /
    • 2015
  • Three types of experiments, based on the physical properties of oily sludge landfilled soil, were conducted to recover total petroleum hydrocarbons (TPH) from the soil. These experiments included gravity separation, solvent extraction using water, and air floatation. The oil portion was not easily separated from the wet (raw) soil because water molecules aggregate the soil particles, despite the fact that the soil was sandy. However, the drying and grinding processes destroyed the aggregates, causing the TPH recovery to increase to approximately 60% when air floatation was used. The drying process decreased the specific gravity of the soil sample, thereby enhancing the overall recovery of TPH from the soil. Although thermal desorption and/or incineration are common choices for heavily dumped sites, physical separation can recover the oil portion instead of simply removing it.

A Study on the RDF Manufacturing of Coffee grounds by using Pilot scale Oil-drying Equipment (Pilot scale 유중건조 장비를 이용한 커피찌꺼기의 고형연료화 연구)

  • Kwon, Ik-Beom;Ha, Jin-Wook
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.20 no.2
    • /
    • pp.443-450
    • /
    • 2019
  • We studied to find the optimal manufacturing conditions of coffee grounds sludge RDF with oil drying method. We expanded the lab scale to pilot scale to compare the efficiency of the oil-drying equipment and The selection of the ratio of coffee grounds and oil, the setting temperature, and the temperature change and water content with time were measured. In order to analyze the characteristics of the research results, characteristics of solid fuels produced(Coffee grounds of oil-dried) by calorimeter, TGA, combustion equipment, and combustion gas measuring instrument were analyzed. As a result, the ratio of oil to coffee grounds was 4: 1, and when the setting temperature was set to $300^{\circ}C$, the water content reached 10wt.% or less within 20 minutes. ln addition, it showed high calorific value of 6,273kcal/kg. However, coffee grounds had a similar composition to wood and showed high luminance and produced a lot of CO in combustion gas. As a result, it is considered to be unsuitable for thermoelectric power plant and camping fuel, but the initial ignition speed is high and the heat generation is high, so it is considered that it can replace the fuels for current use.

Improvement of the Quality of Dried Wild Vegetables by Micro Oil Sprayed Thermal Air Technique

  • Yonghyun Kim;Yunmi Park;Chul-Woo Kim;Uk Lee;Hyun Ji Eo
    • Korean Journal of Plant Resources
    • /
    • v.35 no.6
    • /
    • pp.778-784
    • /
    • 2022
  • Wild vegetables, such as Cirsium setidens, and Aster scaber, are commonly distributed as dried materials because the wild vegetables lose their freshness quickly after harvest and distribution. Dried wild vegetables require rehydration to use as a food ingredient, and the quality of rehydrated wild vegetables is affected by pre-drying and drying methods. Here, we introduce the newly developed pre-drying and drying method, termed "micro oil sprayed thermal air (MOTA) technique". The three wild vegetables processed by the MOTA technique showed improved rehydration rate and reduced time to achieve maximum rehydration rate. Color characteristics were also improved in C. setidens. These results indicate that the MOTA technique improves the overall quality of rehydrated wild vegetables. It is expected that our findings could enhance the marketability of dried wild vegetables by improving overall quality and reducing preparation time.

Experimental Study on Oil Separation from Fry-dried Low-rank Coal

  • Ohm, Tea-In;Chae, Jong-Seong;Lim, Jae-Ho;Moon, Seung-Hyun
    • Clean Technology
    • /
    • v.19 no.1
    • /
    • pp.30-37
    • /
    • 2013
  • Low-rank coal with high water content (32.3 wt%) was dried by fry drying, and the fuel characteristics of the dried coal from which the oil was separated by using a high-speed centrifugal separator were analyzed. After fry drying for 6 min and 10 min, the water content decreased to 5.0 wt% and 4.2 wt% respectively. The higher calorific value (HCV) of the coal increased remarkably after fry drying, from 11,442.0 kJ/kg-wet. The oil content of the fry-dried coal was 15.0 wt% and it decreased with an increase in the reheating temperature: 9.7 wt% at $80^{\circ}C$ to 9.3 wt% at $100^{\circ}C$, and then to 8.5 wt% at $120^{\circ}C$. The recovered oil could then be reused. According to of thermogravimetric analysis (TGA), there was no difference in the weight loss patterns of the coal samples with different coal diameters at a reheating temperature of $120^{\circ}C$. This was because the amount of oil separated by the centrifugal separator was affected by the reheating temperature rather than the coal diameter. And derivative thermogravimetry (DTG) curves of raw coal before the fry-drying process, a peak is formed at $400^{\circ}C$ in which the volatile matter is gasified. In case of the fry-dried coal, the first peak is generated at $350^{\circ}C$, and the second peak is generated at $400^{\circ}C$. The first peak is caused by the oil that is replaced with the water contained in the coal during the fry-drying process. Further, the peaks of the coal samples in which the oil is separated at a reheating temperature of $80^{\circ}C$, $100^{\circ}C$, $120^{\circ}C$, respectively are smaller than that of the coal in which the oil is not separated, and this is caused by that the oil is separated by the centrifugal separator.

Development of Oil-Absorbent Using by Curdlan (Curdlan을 이용한 기름 흡착제의 개발에 관한 연구)

  • 이창문;이기영;최춘순;이인영
    • KSBB Journal
    • /
    • v.16 no.2
    • /
    • pp.216-219
    • /
    • 2001
  • Experimental studies were carried out to develop oil-absorbent using curdlan solution or gel. Curdlan sponge was prepared by freeze drying. Surface of curdlan sponge was observed with Scanning electron microscopy(SEM). Curdlan sponge absorbed more than 9 times oil and curdlan was recovered by gellation. Curdlan solution gelled at higher temperature than 50$^{\circ}C$ and dissolved at pH 11.0 and viscosity of curdlan solution increased at 40∼50$^{\circ}C$.

  • PDF

The Effect of Acon on the Serum and Liver of Rats (상수리첨가 식이가 흰쥐의 혈청지질 및 간장에 미치는 영향)

  • Shin, Doo-Ho;Jung, Sueng-Tai
    • Journal of the Korean Applied Science and Technology
    • /
    • v.13 no.2
    • /
    • pp.55-65
    • /
    • 1996
  • The antioxidant effects of freeze-drying acorn were examined to find how much the freeze-drying acorn can reduce peroxidized corn oil poisoning, which influenced cholesterol, triglyceride, phospholipids, lipidperoxides, GOT(glutamate oxaloacetate transaminase), GPT(glutamate pyruvate transaminase) in serum, and cholesterol, triglyceride, lipidperoxides, fatty acid of phospholipids, SOD(superoxide dismutase), catalase in liver. In this experiment, male rats of Sprague-Dawley strain were used. The rats were divided into 6 groups, which were fed differently for 5 weeks : basal diet, 10% peroxidized corn oil added to basal diet, 1% acorn flour and 10% peroxidized corn oil added to basal diet, 5% acorn flour and 10% peroxidized corn oil added to basal diet, 10% acorn flour and 10% peroxidized corn oil added to basal diet, and 0.25% tannic acid and 10% peroxidized corn oil added to basal diet. The results were as follows : It was found that the peroxidized corn oil-fed 5 weeks induced the elevation of cholesterol, triglycerides, lipid peroxides, GOT, GPT in serum, and cholesterol, triglycerides, lipid peroxides in liver as compared to the basal diet-fed rats, but the acorn flour-fed rats reduced the elevation of these components. In addition, saturated fatty acid in rat liver phospholipids induced the elevation by feeding of peroxidized corn oil and, on the other hand, the acorn flour-fed rats reduced the elevation of saturated fatty acids. The acorn flour-fed rats reduced the activity of SOD in liver while they enhanced the activity of catalase in liver as compared with the peroxidized corn oil-fed rats.

Encapsulation of Avocado Oil Using Spray Drying (분무건조를 이용한 아보카도 오일의 캡슐화)

  • Bae, Eun-Kyung;Kim, Gun-Hee
    • Korean Journal of Food Science and Technology
    • /
    • v.40 no.3
    • /
    • pp.303-310
    • /
    • 2008
  • This study was performed to verify the effects of encapsulation against oil oxidation. Thiobarbituric acid (TBA) values of samples were compared during storage at $60^{\circ}C$, indicating that the encapsulated avocado oil had lower TBA values than the free avocado oil. Microcapsules consisting of a whey protein isolate (WPI)-only wall system had slightly improved oxidative stability; however, spray-dried particles containing a high proportion of maltodextrin (MD) clearly offered better protection from oxidation than the other forms of encapsulation. The chlorophyll (Chl) content of the encapsulated avocado oil was higher than that of the free oil sample. When compared to the control, all wall systems protected the change of the chlorophyll content storage. No large differences were observed between the encapsulated powders according to the various wall materials. The color of the encapsulated oil changed from green to yellowish-green, indicating the formation of pheophytin from chlorophyll. The yellowish color of the oil correlated with a reduced total Chl content. In conclusion, encapsulation with spray drying for avocado oil could lead to improved stability during storage with respect to oxidation and the preservation of chlorophyll.