• Title/Summary/Keyword: Oil heat treatment

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Effects on the Joining Condition of TiAl Alloy and SCM440 by Servo Motor Type Friction Welding (서보모터방식 마찰용접을 이용한 TiAl 합금과 SCM440의 접합에 미치는 용접조건의 영향)

  • Park, Jong-Moon;Kim, Ki-Young;Kim, Kyoung-Kyun;Oh, Myung-Hoon
    • Journal of the Korean Society for Heat Treatment
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    • v.29 no.2
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    • pp.66-74
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    • 2016
  • In this study, characteristics of TiAl alloy and SCM440 (Cr-Mo steel) have been investigated with the various joining condition by servo motor type friction welder. The experimental factors of friction welder used in this study are spindle revolution, friction speed, and distance, upset speed and distance, respectively. Servo motor type friction welder could be controlled by the level of oil pressure, and it could be performed by position control dependence of electrical energy. Mechanical properties and morphology of welded interface were characterized by various joining condition. This aroused due to the bond strength dependence on friction heat and size of the heat affected zone. Therefore, it is necessary to have enough friction heat and decreased heat affected zone for good friction welding between dissimilar metals. An optimum bond was obtained between TiAl alloy and SCM440 by controlling friction speed and distance. At the spindle revolution 4,000 rpm, friction speed 120 mm/min, friction distance 15 mm, the bond strength was found to be 312 MPa.

A Study on the RDF making Process of Heat-dried Sludge from Cheonan by using Oil-drying Method (유중건조를 이용한 천안시 열건조물의 고형연료화 공정 연구)

  • Park, So-yeon;Kim, Sang-bin;Ha, Jin-wook
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.2
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    • pp.660-667
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    • 2018
  • This study examined the optimal manufacturing conditions of RDF using heat-dried sludge from sewage treatment plant in Cheonan with the oil-drying method. The amounts of oil evaporation and oil drying of the heat-dried sludge were measured at different temperatures to evaluate the value of the product. The performance of the product was then measured using a calorimeter and TGA. In addition, the concentration of odor, NH3, H2S, and TVOC during drying was determined using a portable odor-meter. Ingredient analysis was performed by EDS. Considering mass-production, the oil to heat-dried sludge weight ratio was fixed to 4:1. At $130^{\circ}C$, only physical mixing occurred after the instantaneous drying of internal water. Considering the eco-friendly aspects, there was no significant difference in the drying efficiency between $160^{\circ}C$ and $190^{\circ}C$. Therefore, the optimal conditions were a drying temperature of $160^{\circ}C$ within 5 minutes. Finally, the RDF manufactured in this study and fuel used in the thermal power plants were compared. The calorific value was 4,449kcal/kg, the water content was 2% and the ash content was 34%, which is higher than the fuel of thermal power plants. Therefore, it is believed that coal energy as well as wood pellets can be replaced.

A Study on Tribological Characteristics of Powder Sintered Fe-base Alloy (SMF9060) (Fe계 합금 분말 소결품(SMF9060)의 마모 특성 연구)

  • Kim, Sang Youn;Kim, Dae Wook;Park, Yeong Min;Shin, Dong Chul;Kim, Tae Gyu
    • Journal of the Korean Society for Heat Treatment
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    • v.27 no.2
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    • pp.65-71
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    • 2014
  • SMF9060 material is a Fe-based powder sintered alloy that is used for several automobile components such as Synchronize Hub, oil pump and transmission. These components are required excellent wear resistance and durability. In this study, we have performed a dry wear test at the ambient air and Ar gas conditions in the room temperature, and a lubricant wear test at the room temperature and engine oil temperature of $100^{\circ}C$. The amount of wear volume and coefficient friction are measured by a Profilometer and a Ball on disk type wear tester. The wear volume in Ar gas condition was a little higher than that in the ambient air condition. However the wear volume in the lubricant wear condition was much lower than in the dry wear condition. XRD analysis of the debris in Ar gas condition showed that the oxide film was not formed.

Elucidation of Intergranular Corrosion of UNS N08810 alloys (UNS N08810 합금의 입계부식손상과 원인 분석)

  • Kim, Youngsik;Hwangbo, Deok
    • Corrosion Science and Technology
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    • v.11 no.5
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    • pp.196-204
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    • 2012
  • Corrosion failure of petrochemical facilities is one of the difficulties in maintenance, since operating conditions of crude oil production, storage, and refinement are very aggressive. UNS N08810, which has been used for crude oil transportation pipes and storage tanks in petrochemical industries, shows good resistance to general corrosion and localized corrosion in several environments. Among its environments, UNS N08810 showed better corrosion resistance in fuel gas containing sulfuric acid and phosphoric acid and sulfur. However, ductility and toughness at high temperature over about $500^{\circ}C$ were greatly reduced due to microstructural change. In general, welding process is the representative method to join the parts in industrial components. Because the alloy by welding can be sensitized and corroded, the manufacturing process should be controlled. In this work, UNS N08810 was used and heat treatment conditions including solution and stabilization treatments were controlled. Oxalic acid etch test by ASTM A262 Practice A was done to evaluate the qualitative sensitization in room temperature. Huey test by ASTM A262 Practice C was done to evaluate the intergranular corrosion rate in boiling 65% $HNO_3$ solution. Also, the microstructure by thermal history was analyzed. Experimental alloy showed high intergranular corrosion rate and its corrosion mechanism was elucidated.

Development of Volatile Organic Compound Pretreatment Device for Removing Exhaust Gas from Display Manufacturing Process (Display 제조공정 배출가스 처리를 위한 휘발성 유기화합물 전처리 장치 개발)

  • Moon, Gi-Hak;Kim, Jae-Yong
    • Applied Chemistry for Engineering
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    • v.30 no.5
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    • pp.523-529
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    • 2019
  • In this study, we investigated the pretreatment technologies of volatile organic compounds (VOCs) which is a problem as the semiconductor and display industry develops recently. The conventional concentrator used in the direct combustion system, is easily contaminated by the exhaust gas in the manufacturing process of the display, resulting in the low treatment efficiency of generated VOCs. Physical/Chemical analyses of the exhaust gas showed high boiling point and viscosity in addition to a large amount of molecular weight alcohols and oil components. In this study, we tried to treat degrading materials by using the heat exchanger in a pretreatment facility and some materials degrading the concentrator were condensed more than 90%. In addition, it was also confirmed that an auxiliary device of the grease filter could remove the redispersion polymer oil from the heat exchanger.

Improvement of protein extraction efficiency from defatted sesame meal with thermal and enzymatic treatments (열 처리와 효소 처리에 의한 탈지 참깨박 단백질의 추출율 향상)

  • In, Man-Jin
    • Journal of Applied Biological Chemistry
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    • v.63 no.4
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    • pp.291-295
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    • 2020
  • In order to increase the utilization of defatted sesame meal (DSM), a by-product of sesame oil production, the conditions of extraction of insoluble proteins from DSM by enzyme treatment were investigated. As a result of comparing the treatment results of proteolytic enzymes Alcalase, Flavorzyme, Neutrase, and Protamex with control, Protamex was effective in increasing the total solid and protein content. At the reaction conditions of Protamex (50 ℃, pH 6.0), the dosage of enzymes was appropriate for 1% of DSM and 3 h of enzyme reaction time. To improve the efficiency of enzymatic treatment, the protein content extracted increased as the heat treatment temperature increased, and slightly increased above 110 ℃. As a result of investigating the effect of the combination treatment of cell lytic enzyme (Tunicase) and protease (Protamex) on protein solubilization, it was most effective to treat the cell lytic enzyme after processing the protease. After heat treatment (110 ℃, 10 min), sequential treatment of Protamex and Tunicase increased the protein content by about 3.5 times (9.85→35.58 mg/mL) of the non-heated control and 2.2 times (15.83→35.58 mg/mL) of the heat treated control.

Heat-Killed and Live Enterococcus faecalis Attenuates Enlarged Prostate in an Animal Model of Benign Prostatic Hyperplasia

  • Choi, Young-Jin;Fan, Meiqi;Tang, Yujiao;Iwasa, Masahiro;Han, Kwon-Il;Lee, Hongchan;Hwang, Ji-Young;Lee, Bokyung;Kim, Eun-Kyung
    • Journal of Microbiology and Biotechnology
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    • v.31 no.8
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    • pp.1134-1143
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    • 2021
  • In the present study, we investigated the inhibitory effect of heat-killed Enterococcus faecalis (E. faecalis) and live E. faecalis on benign prostatic hyperplasia (BPH). The BPH rat model was established by administering male rats with testosterone propionate (TP, 5 mg/kg, in corn oil) via subcutaneous injections daily for four weeks after castration. The rats were divided into five groups: Con, corn oil-injected (s.c.) + DW administration; BPH, TP (5 mg/kg, s.c.) + DW administration; BPH+K_EF, TP (5 mg/kg, s.c.) + heat-killed E. faecalis (7.5 × 1012 CFU/g, 2.21 mg/kg) administration; BPH+L_EF, TP (5 mg/kg, s.c.) + live E. faecalis (1 × 1011 CFU/g, 166 mg/kg) administration; BPH+Fi, TP (5 mg/kg, s.c.) + finasteride (1 mg/kg) administration. In both of BPH+K_EF and BPH+L_EF groups, the prostate weight decreased and histological changes due to TP treatment recovered to the level of the Con group. Both of these groups also showed regulation of androgen-signaling factors, growth factors, and apoptosis-related factors in prostate tissue. E. faecalis exhibited an inhibitory effect on benign prostatic hyperplasia, and even heat-killed E. faecalis showed similar efficacy on the live cells in the BPH rat model. As the first investigation into the effect of heat-killed and live E. faecalis on BPH, our study suggests that heat-killed E. faecalis might be a food additive candidate for use in various foods, regardless of heat processing.

Heat Shock Protein Augmentation of Angelica gigas Nakai Root Hot Water Extract on Adipogenic Differentiation in Murine 3T3-L1 Preadipocytes

  • Lumbera, Wenchie Marie L.;Cruz, Joseph dela;Yang, Seung-Hak;Hwang, Seong Gu
    • Asian-Australasian Journal of Animal Sciences
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    • v.29 no.3
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    • pp.419-427
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    • 2016
  • There is a high association of heat shock on the alteration of energy and lipid metabolism. The alterations associated with thermal stress are composed of gene expression changes and adaptation through biochemical responses. Previous study showed that Angelica gigas Nakai (AGN) root extract promoted adipogenic differentiation in murine 3T3-L1 preadipocytes under the normal temperature condition. However, its effect in heat shocked 3T3-L1 cells has not been established. In this study, we investigated the effect of AGN root hot water extract in the adipogenic differentiation of murine 3T3-L1 preadipocytes following heat shock and its possible mechanism of action. Thermal stress procedure was executed within the same stage of preadipocyte confluence (G0) through incubation at $42^{\circ}C$ for one hour and then allowed to recover at normal incubation temperature of $37^{\circ}C$ for another hour before AGN treatment for both cell viability assay and Oil Red O. Cell viability assay showed that AGN was able to dose dependently (0 to $400{\mu}g/mL$) increase cell proliferation under normal incubation temperature and also was able to prevent cytotoxicity due to heat shock accompanied by cell proliferation. Confluent preadipocytes were subjected into heat shock procedure, recovery and then AGN treatment prior to stimulation with the differentiation solution. Heat shocked preadipocytes exhibited reduced differentiation as supported by decreased amount of lipid accumulation in Oil Red O staining and triglyceride measurement. However, those heat shocked preadipocytes that then were given AGN extract showed a dose dependent increase in lipid accumulation as shown by both evaluation procedures. In line with these results, real-time polymerase chain reaction (RT-PCR) and Western blot analysis showed that AGN increased adipogenic differentiation by upregulating heat shock protection related genes and proteins together with the adipogenic markers. These findings imply the potential of AGN in heat shock amelioration among 3T3-L1 preadipocytes through heat shock factor and proteins augmentation and enhanced adipogenic marker expression.

Effect of Quenching Heat-treatment on Mechanical Properties and Microstructure of Modified C95600 Bronze (개량형 C95600 청동의 기계적 성질과 미세조직에 미치는 퀜칭 열처리의 영향)

  • Lee, Sung-Yul;Moon, Kyung-Man;Oh, Jae-Hwan;Shin, Dong-Il
    • Journal of Ocean Engineering and Technology
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    • v.25 no.6
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    • pp.97-104
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    • 2011
  • Modified C95600 bronze contains Fe component of 0.7 weight percentage besides Cu-7Al-2.5Si composition. The shape of centrifugal cast is a circular pipe with thick wall. Specimens machined from the centrifugal cast were quenched in oil after isothermal holding at a given heat treatment temperature in the range of $700{\sim}900^{\circ}C$. Mechanical properties and structural morphology are depended on the quenching heat treatment temperature regardless of isothermal holding time. Tensile strength or Brinell hardness is increased with increasing heat treatment temperature. The microstructure caused by quenching contains mixing phases of ${\alpha}+{\beta}'+FeSi+{\kappa}$ which martensite of ${\beta}'$ phase has been transformed from ${\beta}$ phase. Effect of isothermal holding temperature on mechanical properties in case of quenching heat treatment attributes to the change of volume fraction of ${\beta}'$ on the structural morphology. Mechanical characteristics of specimen, initially quenched from $850^{\circ}C$, and then tempered at $500^{\circ}C$, does not show an obvious softening indication, because disappearance of ${\beta}'$ during tempering process can be compensated by precipitation of brittle phase ${\gamma}$.

Enhancement in the Thermal Stability of Microporous UHMWPE Membrane by LED-UV Crosslinking (LED-UV 가교에 의한 UHMWPE 미세다공막의 열 안정성 향상)

  • Jeong-Hwan Kim;Jinho Jang
    • Textile Coloration and Finishing
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    • v.35 no.4
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    • pp.231-238
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    • 2023
  • Microporous gel films of 29 m were prepared by the gel drawing of UHMWPE/soybean oil blend (4:6, w/w) up to 800%. The stretched films containing the optimal photoinitiator concentration, depending on the film thickness, was cross-linked under 365 nm LED-UV irradiation and the oil was extracted with n-hexane, resulting in a gel fraction of 95 % or more. With the formation of the cross-linked structure, the melt-down temperature and melt-down elongation increased by 16 ℃ and by 63% respectively. Also the thermal stability of the crosslinked UHMWPE was proved by the area shrinkage under the heat treatment decreased to 3.8 % compared to 17.4 % for the pristine film, and by the reductions in the combustion heat. The enhanced thermal stability of the crosslinked UHMWPE microporous membranes can be used for various industrial applications such as filters, electric vehicles and energy storage systems.