• Title/Summary/Keyword: O-plasma treatment

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Adhesive strength of PDMS/Substrate by Plasma Treatment (플라즈마 처리에 의한 PDMS/기판에서의 접착력 측정)

  • Gwon, O-Chang;Han, Jun-Hyeon;Mun, Myeong-Un;Yun, Ju-Il
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2015.11a
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    • pp.169-169
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    • 2015
  • Poly(dimethysiloxane, PDMS)은 그 다양한 사용분야 때문에 지속적으로 연구분야에서 연구주제가 되고 있었다. 본 논문에서는 산소 플라즈마 처리에 의한 PDMS/기판에서의 접착강도를 peel 테스트를 통하여 정량적으로 측정하였다.

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Attenuating Effects of N-acetylcysteine (NAC) against Fish Parasiticide-induced Toxicity in Carp Cyprinus carpio (잉어(Cyprinus carpio)에서 어류 구충제에 대한 N-acetylcysteine(NAC)의 독성 저감 효과)

  • Park, Kwan-Ha
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.44 no.5
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    • pp.484-489
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    • 2011
  • This study examined whether N-acetylcysteine (NAC), a glutathione precursor, could attenuate toxic effects of three fish anti-parasitic agents, trichlorfon, hydrogen peroxide ($H_2O_2$) and formalin, all of which are known to exert side effects through free radical production. Common carp Cyprinus carpio were fed with NAC (approx. 50 mg/kg/day) for 3 consecutive days prior to anti-parasite bathing for a 24 hr period. Mortality rates were examined during this 24 hr bathing period, and selected hematological and biochemical parameters were also assessed at the termination of anti-parasite exposure. The mortality rates and plasma glucose elevations caused by all three anti-parasitics were significantly reduced by NAC pretreatment. Trichlorfon, but not $H_2O_2$ or formalin, elevated plasma levels of aspartatetransaminase (AST) and alanine-transaminase (ALT), and these elevations were attenuated by NAC. There was no change in hematocrit values in any treatment. The results provide evidence for the attenuating effects of NAC against toxicity caused by anti-parasite agents that act through free radical-producing properties. The results found in this study also suggest that NAC may be administered to fish to minimize toxicity in fish parasiticide use.

Temperature Dependence of Resistivity in As Implanted LPCVD Polycrystalline Silicon Films (LPCVD로 제조된 다결정실리콘에 As를 주입한 시료의 비저항에 대한 온도의존성 연구)

  • Ha, Hyoung-Chan;Kim, Chung-Tae;Ko, Chul-Gi;Chun, Hui-Gon;Oh, Kye-Hwan
    • Korean Journal of Materials Research
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    • v.1 no.1
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    • pp.23-28
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    • 1991
  • The resistivity of polycrystalline silicon film deposited by low pressure chemical vapor deposition and doped by arsenic Implantation has been investigated as a function of dopant concentration and testing temperature ranging from $25^{\circ}C$ to $105^{\circ}C$ . The resistivity vs. doping concentration curve had a peak point with highest activation energy with respect to the dependence of the resistivity on temperature. We showed that $O_2$ plasma anneal followed by heat-treatment in $N_2$ ambient was able to recover the resistivity degraded by the plasma deposited passivation layers.

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Heat Treatment Effects on the Phase Evolutions of Partially Stabilized Grade Zirconia Plasma Sprayed Coatings

  • Park, Han-Shin;Kim, Hyung-Jun;Lee, Chang-Hee
    • Journal of the Korean institute of surface engineering
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    • v.34 no.5
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    • pp.486-493
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    • 2001
  • Partially stabilized zirconia (PSZ) is an attractive material for thermal barrier coating. Zirconia exists in three crystallographic phases: cubic, tetragonal and monoclinic. Especially, the phase transformation of tetragonal phase to monoclinic phase accompanies significant volume expansion, so this transition generally results in cracking and contributes to the failure of the TBC system. Both the plasma sprayed ZrO$_2$-8Y$_2$O$_3$ (YSZ) coat and the ZrO$_2$,-25CeO$_2$,-2.5Y$_2$O$_3$ (CYSZ) coat are isothermally heat -treated at 130$0^{\circ}C$ and 150$0^{\circ}C$ for 100hr and cooled at different cooling rates. The monoclinic phase is not discovered in all the CYSZ annealed at 130$0^{\circ}C$ and 150$0^{\circ}C$. In the 150$0^{\circ}C$ heat-treated specimens, the YSZ contains some monoclinic phase while none exists in the 130$0^{\circ}C$ heat-treated YSZ coat. For the YSZ, the different phase transformation behaviors at the two temperatures are due to the stabilizer concentration of high temperature phases and grain growth. For the YSZ with 150$0^{\circ}C$-100hr annealing, the amount of monoclinic phase increased with the slower cooling rate. The extra oxygen vacancy, thermal stress, and c to t'phase transformation might suppress the t to m martensitic phase transformation.

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Wear characteristics of plasma sprayed yttria-stabilized zirconia coating as phase transformation (지르코니아 용사코팅의 상변화에 따른 마멸특성)

  • Park, Chan;Chae, Young-Hun;Kim, Seock-Sam
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.11a
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    • pp.322-330
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    • 2001
  • The plasma-sprayed 8%Y$_2$O$_3$-Zirconia coating was studied to know the relationship between phase transformation and wear properties after several heat treatment. Wear tests were carried out with ball on disk on 50N, 70N, 90N. The specimen in this study was cast iron and tests were performed on room temperature. The transformation of phase and residual stress was measured by x-ray diffraction method(XRD) and worn surface were observed by SEM.

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Characterion of Calcium Phosphate Films Grown on Surgicl Ti-6AI-4V By Ion Beam Assisted Deposition

  • Lee, I-S.;Song, J-S.;Choi, J-M;Kim, H-E.
    • Journal of the Korean Vacuum Society
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    • v.7 no.s1
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    • pp.30-36
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    • 1998
  • The plasma-spray technique is currently the most frequently used method to produce calcium phosphate coatings. Hydroxyapatite(HAp), one form of calcium phosphate, is preferred by its ability to form a direct bond with living bone, resulting in improvements of implant fixation and faster bone healing. Recently, concerns have been raised regarding the viable use and long-term stability of plasma-spray HAp coatings due to its nature of comparatively thick, porous, and poor bonding strength to metal implants. Thin layers (maximum of few microns) of calcium phosphate were formed by an e-beam evaporation with and without ion bombardments. The Ca/P ration of film was controlled by either using the evaporants having the different ration of Ca/P with addition of CaO, or adjusting the ion beam assist current. The Ca/P ration had great effects on the structure formation after heat treatment and the dissolution bahavior. The calcium phosphate films produced by IBAD exhibited high adhesion strength.

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In-situ Synthesis of Cu-TiB2 Nanocomposite by MA/SPS

  • Kwon, Young-Soon;Kim, Ji-Soon;Kim, Hwan-Tae;Moon, Jin-Soo;D.V Dudina;O.I. Lomovsky
    • Journal of Powder Materials
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    • v.10 no.6
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    • pp.443-447
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    • 2003
  • Nano-sized $TiB_2$ was in situ synthesized in copper matrix through self-propagating high temperature synthesis (SHS) with high-energy ball milled Ti-B-Cu elemental mixtures as powder precursors. The size of $TiB_2$ particles in the product of SHS reaction decreases with time of preliminary mechanical treatment ranging from 1 in untreated mixture to 0.1 in mixtures milled for 3 min. Subsequent mechanical treatment of the product of SHS reaction allowed the $TiB_2$ particles to be reduced down to 30-50 nm. Microstructural change of $TiB_2$-Cu nanocomposite during spark plasma sintering (SPS) was also investigated. Under simultaneous action of pressure, temperature and electric current, titanium diboride nanoparticles distributed in copper matrix move, agglomerate and form a interpenetrating phase composite with a fine-grained skeleton.

A study for properties of AZO thin film prepared to Ar-plasma treatment using ICP-CVD (ICP-CVD에 의해 Ar 플라즈마 처리된 AZO 박막의 표면 거칠기에 관한 연구)

  • Bang, Tae-Bok;Ryu, Sung-Won;Kim, Deok-Su;Cho, Do-Hyun;Rhee, Byung-Roh;Kim, Jong-Jae;Park, Seoung-Hwan;Hong, Woo-Phyo;Kim, Hwa-Min
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.386-387
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    • 2007
  • ICP-CVD(Inductively Coupled Plasma-Chemical Vapor Deposition)를 이용하여 플라즈마 처리에 따른 Al이 도핑된 ZnO(AZO) 박막의 표면 부착력과 굴절율, 표면거칠기에 관한 연구를 하였다. 플라즈마 처리는 인가전압, 시간을 변수로 하였고 반응 가스는 Ar을 사용하였다. 표면조성은 AFM, 광학적 특성은 UV-Vis 분광계를 이용한 광투과도 측정으로부터 굴절률과 밴드갭을 조사하였고 표면 부착력은 접촉각 분석기(제조사:Kruss)를 사용하여 조사하였다. 플라즈마 처리 시간이 길어짐에 따라 박막 표면의 거칠기가 커지고 부착력은 증가하는 것으로 나타났다.

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