• 대한토목학회논문집
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• 제28권4A호
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• pp.529-536
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• 2008

구조물의 파괴 거동은 하중의 재하 속도에 따라 달라지는 특성을 보이는데, 이는 재료의 속도 의존성으로부터 비롯된다고 할 수 있다. 이러한 현상은 공학의 여러 분야에서 관심사였지만, 파괴 메커니즘이 명확히 규명되지 않았기 때문에 수치 해석을 통한 연구에는 그 한계점과 어려움이 상존하였다. 본 연구에서는 파괴 거동의 속도 의존성을 이해하고자, 취성재료를 대상으로 입자동역학을 이용한 수치해석을 수행하였다. 직접 인장 시험 시뮬레이션을 위해 노치가 있는 시편을 모델링하고, 취성재료가 갖는 특성을 표현하기 위해 Lennard-Jones 포텐셜을 사용하였다. 6가지의 다른 하중 속도에 따른 균열의 거칠기, 균열의 후퇴와 멈춤, 분기 현상과 같은 동적 파괴 특성을 관찰하였다. 해석 결과를 통해 하중 속도에 따른 파괴 거동의 변화 원인을 에너지 유입-소모율의 개념을 도입하여 설명하고, 재료의 파괴 메커니즘이 갖는 속도 의존성에 대해 이해할 수 있는 단초를 마련하였다. 또한, 기존 실험과의 비교를 통해 실제적인 현상과의 유사성을 밝힘으로써 입자동역학의 공학적 적용 가능성을 제시하였다.

• 콘크리트학회논문집
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• 제14권3호
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• pp.357-364
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• 2002

CLWL-DCB 시험편에 대한 변위제어 파괴실험으로 381mm의 균열성장에 대한 저항곡선이 유도되었다. 변형률 게이지를 사용하여 측정된 평균 균열성장속도는 0.70 mm/sec와 55mm/sec이었다. 초기균열에서 측정된 회전각도는 0.70 mm/sec와 55mm/sec의 균열속도에 대해 각각 최소한 171mm와 93mm의 균열성장 이전에 특이성이 존재하는 것을 보여주었다. 저항곡선의 최대 기울기는 0.70mm/sec 균열속도에 대해 25.4mm와 88.9mm 그리고 55mm/sec 균열속도에 대해 50.8 mm와 127mm의 균열성장길이 사이에서 발생되며, 미소균열 국부화에 의한 것으로 판단된다. 빠른 균열속도에서 미소균열성장 구역은 보다 길게 형성되며, 미소균열의 국부화 동안에도 큰 균열성장을 보였다. 0.70mm/sec 균열속도의 파괴저항은 152.4mm의 균열성장 이후에 평균 파괴에너지율의 약 70%인 143N/m의 비교적 일정한 값을 유지하였다. 55mm/sec 균열속도는 254mm 균열성장에서 최대 파괴저항 245N/m까지 증가한 후 파괴저항의 감소되어 불안정 균열성장이 발생될 수 있음을 보여준다. 55mm/sec 균열속도의 저항곡선은 TPB 실험과 유사하여, 시험편의 크기가 작거나 균열의 속도가 빠른 경우에 취성거동을 할 수 있는 것을 보여준다.

• 터널과지하공간
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• 제26권5호
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• pp.396-408
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• 2016

암석파괴역학은 토목공학과 암반공학의 다양한 분야에서 널리 적용되는 학문이다. 그러나 대부분의 암반 공학 문제에서 mode II 거동이 우세함에도 불구하고 관련 연구는 mode I 거동에 대한 것이 대부분이다. 현재 mode I의 경우 4개, mode II 파괴인성의 경우 단 한 개의 ISRM 표준시험법이 있다. 본 연구에서 제안하는 새로운 시험법은 문헌조사를 통해서 필요조건으로 구속압 가능 여부, 노치성형의 용이성, 기존 시험장비의 활용, 단순한 시험절차를 정하고 이에 부합하도록 개발하였으며 SCC(Short Core in Compression)로 이름을 정하였다. Mode II 파괴인성 계산에 필요한 응력확대계수 계산식을 3차원 수치해석을 통해 선하중과 분포하중 조건에 대해서 구하였고 노치성형을 위한 지그도 제작하였다. 개발된 시험법을 MTS 시스템을 사용하여 화강암에 적용하였으며 가압속도는 0.002 mm/s로 하였다. 시험 결과 $2.33MPa{\sqrt{m}}$의 mode II 파괴인성을 얻었다. 동일한 화강암 블록에서 확보한 시험편에 대하여 간접인장시험으로 구한 mode I 파괴인성은 $1.12MPa{\sqrt{m}}$였다. 따라서 $K_{IIC}/K_{IC}=2.08$로 mode II 파괴인성이 mode I보다 크게 나타났다. 또한 비교적 매끄러운 파괴면과 암분의 생성을 통하여 SCC 시험법이 mode II 거동을 잘 표현함을 확인하였다. 따라서 제안된 SCC 시험법은 암석의 mode II 파괴인성을 결정하는 데 사용할 수 있을 것으로 판단된다.

• 대한기계학회논문집A
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• 제39권4호
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• pp.405-413
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• 2015

최근 미국에서는 가동기간이 오래된 원전 매설배관에서 부식 및 침식에 의해 삼중수소 누설로 지하수가 오염되는 사례가 급증하고 있다. 따라서, 현재 원전 안전등급 매설배관으로 사용되고 있는 금속재료의 배관을 대신해서 부식 및 침식 등의 열화 손상에 대한 저항성이 우수한 고밀도 폴리에틸렌(HDPE) 배관을 ASME Code Class 3 안전계통 배관으로 사용하기 위한 연구가 수행되고 있다. 본 연구에서는 발전소 가동 중 매설배관에 가해질 수 있는 하중과 온도 범위를 바탕으로 HDPE 배관 융착부에 대한 인장 시험과 저속균열성장 (SCG) 시험을 수행하였다. 시험 결과로 얻은 SCG 시험편의 파단면을 분석하여 HDPE 재료의 파손 기구를 파악하였다. 이를 바탕으로 3D 유한요소 해석을 이용하여 균열이 있는 HDPE 재료가 버틸 수 있는 한계하중에 대한 검증을 수행하였다.

• 대한치과보철학회지
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• 제43권1호
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• pp.52-60
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• 2005

Purpose. The intent of this study was to evaluate the effects of curing conditions on self-curing denture base resins to find out proper condition in self-curing resin polymerization. Materials and methods, In this study, 3 commercial self-curing denture base resins are used Vertex SC, Tokuso Rebase and Jet Denture Repair Acrylic. After mixing the self curing resin, it was placed in a stainless steel mold(3$\times$6$\times$60mm). The mold containing the resin was placed under the following conditions: in air at 23$^{\circ}C$; or in water at 23$^{\circ}C$; or in water at 23$^{\circ}C$ under pressure(20psi); or in water at 37$^{\circ}C$ under pressure(20psi) or in water at 50$^{\circ}C$ under pressure(20psi) , or in water at 65$^{\circ}C$ under pressure(20psi), respectively. Also heat-curing denture base resin is polymerized according to manufactures' instructions as control. Fracture toughness was measured by a single edge notched beam(SENB) method. Notch about 3mm deep was carved at the center of the long axis of the specimen using a dental diamond disk driven by a dental micro engine. The flexural test was carried out at a crosshead speed 0.5mm/min and fracture surface were observed under measuring microscope. Results and conclusion . The results obtained were summarized as follows : 1. The fracture toughness value of self-curing denture base resins were relatively lower than that of heat-curing denture base resin. 2. In Vertex SC and Jet Denture Repair Acrylic, higher fracture toughness value was observed in the curing environment with pressure but in Tokuso Rebase, low fracture toughness value was observed but there was no statistical difference. 3. Higher fracture toughness value was observed in the curing environment with water than air but there was no statistical difference. 4. Raising the temperature in water showed the increase of fracture toughness.

• Restorative Dentistry and Endodontics
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• 제18권1호
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• pp.1-26
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• 1993

The purpose of this study was to investigate the effect of acid etching on the surface appearance and fracture toughness of five glass ionomer cements. Five kinds of commercially available glass ionomer cements including chemical curing filling type, chemical curing lining type, chemical curing metal reinforced type, light curing tilling type and light curing lining type were used for this study. The specimens for SEM study were fabricated by treating each glass ionomer cement with either visible light curing or self curing after being inserted into a rubber mold (diameter 4mm, depth 1mm). Some of the specimens were etched with 37% phosphoric acid for 0, 15, 30, 60, go seconds, at 5 minutes, 1 hour and 1 day after mixing of powder and liquid. Unetched ones comprised the control group and the others were the experimental groups. The surface texture was examined by using scanning electron microscope at 20 kV. (S-2300, Hitachi Co., Japan). The specimens for fracture toughness were fabricated by curing of each glass ionomer cement previously inserted into a metal mold for the single edge notch specimen according to the ASTME399. They were subjected to a three-point bend test after etching for 0, 30, 60, and 90 seconds at 5 minutes-, 1 hour-and 1 day-lapse after the fabrication of the specimens. The plane strain fracture toughness ($K_{IC}$) was determined by three-point bend test which was conducted with cross-head speed of 0.5 mm/min using Instron universal testing machine (Model No. 1122) following seven days storage of the etched specimens under $37^{\circ}C$, 100% humidity condition. Following conclusions were drawn. 1. In unetched control group, crack was present, but the surface was generally smooth. 2. Deterioration of the surface appearance such as serious dissolving of gel matrix and loss of glass particles occured as the etching time was increased beyond 15 s following Immediate etching of chemical curing type of glass ionomer cements. 3. Etching after 1 h, and 1 d reduced surface damage, 15 s, and 30s etch gave rough surface appearance without loss of glass particle of chemical curing type of glass ionomer cements. 4. Light curing type glass ionomer cement was etched by acid, but there was no difference in surface appearances according to various waiting periods. 5. It was found that the value of plane stram fracture toughness of glass ionomer cements was highest in the light curing filling type as $1.79\;MNm^{-1.5}$ followed by the light curing lining type, chemical curing metal reinforced type, chemical curing filling type and chemical curing lining type. 6. The value of plane stram fracture toughness of the chemical curing lining type glass ionomer cement etched after 5 minutes was lower than those of the cement etched after 1 hour or day or unetched (P < 0.05). 7. Light curing glass ionomer cement showed Irregular fractured surface and chemical curing cement showed smooth fractured surface.

• Restorative Dentistry and Endodontics
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• 제25권2호
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• pp.243-253
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• 2000

The purpose of this in vitro study was to evaluate dentin bonding by two different dentin bonding systems(DBS) using acetone based primer or adhesive [All Bond 2(AB2), One Step(OS)] when they were applied by wet or dry bonding technique. Morphology of resin-dentin interface and hybrid layer thickness(HLT) were investigated using Confocal Laser Scanning Microscope(CLSM) and compared to shear bond strength(SBS). 72 extracted sound human molars were randomly divided into 4 groups of 18 teeth each - Group 1.(AW); AB2 by wet bonding. Group 2(AD); AB2 by dry bonding. Group 3.(OW); OS by wet bonding, Group 4.(OD); OS by dry bonding. In 6 teeth of each group, notch-shaped class V cavities(depth 2mm) were prepared on buccal and lingual surface at the cementoenamel juction(12 cavities per group). To obtain color contrast in CLSM observation, bonding resins of each DBS were mixed with rhodamine B and primer of AB2 was mixed with sodium fluorescein. Prepared teeth of each group were treated with AB2, OS, respectively according to the manufacturer's instructions except for dentin surface moisture treatment after acid etching. In group 1 and 3, after acid etching, excess water was removed with wet tissue(Kimwipes), leaving consistently shiny, visibly hydrated dentin surface. In group 2 and 4, dentin surface was dried for 10 seconds at 1 inch distance. The treated teeth were then packed with composite resin(${\AE}$litefil) and light-cured. 12 microscopic samples($60{\sim}80{\mu}m$ thickness) of each group were obtained after longitudinal section and grinding(Exakt cutting and grinding system). Morphological investigation of resin-dentin interface and HLT measurement using CLSM were done. For measurement of SBS, remaining 12 teeth of each group were flattened occlusally to remove all enamel and grinded to 500 grit SiC(Pedemet Specimen Preparation Equipment). After applying DBS on the exposed dentin surface, composite resin was applied in the shape of cylinder, which has 5mm diameter, 1.5mm thickness, and light cured. SBS was measured using Instron with a crosshead speed of 0.5mm/min. It was concluded as follows, 1. HLT of AW(mean: $2.59{\mu}m$) was thicker than any other group, and followed by AD, OW, OD in descending order(mean; 2.37, 2.28, $1.92{\mu}m$). Only OD had statistically significant differences(p<0.05) to AW and AD. 2. There were intimate contact of resin and dentin at the interface in wet bonding groups, but gaps or irregular interfaces were observed in dry bonding groups. 3. The length, diameter, density of resin tags were various even in the same group without significant differences between groups and lots of adhesive lateral branches were observed. 4. There were no statistically significant difference of SBS between AB2 and OS, but SBS of wet bonding groups were significantly higher(p<0.05) than dry bonding groups. 5. There were no consistent relationships between HLT and SBS.

• 한국구조물진단유지관리공학회 논문집
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• 제10권3호
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• pp.185-196
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• 2006

파괴인성은 균열의 개시와 전파에 대한 재료 고유의 상수로서 파괴역학에서 가장 중요한 재료상수 중의 하나이다. 콘크리트의 모드 I 파괴인성 측정에 대하여 RILEM 기술 위원회 89-FMT는 2-파라메타 모델에 근거한 3점 휨 시험법을 제시하였다. 그러나 혼합모드에 대한 시험법은 아직까지 표준으로 제안된 방법이 없는 실정이며, 또한 RILEM에서 제안한 3점 휨 시험법은 실험법이 복잡하다. 따라서 본 연구에서는 굵은골재의 최대치수가 각각 20mm, 40mm이고, 동일한 설계기준강도를 가지는 콘크리트로써 다양한 크기의 브라질리언 디스크를 제작하였다. 그리고 브라질리언 디스크의 모드 I 파괴인성을 RILEM 3점 휨 시험결과와 비교하였다. 비교 결과, 굵은골재의 최대치수에 따른 브라질리언 디스크의 적정 크기(두께, 직경) 및 노치 길이 비를 제시하였다. 또한 모드 I 시험으로부터 결정된 치수의 브라질리언 디스크로 혼합모드 시험을 수행한 결과 디스크 시편은 혼합모드 파괴의 연구 및 시험에 유용함을 알 수 있었다. 모드 I 및 혼합모드 시험에서 브라질리언 디스크의 응력확대계수는 유한요소해석(FEA)으로 구하였으며 FEA의 결과를 검증하기 위하여 5개항 근사법(Five terms approximation)에 의한 결과와 비교하였다.

• Restorative Dentistry and Endodontics
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• 제26권4호
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• pp.332-340
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• 2001

Flowable composite resin has lower filler content, increased flow, and lower modules of elasticity. It is suggested that flowable composite resin can be bonded to the tooth structure intimately and absorb or dissipate the stress. Therefore, it may be advantageous to use flowable composite resin for the base material of class II restoration and for the class V restoraton. The purpose of this study was to evaluate the microleakage and shear bond strength of four flowable composite resins (Aeliteflo, Flow-It, Revolution, Ultraseal XT Plus) compared to Z100 using Scotchbond Multi Purpose dentin bonding system. To evaluate the microleakage, notch-shaped class V cavities were prepared on buccal and lingual surfaces of 80 extracted human premolars and molars on cementum margin. The teeth were randomly divided into non-thermocycling group (group 1) and thermocycling group (group 2) of 40 teeth each. The experimental teeth of each group were randomly divided onto five subgroups of eight samples (sixteen surfaces). The Scotchbond Multi-Purpose and composite resin were applied for each group following the manufacturer's instructions. the teeth of group 2 were thermocycled five hundred times between 5$^{\circ}C$ and 55$^{\circ}C$. The teeth of group 2 were placed in 2% methylene blue dye for 24 hours, then rinsed with tab water. The specimens were embedded in clear resin, and sectioned longitudinally with a diamond saw. The dye penetration on each of the specimen were observed with a stereomicioscope at $\times$20 magnification. To evaluate the shear bond strength, 60 teeth were divided into five groups of twelve teeth each. The experimental teeth were ground horizontally below the dentinoenamel junction, so that no enamel remained. After applying Scotchbond Multi-Purpose on the dentin surface, composite resin was applied in the shape of cylinder. The cylinder was 4mm in diameter and 2mm in thickness. Shear bond strength was measured using Instron with a cross-head speed of 0.5mm/min. After shear bond strength measurement, mode of failure was evaluated with a stereomicroscope at $\times$30 magnification. All data were statistically analyzed by One Way ANOVA and Student-Newman-Keuls method. The correlation between microleakage and shear bond strength was analyzed by linear regression. The results of this study were as follows ; 1. In non-thermocycling group, the leakage value of Z100 was significantly lower than those of flowable composite resins at the enamel and dentin margin, margin, except that Revolution showed the lower leakage value than that of Z100 at the dentin margin (p<0.05). 2. In thermocycling group, the leakage values of Z100 and Ultraseal XT Plus were lower than those of other subgroup at the enamel and dentin margin, except that Flow-It showed the lower leakage value than that of Ultraseal XT Plus at the dentin margin (p<0.05). 3. The leakage value of Z100 and Ultraseal XT Plus in thermocycling group were not higher than that in non-thermocycling group at the enamel margin. The leakage value of Z100 in thermocycling group was not higher than that in non-thermocycling group at the dentin margin (p<0.05). 4. As for the shear bond strength measurement, there were no statistically significant differences among groups (p<0.05). The shear bond strengths given in descending order were as follows: Z100(16.81$\pm$2.98 MPa), Flow-It(14.8$\pm$4.43 MPa), Aeliteflo(14.34$\pm$3.69 MPa), Revolution(13.46$\pm$4.23 MPa), Ultraseal XT Plus(12.83$\pm$3.16 MPa). 5. Failure modes of all specimens were adhesive failures. 6. There was no correlation between microleakage and shear bond strength.