• Bulletin of the Korean Chemical Society
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• 제35권7호
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• pp.2049-2056
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• 2014

A simple method for exfoliating pristine graphite to yield mono-, bi-, and multi-layers of graphene sheets as a highly concentrated (5.25 mg/mL) and yielded solution in an organic solvent was developed. Pre-thermal treatment of pristine graphite at $900^{\circ}C$ in a sealed stainless steel bath under high pressures, followed by sonication in 1-methyl-2-pyrrolidinone solvent at elevated temperatures, produced a homogeneous, well-dispersed, and non-oxidized graphene solution with a low defect density. The electrical conductivities of the graphene sheets were very high, up to 848 S/cm. These graphene sheets were used to fabricate graphene-polyimide nanocomposites, which displayed a higher electrical conductivity (1.37 S/m) with an improved tensile strength (95 MPa). The synthesized graphene sheets and nanocomposites were characterized by transmission electron microscopy, scanning electron microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, and Raman spectroscopy.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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• pp.91-91
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• 2008

$SnO_2-B_2O_3-P_2O_5$ system were prepared by melt-quenching technique in the compositional series containing 50, 55 aod 60mol.% of $SnO_2$. A large glass-forming region was found at the phosphate side of the ternary system with homogeneous glasses containing up to 5-25mol.% of $B_2O_3$. For these glasses, thermal expansion coeffient($\alpha$), glass transition temperature(Tg), and glass softening temperature(Ts), were determined. The values a decrease with increasing $B_2O_3$ content, while Tg and Ts increased. The reason for the observed changes is local structure of the glasses. Local structure of the glasses was investigated by Raman and FT-IR measurements, suggesting that the number of bridging oxygens decreased whereas the non-bridging oxygen concentration increased with increasing $SnO_2$ content in the glasses.

• Structural Engineering and Mechanics
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• 제62권4호
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• pp.401-415
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• 2017

A new higher shear deformation theory (HSDT) is presented for the thermal buckling behavior of functionally graded (FG) sandwich plates. It uses only four unknowns, which is even less than the first shear deformation theory (FSDT) and the conventional HSDTs. The theory considers a hyperbolic variation of transverse shear stress, respects the traction free boundary conditions and contrary to the conventional HSDTs, the present one presents a new displacement field which includes undetermined integral terms. Material characteristics and thermal expansion coefficient of the sandwich plate faces are considered to be graded in the thickness direction according to a simple power-law distribution in terms of the volume fractions of the constituents. The core layer is still homogeneous and made of an isotropic material. The thermal loads are supposed as uniform, linear and non-linear temperature rises within the thickness direction. An energy based variational principle is used to derive the governing equations as an eigenvalue problem. The validation of the present work is carried out with the available results in the literature. Numerical results are presented to demonstrate the influences of variations of volume fraction index, length-thickness ratio, loading type and functionally graded layers thickness on nondimensional thermal buckling loads.

• Structural Engineering and Mechanics
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• 제47권4호
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• pp.559-573
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• 2013

Geometrically non-linear axisymmetric bending of a shallow spherical shell with a clamped or a simply supported edge under axisymmetric load was investigated numerically. The partial load was introduced by the Heaviside step function, and the solution was obtained by the finite difference and the Newton-Raphson methods. The thickness of the shell was considered to be uniform and the material was assumed to be homogeneous and isotropic. Sensitivity analysis was made for three geometrical parameters. The accuracy of the algorithm was checked by comparing the central deflection, the radial membrane stress at the edge, or the transverse shear force with the solutions of plates and shells in the literature and good agreement was obtained. The main findings of the study can be outlined as follows: (i) If the shell is fully loaded the central deflection of a clamped shell is larger than that of a simply supported shell provided that the shell is not very shallow, (ii) if the shell is partially loaded the central deflection of the shell is sensitive to the parameters of thickness, depth, and partial loading but the influence of the boundary conditions is negligible.

• Steel and Composite Structures
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• 제28권3호
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• pp.349-362
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• 2018

This paper presents a semi-analytical solution for the creep analysis and life assessment of 304L austenitic stainless steel thick truncated conical shells using multilayered method based on the first order shear deformation theory (FSDT). The cone is subjected to the non-uniform internal pressure and temperature gradient. Damages are obtained in thick truncated conical shell using Robinson's linear life fraction damage rule, and time to rupture and remaining life assessment is determined by Larson-Miller Parameter (LMP). The creep response of the material is described by Norton's law. In the multilayer method, the truncated cone is divided into n homogeneous disks, and n sets of differential equations with constant coefficients. This set of equations is solved analytically by applying boundary and continuity conditions between the layers. The results obtained analytically have been compared with the numerical results of the finite element method. The results show that the multilayered method based on FSDT has an acceptable amount of accuracy when one wants to obtain radial displacement, radial, circumferential and shear stresses. It is shown that non-uniform pressure has significant influences on the creep damages and remaining life of the truncated cone.

• 대한토목학회논문집
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• 제32권6A호
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• pp.399-409
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• 2012

비세장 복부판을 갖고 균일모멘트를 받는 HSB 강재가 적용된 플레이트거더의 비탄성 횡비틀림좌굴 영역 휨강도 특성을 비선형 유한요소해석으로 분석하였다. HSB600 및 HSB800 강재로 제작된 균질단면 강거더와 HSB800 강재와 SM570-TMC 강재를 함께 적용한 하이브리드단면 거더를 고려하였으며, 일반강재와의 상대 비교를 위하여 SM490-TMC 강거더에 대한 해석도 수행하였다. 해석대상 비합성 I-거더 단면의 플랜지와 복부판을 쉘요소로 모델링하고 ABAQUS 프로그램을 이용하여 재료 및 기하학적 비선형 유한요소해석을 수행하였다. 강재는 탄소성-변형경화 재료로 모델링하였고 초기변형과 단면의 잔류응력을 고려하였으며, 이들이 비탄성 횡비틀림좌굴 영역에서 휨거동에 미치는 영향을 분석하였다. HSB 고강도강을 적용한 플레이트거더의 FE 해석과 한계상태법 도로교설계기준, AASHTO LRFD, Eurocode 등 국내외 주요 설계기준에 의한 공칭휨강도와 비교하고 이들 설계기준을 평가하였다.

• 터널과지하공간
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• 제11권4호
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• pp.362-367
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• 2001

지반에서 겨울에 발생할 수 있는 단단한 상부층은 방진벽의 진동차단성능을 변화시킬 수 있다. 본 논문은 상부에 단단한 층이 존재하는 층진 지반(layered soil)에서 표면파의 진동전파와 강성 방진벽의 진동차단 성능에 관한 것이다. 연구는 이차원문제로, 경계요소법을 이용한 수치해석적 방법에 의해 수행되었으며, 진동원은 수직방향으로 조화가 진을 받는 줄기초이다. 검토된 지반은 세 가지로, 균질의 반무한 지반과, 단단한 상부층의 두께를 달리하는 두 개의 지반이다. 단단한 상부층을 갖는 지반에서는 굴절의 지반과 비교하여 아주 커다란 진폭의 감소가 나타났으며, 진동전파 속도의 경우, 물성치에 의해 계산으로 구해지는 진동전파 속도만큼의 크기가 나타나지 않았다. 더욱이 동결지반에서의 진폭은 비동결지반에서 보다 거리에 따라 아주 작은 값이 구해졌다.

• Steel and Composite Structures
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• 제25권2호
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• pp.157-175
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• 2017

The novelty of this work is the use of a new displacement field that includes undetermined integral terms for analyzing thermal buckling response of functionally graded (FG) sandwich plates. The proposed kinematic uses only four variables, which is even less than the first shear deformation theory (FSDT) and the conventional higher shear deformation theories (HSDTs). The theory considers a trigonometric variation of transverse shear stress and verifies the traction free boundary conditions without employing the shear correction factors. Material properties of the sandwich plate faces are considered to be graded in the thickness direction according to a simple power-law variation in terms of the volume fractions of the constituents. The core layer is still homogeneous and made of an isotropic material. The thermal loads are assumed as uniform, linear and non-linear temperature rises within the thickness direction. An energy based variational principle is employed to derive the governing equations as an eigenvalue problem. The validation of the present work is checked by comparing the obtained results the available ones in the literature. The influences of aspect and thickness ratios, material index, loading type, and sandwich plate type on the critical buckling are all discussed.

• 한국건축시공학회지
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• 제2권3호
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• pp.163-170
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• 2002

Recently, polishing tile(porcelain homogeneous polished tile) was used in the construction field as a finishing material. But, there happened some problems such as tile exfoliation by construction condition in early ages. Also, for use of polishing tile in the dry wall system which used to lightweight wall, the examination of adhesive stability of polishing tile is needed. In this study, adhesive strength of Polishing tile was investigated by tile bond types on gypsum board and non asbestos board coated by tar-urethane and Polymer modified cementitious waterproofing membrane(Series I). Then, the effect of heat stress and vibration was estimated on gypsum and non asbestos board(Series II). As the result of study are the follows; (1) Polishing tile(600$\times$400mm) construction on waterproofing layer : Both laboratory estimation and spot examination sieve were happened that fall of tile because their hardening speed is late. (2) To using powder style adhesives in the dry wail with waterproofing layer : Adhesive strength of tile is Influenced by interface bond area and base side condition. (3) Shock and heat stresses : obvious decline of adhesive strength is not happened

• 방사선산업학회지
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• 제17권4호
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• pp.345-357
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• 2023

Nuclear forensics has been understood as a mendatory component in the international society for nuclear material control and non-proliferation verification. Radiochronometry of nuclear activities for nuclear forensics are decay series characteristics of nuclear materials and the Bateman equation to estimate when nuclear materials were purified and produced. Radiochronometry values have uncertainty of measurement due to the uncertainty factors in the estimation process. These uncertainties should be calculated using appropriate evaluation methods that are representative of the accuracy and reliability. The IAEA, US, and EU have been researched on radiochronometry and uncertainty of measurement, although the uncertainty calculation method using the Bateman equation is limited by the underestimation of the decay constant and the impossibility of estimating the age of more than one generation, so it is necessary to conduct uncertainty calculation research using computer simulation such as Monte Carlo method. This highlights the need for research using computational simulations, such as the Monte Carlo method, to overcome these limitations. In this study, we have analyzed mathematical models and the LHS (Latin Hypercube Sampling) methods to enhance the reliability of radiochronometry which is to develop an uncertainty algorithm for nuclear material radiochronometry using Bateman Equation. We analyzed the LHS method, which can obtain effective statistical results with a small number of samples, and applied it to algorithms that are Monte Carlo methods for uncertainty calculation by computer simulation. This was implemented through the MATLAB computational software. The uncertainty calculation model using mathematical models demonstrated characteristics based on the relationship between sensitivity coefficients and radiative equilibrium. Computational simulation random sampling showed characteristics dependent on random sampling methods, sampling iteration counts, and the probability distribution of uncertainty factors. For validation, we compared models from various international organizations, mathematical models, and the Monte Carlo method. The developed algorithm was found to perform calculations at an equivalent level of accuracy compared to overseas institutions and mathematical model-based methods. To enhance usability, future research and comparisons·validations need to incorporate more complex decay chains and non-homogeneous conditions. The results of this study can serve as foundational technology in the nuclear forensics field, providing tools for the identification of signature nuclides and aiding in the research, development, comparison, and validation of related technologies.