• 대한조선학회지
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• 제10권2호
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• pp.9-18
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• 1973

The effects of carburization on the fatigue strength and cracks were studied. The fatigue phenomena of the carburized specimens were compared with noncarburized specimens those were either heat-treated or un-treated. The fatigue strength of these specimens were measured by rotating bending fatigue machine. The obtained results indicated that the fatigue strength of carburized specimens were increased ranging from 24-59 % than those of un-treated, and 22-38% than those of heat-treated. The Vickers hardness of carburized were also increased as much as 138-195% than those of un-treated, and 42-125% than those of heat-treated. The microscopic observation of the carburized specimens mostly composed of minute pearlitic structure at hard case exhibited to have more localized slip than those of non-carburized specimens.

• 열처리공학회지
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• 제35권5호
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• pp.239-245
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• 2022

The purpose of this study is to evaluate the degree of microstructural change of materials using ultrasonic nonlinear parameters. For microstructure change, isothermal heat-treated ferritic 2.25Cr steel and low-cycle fatigue-damage copper alloy were prepared. The variation in ultrasonic nonlinearity was analyzed and evaluated through changes in hardness, ductile-brittle transition temperature, electron microscopy, and X-ray diffraction tests. Ultrasonic nonlinearity of 2.25Cr steel increased rapidly during the first 1,000 hours of deterioration and then gradually increased thereafter. The variation in non-linear parameters was shown to be coarsening of carbides and an increase in the volume fraction of stable M6C carbides during heat treatment. Due to the low-cycle fatigue deformation of oxygen-free copper, the dislocation that causes lattice deformation developed in the material, distorting the propagating ultrasonic waves, and causing an increase in the ultrasonic nonlinear parameters.

• 대한안전경영과학회:학술대회논문집
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• 대한안전경영과학회 2009년도 춘계학술대회
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• pp.413-421
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• 2009

This paper investigates tensile characteristics of the stress aging heat-treated SM45C steel which are aging temperature at $250^{\circ}C$, $300^{\circ}C$, aging time at 1, 3 hours, and applied load at 300, 400N conditions by using acoustic emission. Most suitable aging condition was aging temperature $300^{\circ}C$, aging time 1 hour, and aging applied load 300N. And increased yield load 28.3% than non-treatment specimen in this condition. AE energy in elastic limit increased about 16.7 times than non-treatment specimen. When aging time is 3 hours, yield load decreased than other conditions that possibility is high to have itself defect on inside the specimen or coarse grain size precipitation is different in happened over-aging phenomenon. Especially, in case of $300^{\circ}C$, 3 hours and 400N condition appeared AE energy in elastic limit fairly high about 30 times than non-treatment specimen. This is considered by emit a lot of energies when material causes plastic deformation because the ductility increases on specimen by over-aging phenomenon.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 추계학술대회 논문집
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• pp.132-136
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• 2009

The importance and interests for saving of energy and cost in industry has been steadily grown up. Therefore, process optimization to reduce the processing step and energy is one of the most important things. The micro-alloyed steel of which post-heat-treatment is not necessary, has attractive points for high strength materials. However, for the application of non-heat-treated steel to structural parts, it is necessary to confirm the reliability of mechanical properties. In order to estimate mechanical properties. The microstructure, hardness, tensile strength, compressive strength and tensile fatigue strength of micro-alloyed steel having 900MPa tensile strength has been investigated.

• Corrosion Science and Technology
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• 제23권4호
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• pp.283-288
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• 2024

Hot-dip Zn-Mg-Al coatings have a complex microstructure consisting of Zn, Al, and MgZn₂ phases. Its crystal structure depends on alloy content and cooling rates. Microstructure and corrosion resistance of these coatings might be affected by heat treatment. To investigate effect of heat treatment on microstructure and corrosion resistance of Zn-Mg-Al coatings, Zn-1.5%Mg-1.5%Al coated steel was heated up to 550 ℃ at a heating rate of 80 ℃/s and cooled down to room temperature. At above 500 ℃, the ternary phase of Zn-MgZn₂-Al was melted down. Only Zn and MgZn₂ phases remained in the coating. Heat- and non-heat-treated specimens showed similar corrosion resistance in Salt Spray Test (SST). When a Zn-3.0%Mg-2.5%Al coated steel was subjected to heat treatment at 100 ℃ or 300 ℃ for 200 h and compared with GA and GI coated steels, the microstructure of coatings was not significantly changed at 100 ℃. However, at 300 ℃, most Al in the coating reacted with Fe in the substrate, forming a Fe-Al compound layer in the lower part of the coating. MgZn₂ was preferentially formed in the upper part of the coating. As a result of SST, Zn-Mg-Al coated steels showed excellent corrosion resistance, better than GA and GI.

• 대한기계학회논문집A
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• 제22권2호
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• pp.311-320
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• 1998

The cryogenic fracture behaviors of austenitic stainless steel HN2 developed for nuclear fusion reactor were evaluated quantitatively by using the small punch(SP) test. The electrochemical polarization test was applied to study thermal aging degradation of HN2 steel. The X-ray diffraction(XRD) analysis was conducted to detect carbides and nitrides precipitated on the grain boundary of the heat treated HN2 steel. The mechanical properties of the HN2 steel significantly decreased with increasing time and temperature of heat treatment or with decreasing testing temperature. The integrated charge(Q) obtained from electrochemical polarization test showed a good correlation with the SP energy(ESP) obtained by means of SP tests. From the results observed in the x-ray diffraction and anodic polarization curve, it was known that the material the grain boundary. Combining SP test and electrochemical polarization test, it could be useful tools to non-destructively evaluate the cryogenic fracture behaviors and the aging degradation for cryogenic structural material.

• Applied Science and Convergence Technology
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• 제24권4호
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• pp.84-89
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• 2015

The base pressure and outgassing rate of a mild steel chamber were measured and compared to those of a stainless steel chamber. A combined sputter-ion and non-evaporable getter pump with a nominal pumping speed of 490 l/s generated the base pressure of $2.7{\times}10^{-11}$ mbar in the mild steel chamber and $1.2{\times}10^{-10}$ mbar in the stainless steel chamber. The rate-of-rise measurements show that the mild steel has an extremely low outgassing rate of $2.6{\times}10^{-13}$ mbar $ls^{-1}cm^{-2}$, which is about one-order of magnitude smaller than the outgassing rate of the stainless steels. Vacuum annealing of the mild steel at $850^{\circ}C$ reduced the outgassing rate further to $8.8{\times}10^{-14}$ mbar $ls^{-1}cm^{-2}$, which was comparable to the outgassing rate of a heat treated stainless steel for extreme-high vacuum use.

• 한국기계가공학회지
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• 제21권3호
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• pp.12-21
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• 2022

Directed energy deposition (DED) was adopted as a metal additive manufacturing method to develop a mold for the hot stamping process. The test piece was machined from Heatvar laminate material, and results were obtained through microstructure and defect observations, as well as hardness, tensile strength, and joint strength tests. 1) Spherical pores and irregular-shaped cavities were observed as lamination defects, and columnar dendrites formed in the structure, which tended to become coarse upon heat treatment. 2) The hardness of the heat-treated material (480HV) was slightly lower than that of the non-heat-treated material (500HV). 3) In the tensile test, the maximum tensile stress and strain of the heat-treated material were 1392 MPa and 15%, respectively, which were slightly higher than the values of 1381 MPa and 13%, respectively, for the non-heat-treated material. 4) In the case of the early final fracture in the tensile test, in most cases, pores or irregularly shaped cavities were observed at the fracture surface or near the surface. 5) In the joint strength test, most of the specimens finally fractured in the laminated metal area, and the fracture surface was intragranular. In addition, dimples formed over the entire area on the fracture surface of the fractured specimen after sufficient elongation.

• 한국기계가공학회지
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• 제12권2호
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• pp.20-26
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• 2013

This study focused on how it affects the surface roughness of work piece in cutting SCM415 steel, widely used steel in industry, by TiCN and TiN tools. Following conclusion was drawn from several experiments. The surface roughness of heat treated workpiece was better than that of non heat-treated materials. Moreover, the roughness of surface roughness(Ra 0.25) on feeding rate of 0.05 was better when it was in wet process, rather than dry process. As the feeding rate increases, TiCN coating tool shows better roughness of surface than TiN tool. Also, in heated treatment, TiCN coating tool shows the least straightness dimension deviation at feeding rate of 0.05, 0.15mm/rev, and concave-like R shape appears by the feeding rate orders of 0.05, 0.15, 0.1, 0.125 and 0.075mm/rev.

• 대한금속재료학회지
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• 제47권9호
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• pp.573-579
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• 2009

Titanium/aluminum/stainless steel(Ti/Al/STS) clad materials have received much attention due to their high specific strength and corrosion-resisting properties. However, it is difficult to fabricate these materials, because titanium oxide is easily formed on the titanium surface during heat treatment. The aim of the present study is to derive optimized cladding conditions and thereupon obtain the stable quality of Ti/Al/STS clad materials. Ti sheets were prepared with and without pre-heat treatment and Ti/Al/STS clad materials were then fabricated by cold rolling and a post-heat treatment process. Microstructure of the Ti/Al and STS/Al interfaces was observed using a Scanning Electron Microscope(SEM) and an Energy Dispersed X-ray Analyser(EDX) in order to investigate the effects of Ti pre-heat treatment on the bond properties of Ti/Al/STS clad materials. Diffusion bonding was observed at both the Ti/Al and STS/Al interfaces. The bonding force of the clad material with non-heat treated Ti was higher than that with pre-heat treated Ti before the cladding process. The bonding force decreased rapidly beyond $400^{\circ}C$, because the formed Ti oxide inhibited the joining process between Ti and Al. Bonding forces of STS/Al were lower than those of Ti/Al, because brittle $Fe_3Al$, $Al_3Fe$ intermetallic compounds were formed at the interface of STS/Al during the cladding process. In addition, delamination of the clad material with pre-heat treated Ti was observed at the Ti/Al interface after a cupping test.