• 한국해양공학회지
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• 제9권1호
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• pp.101-110
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• 1995

In SMA(Shape Memory Alloy), the degradation by fatigue is one of the most important problems to be overcome, when SMA is used for robot-actuator materials. The actuator is operated repetitively for long time and its repeating operation develops the fatigue degradation of SMA. The fatigue degradation changes the transformation temperature and deformation behavior and results in inaccurate operation and deformation which results form repeating operation is to be investigated in advance and the scheme to resolve those problems have to be made for the design of actuator. In this paper, for the improvement of the fatigue degradation by repetive movement and better control of the correct movement by the stability of martensite transformation in the development of Robots actuator, Pre-strain(0, 1.5, 5, 8%) are loaded in the specimens and fatigue testing were carried out by the method of heating and cooling in direct condition. From the results of these experiments, the effect on pre-strain which affect the transformation characteristic and fatigue degradation phenomena were correctly investigated.

• 한국생산제조학회지
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• 제20권6호
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• pp.720-728
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• 2011

Lap joint welding conducts low carbon steel plates using a 2.0kW continuous wave Nd:YAG laser beam. The specimen is composed of thin plate of 20 sheets. Process Variables contain two controlled parameters of the laser power and the welding speed. In order to quantitatively examine the characteristics of the lap welding, the welding quality of the cut section, stain-stress behavior, and the hardness of the welded part are investigated. The weld width difference between the top and the bottom because the welding speed is increased. The reason, cooling rate is decreased because of fast welding speed. When the heat input is higher, larger volume of the base metal will melt and the welding heat has longer time to conduct into the bottom from the top. The microstructure and tensile properties of the joints are investigated in order to analyze the effects of heat input on the quality of laser welded specimen. From the results of the investigation, We observe that welding quality is good for the laser power of 1800W, and laser welding speed from 1.8m/min to 2.2m/min.

• 대한기계학회논문집A
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• 제31권4호
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• pp.525-531
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• 2007

The operating temperature has been increased to improve the efficiency of gas turbine. The most advanced Gas turbine is operated at above $1,500^{\circ}C$. Improvement in material and cooling method permit hot gas path component to run at increased temperature. But, the repair of blades which are developed with advanced manufacture technique is difficult to use normal welding. Most of gas turbine blades are made of precipitation harden nickel base superalloy, which is very hard to weld. Therefore, the employment of welding filler on blade is solid solution nickel base superalloy(Hastelloy X, Inconel 617). In this study, Tensile test in high temperature was conducted on welded GTD111DS with GTD111 to evaluate effect of variation of pre, post treatment. The result of this study showed that the specimen was treated with optimum pre and post treatment(preweld HT($1200^{\circ}C$), Post treatment($1100^{\circ}C$ HIP, $1200^{\circ}C$ + $1100^{\circ}C$ + $800^{\circ}C$ HT) is mush superior.

• Corrosion Science and Technology
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• 제10권2호
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• pp.60-64
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• 2011

Lean duplex stainless steels have been developed in Korea for the purpose of being used in the seawater systems of industry. There are also many important seawater systems in nuclear power plants. These systems supply seawater to cooling water condenser tubes, heat exchanger tubes, related pipes and chlorine injection systems. The flow velocity of some part of seawater systems in nuclear power plants is high and damages of components from corrosion are severe. The considered lean duplex stainless steels are STS329LD (20.3Cr-2.2Ni-1.4Mo) and STS329J3L (22.4Cr-5.7Ni-3Mo) and PRENs of them are 29.4 and 37.3 respectively. Physical, mechanical and micro-structural properties of them are evaluated, and electrochemical corrosion resistance is measured quantitatively in NaCl solution. Critical Pitting Temperatures (CPT)s are measured on these alloys and pit depths are evaluated using laser microscope. Long period field tests on these alloys are now being performed, and some results are going to be presented in the following study.

• Journal of Welding and Joining
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• 제16권3호
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• pp.111-120
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• 1998

To predict and evaluate metallurgical and mechanical behavior of th welds, it is essential to understand solidification behavior and microstructural evolution experienced in the welds, neither of which follows the equilibrium phase diagram because of rapid heating and cooling conditions. Metallurgical phenomena in austenitic stainless steel fusion welds, types 304, 309S, 316L, 321 and 304N, were investigated in this study. Autogenous GTA welding was performed on weld coupons, and primary solidification mode and phase distribution were investigated from the welds. Varestraint test was employed to evaluate solidification cracking susceptibilities of the alloys. GTA weld fusion zones in type 304, 321 and 304N stainless steels experienced primary ferrite solidification while those in type 309S primary austenite solidification. Type 316L exhibited a mixed type of primary ferrite and primary austenite solidification. The primary solidification mode strongly depended on $Cr_{eq}/Ni_{eq}$ ratio. In terms of solidification cracking susceptibility, type 309S that solidified as primary austenite exhibited high cracking susceptibility while the alloys experienced primary ferrite solidification showed low cracking susceptibility. The relative ranking in solidification cracking susceptibility was type 304=type 304N < type 321 < type 316L < type 309S.

• 대한금속재료학회지
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• 제46권6호
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• pp.377-381
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• 2008

Prism sheet of LCD BLU which depends on supply from Japan and U.S.A was studied by using Si anisotropic etching and injection molding technologies. First, the prism sheet was patterned on Si wafer through photolithography, and the best conditions of Si etching were determined through etching Si wafer with TMAH to obtain straight optimized zigzag patterns, and a cross pattern to provide light diffusion and concurrent focusing. The etch rate of TMAH was concluded to be constant for $25wt%-70^{\circ}C$ condition. Ni stamp of prism sheet was made by electrodeposition using patterned Si wafer, normal or fast H/C(Heating/Cooling) injections were carried out to fabricate prism sheet. It was known that fast H/C injection could fabricate prism sheet more accurately than normal injection. Zigzag patterns and the cross pattern showed higher transmissivity than the straight patterns because of light diffusion through diagonal direction. The fast H/C injection for zigzag patterns showed lower transmissivity than normal injection because there occurred more light diffusion through precise injection patterns, but the fast H/C injection for straight patterns showed only refraction without diffusion, causing lower transmissivity than normal injection.

• 한국자기학회지
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• 제16권5호
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• pp.255-260
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• 2006

기본조성 $(Ni_{0.35}Cu_{0.2}Zn_{0.45})_{1.02}(Fe_2O_3)_{0.98}$과 NiO 비율을 증가시키고 ZnO을 감소시킨 또 다른 기본조성 $(Ni_{0.4}Cu_{0.2}Zn_{0.4})_{1.02}(Fe_2O_3)_{0.98}$에 grain boundary의 높은 저항층을 형성하고 flux로서 사용하기 위해서 0.1 mol% $CaCO_3$와 입자의 성장을 촉진시켜 낮은 손실, 높은 투자율을 얻기 위한 목적으로 $V_2O_5$를 0.03mo1% 첨가하였다. 이들 원료들을 혼합한 후 $600^{\circ}C$에서 2시간 동안 가소시킨 분말을 toroid 시편으로 만들어 소결온도 $1,050^{\circ}C,\;1,070^{\circ}C,\;1,100^{\circ}C$에서 각각 2시간 동안 공기 중에서 소결하였다. 각 시편들에 대한 밀도는 $4.90{\sim}5.10g/cm^3$으로 나타났고, 각 시편들의 고유저항은 $10^8{\sim}10^{12}{\Omega}-cm$으로 측정되었으며, 결정립의 크기는 대략 $3.0{\sim}8.0{\mu}m$이었다. 시편들의 자기유도 특성 값이 대부분 우수하게 나타났으며, 그 중에서도 기본조성 $(Ni_{0.4}Cu_{0.2}Zn_{0.4})_{1.02}(Fe_2O_3)_{0.98}$에 $CaCO_3$와 $V_2O_5$를 첨가하고 $1,070^{\circ}C$에서 소결한 시편의 특성 값이 잔류자기유도 1,660 G, 최대자기유도 4,000 G로 약간 더 우수하게 측정되었으며, 각각 시편들의 보자력은 $0.15{\sim}0.25\;Oe$로 전형적인 연자성 재료의 범위로 나타났다. 초투자율, 손실계수, 및 큐리온도는 각각 $2,948{\sim}2,997,\;171{\sim}208,\;191{\sim}202^{\circ}C$로 나타나 Ni-Zn ferrite에서 측정되는 값들과 대동소이했다. 물리적인 특성값(고유저항, 자기유도, 초투자율, 손실계수, 큐리온도 등)으로 미루어보아 각종 microwave 통신기기 core 및 고 투자율 deflection yoke core 등으로 사용이 가능하다.

• 한국산학기술학회논문지
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• 제13권2호
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• pp.808-816
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• 2012

본 논문은 열 해석 시뮬레이션과 주조로의 구조 변경을 통한 실리콘 잉곳의 방향성 응고에 대한 연구이다. 열 해석 시뮬레이션에 의한 결과, 용융은 유지 시간이 80분일 때 실리콘이 전체적으로 고르게 용융 온도에 도달하였고 냉각은 상부 냉각 온도가 $1,400^{\circ}C$와 60분 냉각 시 가장 좋은 결과 값을 나타내었다. 제작된 웨이퍼가 기존의 상용웨이퍼보다 결정립계에서의 에칭이 훨씬 적게 이루어졌다. FTIR 측정결과 산소와 탄소 모두 모두 임계값 이하의 불순물로 존재함을 확인하였다. NAA 분석 결과 총 18가지 금속 불순물이 검출 되었지만, 농도 분포는 같은 위치에서 위와 아래의 차이는 크게 나지 않고, 어떤 특정한 위치에서 한쪽으로 집중되거나 어떤 경향성 없이 전체의 샘플의 모든 부분에서 농도가 거의 일정하게 분포를 나타냈다.

• 한국분말재료학회지
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• 제23권3호
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• pp.247-253
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• 2016

In this study, solid solution heat treatment of consolidated nickel-based superalloy powders is carried out by hot isotactic pressing. The effects of the cooling rate of salt quenching, and air cooling on the microstructures and the mechanical properties of the specimens are analyzed. The specimen that is air cooled shows the formation of serrated grain boundaries due to their obstruction by the carbide particles. Moreover, the specimen that is salt quenched shows higher strength than the one that is air cooled due to the presence of fine and close-packed tertiary gamma prime phase. The tensile elongation at high temperatures improves due to the presence of grain boundary serrations in the specimen that is air cooled. On the contrary, the specimen that is salt quenched and consists of unserrated grain boundaries shows better creep properties than the air cooled specimen with the serrated grain boundaries, due to the negative creep phenomenon.

• 한국재료학회지
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• 제22권1호
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• pp.42-45
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• 2012

The mechanical behavior and microstructural evolution during high temperature tensile deformation of recrystallized Ni3Al polycrystals doped with boron were investigated as functions of initial grain size, tensile strain rate and temperature. In order to obtain more precise information on the deformation mechanism, tensile specimens were rapidly quenched immediately after deformation at a cooling rate of more than $2000Ks^{-1}$, and were then observed by transmission electron microscopy (TEM). Mechanical tests in the range of 923 K to 1012 K were carried out in a vacuum of less than $3{\times}10^{-4}$ Pa using an Instron-type machine with various but constant cross head speeds corresponding to the initial strain rates from $1.0{\times}10^{-4}$ to $3.1{\times}10^{-5}s^{-1}$. After heating to deformation temperature, the specimen was kept for more than 1.8 ks before testing. The following results were obtained: (1) Flow behavior was affected by initial strain size; with decreasing initial grain size, the level of a stress peak in the true stress-true strain curve decreased, the steady state region was enlarged and elongation increased. (2) On the basis of TEM observation of rapidly quenched specimens, it was confirmed that dynamic recrystallization certainly occurred on deformation of fine-grained ($3.3{\mu}m$) and intermediate-grained ($5.0{\mu}m$) specimens at an initial strain rate of $3.1{\times}10^{-5}s^{-1}$ and at 973 K. (3) There were some dislocation-free grains among the new recrystallized grains. The obtained results suggest that both dynamic recrystallization and grain boundary sliding are operative during high temperature deformation.