• Title/Summary/Keyword: National measurements standards

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Development of Primary Standard Gas Mixtures of Fourteen Volatile Organic Compounds in Hazardous Air Pollutants for Accurate Ambient Measurements in Korea (at 1 μmol/mol Levels) (유해대기오염물질 중 14종의 휘발성유기화합물 1차 표준가스개발 (1 μmol/mol 수준))

  • Kang, Ji Hwan;Kim, Young Doo;Kim, Mi Eon;Lee, Jinhong;Lee, Sangil
    • Journal of Korean Society for Atmospheric Environment
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    • v.34 no.2
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    • pp.331-341
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    • 2018
  • Hazardous air pollutants(HAPs) in the atmosphere are regulated as major air pollutants in Korea by the Air Pollution Control Act. In order to manage and control HAPs, accurate standards, which are traceable to the International System of Units(SI), are required. In this study, primary standard gas mixtures(PSMs) of volatile organic compounds(VOCs) which are specified as HAPs were developed at $1{\mu}mol/mol$ levels. The selected fourteen VOCs include Benzene, Toluene, Ethylbenzene, m-Xylene, Styrene, o-Xylene, Chloroform, 1,1,2-Trichloroethane, Trichloroethylene, Tetrachloroethylene, 1,1-Dichloroethane, Carbon tetrachloride, 1,3-Butadiene, and Dichloromethane. The HAPs PSMs were gravimetrically prepared in aluminum cylinders and their consistency was verified within the relative expanded uncertainty of 0.71% (k=2). Potential adsorption loss onto the internal surface of cylinders was estimated by cylinder-to-cylinder division method. No adsorption loss was observed within the uncerainty of 0.53%. The long-term stability of the HAPs PSMs was evaluated comparing with freshly prepared HAPs PSMs. The HAPs PSMs were stable for one year within the uncertainty of 0.38%. The final uncertainty of the PSMs was determined by combining the preparation uncertainty, verification uncertainty, and stability uncertainty. Finally, traceable and stable HAPs PSMs at $1{\mu}mol/mol$ levels were developed with the uncertainty of less than 0.76% in high-pressure aluminum cylinders.

The Development Study of A Manganese Sulphate Bath System ($MnSO_4$용액조 장치 개발 연구)

  • Hwang, Sun-Tae;Lee, Kyung-Ju;Choi, Kil-Oung;Kim, Won-Sik
    • Journal of Radiation Protection and Research
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    • v.11 no.1
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    • pp.70-76
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    • 1986
  • In order to establish the national standards of neutron measurements, a manganese sulphate ($MnSO_4$) bath system was developed under the IAEA technical support. This bath system was made up of a spherical s.s. 316 L bath, of 3.5 mm thick and of 125 cm internal diagmeter, filled with a manganese sulphate solution, a solution circulating system, and a $^5Mn\;{\gamma}-ray$ monitoring system. The solution pumped from the bath was introduced into a Marinelli beaker-type monitor vessel which was equipped with two seperate detectors, $3.8cm{\phi}{\times}3.8cm$ NaI(T1) crystals. The performance of the system were tested using the neutron sources, $^{241}Am-Be\;and\;^{252}Cf$, mounted at the center of the bath. From the decay curve analysis of $^{56}Mn$ activity, neutron emission rate of $^{252}Cf$ by the comparative method was obtained to be $3.71{\times}10^7\;n/s\;per\;50{mu}g$ as of November 15, 1985.

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Tunable compression of wind tunnel data

  • Possolo, Antonio;Kasperski, Michael;Simiu, Emil
    • Wind and Structures
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    • v.12 no.6
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    • pp.505-517
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    • 2009
  • Synchronous wind-induced pressures, measured in wind-tunnel tests on model buildings instrumented with hundreds of pressure taps, are an invaluable resource for designing safe buildings efficiently. They enable a much more detailed, accurate representation of the forces and moments that drive engineering design than conventional tables and graphs do. However, the very large volumes of data that such tests typically generate pose a challenge to their widespread use in practice. This paper explains how a wavelet representation for the time series of pressure measurements acquired at each tap can be used to compress the data drastically while preserving those features that are most influential for design, and also how it enables incremental data transmission, adaptable to the accuracy needs of each particular application. The loss incurred in such compression is tunable and known. Compression rates as high as 90% induce distortions that are statistically indistinguishable from the intrinsic variability of wind-tunnel testing, which we gauge based on an unusually large collection of replicated tests done under the same wind-tunnel conditions.

Structural and Magnetic Properties of LiZnO Added MgFe2O4 Composite

  • Tadi, Ravindar;Kim, Yong-Il;Kim, Cheol-Gi;Ryu, Kwon-Sang
    • Journal of Magnetics
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    • v.15 no.4
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    • pp.165-168
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    • 2010
  • $Li_{0.1}Zn_{0.9}O$ and $MgFe_2O_4$ powders were synthesized using chemical methods and mixed in different proportions to prepare a mixture of $Li_{0.1}Zn_{0.9}O$ and $MgFe_2O_4$ that was thermally treated between 900 to $1100^{\circ}C$ for 1 hour. Structural characterization was done using X-ray powder diffraction measurements. Grain sizes and morphologies of $Li_{0.1}Zn_{0.9}O$, $MgFe_2O_4$, and $Li_{0.1}Zn_{0.9}O+MgFe_2O_4$ samples were observed using a scanning electron microscope. Variation of magnetic properties of the $Li_{0.1}Zn_{0.9}O+MgFe_2O_4$ samples due to the addition of $Li_{0.1}Zn_{0.9}O$ was studied in relation to the structural changes occurring due to the thermal treatment. In particular, changes in the cationic distribution between the tetrahedral and octahedral positions were studied with respect to the increase of the annealing temperature. Magnetization was found to be dependent on the cations distributed in the tetrahedral and octahedral sites of the $MgFe_2O_4$.

Time-resolved photoluminescence spectroscopy of InGaN multiple quantum wells

  • Lee, Joo-In;Shin, Eun-joo;Lee, J.Y. m;Kim, S.T.;G.S. Lim;Lee, H.G.
    • Journal of Korean Vacuum Science & Technology
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    • v.4 no.1
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    • pp.23-26
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    • 2000
  • We have fabricated by metal organic chemical vapor deposition (MOCVD) In$\_$0.13/Ga$\_$0.87/N/GaN multiple quantum well (MQW) with thickness as thin as 10 A and barriers also of th same width on (0001) sapphire substrate. We have investigated this thin MQW by steady-state and time-resolved photoluminescence(PL) in picosecond time scale in a wide temperature range from 10 to 290 K. In the PL at 10 K, we observed a broad peak at 3.134 eV which was attributed to the quantum well emission of InGaN. The full width at half maximum (FWHM) of this peak was 129 meV at 10 K and its broadening at low temperatures was considered to be due to compositional fluctuations and interfacial disorder in the alloy. The narrow width of the quantum well was mainly responsible for the broadening of the emission linewidth. We also observed an intense and sharp peak at 3.471 eV of GaN barrier. From the temperature dependent PL measurements, the activation energy of the InGaN quantum well emision peak was estimated to be 69 meV. The lifetime of the quantum well emission was found to be 720 ps at 10 K, which was explained in terms of the exciton localization arising from potential fluctuations.

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150 nm Pitch Measurement using Metrological AFM (길이 소급성을 갖는 AFM을 이용한 150nm 피치 측정)

  • ;I. Misumi;S. Gonda;T. Kurosawa
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.264-267
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    • 2003
  • Pitch measurements of 150 nm pitch one-dimensional grating standards were carried out using an contact mode atomic force microscopy(C-AFM) with a high resolution three-axis laser interferometer. It was called as 'Nano-metrological AFM' In Nano-metrological AFM, Three laser interferometers were aligned well to the end of AFM tip. Laser sources of the three-axis laser interferometer in the nano-metrological AFM were calibrated with an I$_2$-stablilzed He-Ne laser at a wavelength of 633 nm. So, the Abbe error was minimized and the result of the pitch measurement using the nano-metrological AFM has a traceability to the length standard directly. The uncertainty in the pitch measurement was estimated in accordance with the Guide to the Expression of Uncertainty in Measurement(GUM). The Primary source of uncertainty in the pitch-measurements was derived from repeatability of pitch-measurement, and its value was approx 0.186 nm. Expanded uncertainty(k=2) of less than 5.23 nm was obtained. It is suggested that the metrological AFM is a useful tool for the nano-metrological standard calibration.

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Effect of Nitrogen Treatment on the Structure and Magnetic Properties of $RuSr_2(EuCe)Cu_2O_z$ Compound (질소 열처리에 따른 $RuSr_2(EuCe)Cu_2O_z$ 계의 구조 및 자기적 특성)

  • Lee, H.K.;Kim, Y.I.;Kim, Y.C.
    • Progress in Superconductivity
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    • v.13 no.3
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    • pp.178-183
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    • 2012
  • Two $RuSr_2(EuCe)Cu_2O_z$ samples (as prepared and after $N_2$ treatment) have been investigated by thermogravimetric (TC) analysis, high-resolution x-ray powder diffraction and magnetization measurements. TG measurements which were carried out in $H_2/Ar$ atmosphere showed that the $N_2$ treatment of the as-prepared sample at $650^{\circ}C$ for 2h leads to a decrease in the oxygen content z by about 0.25. This oxygen depletion was accompanied by an increase in the magnetic transition temperature from 54.0 K to 114.9 K. This magnetic behavior is discussed in connection with the results of Rietveld analysis of the x-ray diffraction data which showed that the $N_2$ treatment resulted in both a significant increase in the rotation angle of the $RuO_6$ octahedra and a decrease in c-lattice parameter of the sample.

Estimation of Measurement Uncertainty for Vibration Tests in the Machine Tool Main Spindle (공작기계 주축회전체 진동 측정에서의 불확도 추정 방법)

  • Lee, Jung-Hoon;Yoon, Sang-Hwan;Chau, Dinh Minh;Park, Min-Won
    • Journal of the Korean Society for Precision Engineering
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    • v.28 no.4
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    • pp.404-409
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    • 2011
  • Report on the notion of uncertainty is important. The reason is that the measured value includes a lot of uncertain factors. Reliable results can't be derived without the notion of uncertainty. The mathematical model to evaluate uncertainty considering the quality of vibration is important to evaluate uncertainty, and it must contain the every quantity which contributes significantly to uncertainty in the measured results. In this paper, the evaluation of uncertainty analysis about rotor vibration measurements of machine tools is presented to evaluate the most important factors of uncertainty.

A Study on Development of Chinese Men's Apparel Sizing System (중국(中國) 성인남성용(成人男性用) 의류치수규격(衣類値數規格) 설정연구(設定硏究) I)

  • Sohn, Hee-Soon;Lim, Soon;Kim, Jee-Yeon
    • Journal of Fashion Business
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    • v.8 no.1
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    • pp.1-15
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    • 2004
  • The purpose of this study is to provide for some basic data useful to production of the apparels fit and measured well for the Chinese men. For this purpose, Chinese men's apparel measurements and specifications were determined per area group(Beijing/ Shanghai) according to the Men's Wear Specifications (GB/T 1335.1-1997), National Standards of People's Republic of China. The collected data were statistically processed using SAS 6.12 for technical statistical analysis, correlation analysis, factor analysis, group-wise analysis and ANOVA. The results of this study can be summarized as follows; 1. As a result of dividing the Chinese men into Beijing and Shanghai men and thereby, setting height and upper chest circumference for upper garments and height and waist for lower garments. 2. Analyzing the correlations according to the three-fold classifications of height/upper chest circumference/waist for garment specifications, 17 specifications based on heights and upper chest circumferences for Beijing men's upper garments could be designed within the deviation level of 2%, while 15 specifications based on waist measurements could be designed (between $70{\sim}98cm$) for their lower garments within the deviation level of 4%. Thus, a total of 60 combinations of the specifications could be obtained. 3. 16 specifications based on heights and upper chest circumferences for Shanghai men's upper garments could be designed within the deviation level of 2%, while 16 specifications based on waist measurements could be designed (between $68{\sim}98cm$) for their lower garments within the deviation level of 3%. Thus, a total of 56 combinations of the specifications could be obtained. For other reference measurements, grading measures were set for each type and body part, while the average measures of major body parts were calculated.

A Study on the Nutritional Assessment of Early Childhood Using Mid-Upper-Arm Circumference (상박위(上膊圍)에 의(依)한 성장기(成長期) 아동(兒童)에 영양상태(營養狀態)의 판정(判定)에 관(關)한 연구(硏究))

  • Tchai, B.S.;Nam, Y.K.;Chung, Y.J.
    • Journal of Nutrition and Health
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    • v.8 no.4
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    • pp.9-14
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    • 1975
  • Growth retardation and a variable degree of body disproportion are recognized features of malnutrition, and mild and moderate protein-calorie malnutrition(PCM). Among the various body measurements suggested to assess the prevalence of all grades of PCM as judged by growth retardation and by body disproportion, the 'mid-upper-arm circumference'-abbreviated to 'arm-circumference' has been suggested as a potential useful simple field index for the assessment of PCM showing that the measurement would give composite information simultaneously on three important effects on PCM-deficit in the muscle protein reservoirs, availability of calorie stores in the form of subcutaneous fat, and growth failure. And this is selected because of its easy accessibility, and less involvement with clinical edema. This study is conducted to make a comparison between the percentage of Korean weight for age standards and the percentage of mid-upper-arm circumference for age standards of 175 preschool children aged $3{\sim}72$ months who are selected among the low-income residents in Seoul. In this study, a comparison is made between the results obtained by expressing the observed weight of the child as a percentage of Korean standard, referred to as 'weight-for-age' and the observed arm-circumference expressed as a percentage of the age-specific arm standard of Jelliffe, referred to as 'arm-for-age'. All the measurements were taken following the techniques described by Jelliffe. The left mid upper arm was measured using a glass-fibre tape and the Fairbanks Morse beam balance was used for weighing. 80% level of weight for age Korean standard and 85% level of arm for are Jelliffe standard were used as an upper borderline limit for PCM. Comparing the 80% weight-for-age and the 85% arm-for-age standard as an upper limit for PCM, for children aged $3{\sim}72$ months, results in 84.6% agreement with the sensitivity of 86.4% and its specificity of 83.5%. If arm circumference alone had been measured and judgement made on this basis, then only 5.1% of the children would have been 'wrongly' classified. And there is a moderately close correlation between arm circumference and weight for age as the data in Table 4 shows. The problem therefore lies in the standard for arm circumference in normal children and in determining what is the lower limit of normal. Once this is clearly difined, one can rely more confidently on arm circumference measurements alone for the nutritional assessment of early childhood.

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