• Title/Summary/Keyword: National Measurement Standards

검색결과 422건 처리시간 0.024초

Pitch Measurement of 150 nm 1D-grating Standards Using an Nano-metrological Atomic Force Microscope

  • Jonghan Jin;Ichiko Misumi;Satoshi Gonda;Tomizo Kurosawa
    • International Journal of Precision Engineering and Manufacturing
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    • 제5권3호
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    • pp.19-25
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    • 2004
  • Pitch measurements of 150 nm one-dimensional grating standards were carried out using a contact mode atomic force microscopy with a high resolution three-axis laser interferometer. This measurement technique was named as the 'nano-metrological AFM'. In the nano-metrological AFM, three laser interferometers were aligned precisely to the end of an AFM tip. Laser sources of the three-axis laser interferometer in the nano-metrological AFM were calibrated with an I$_2$ stabilized He-Ne laser at a wavelength of 633 nm. Therefore, the Abbe error was minimized and the result of the pitch measurement using the nano-metrological AFM could be used to directly measure the length standard. The uncertainty in the pitch measurement was estimated in accordance with the Guide to the Expression of Uncertainty in Measurement (GUM). The primary source of uncertainty in the pitch-measurements was derived from the repeatability of the pitch-measurements, and its value was about 0.186 nm. The average pitch value was 146.65 nm and the combined standard uncertainty was less than 0.262 nm. It is suggested that the metrological AFM is a useful tool for the nano-metrological standard calibration.

Development of primary reference gas mixtures of 18 volatile organic compounds in hazardous air pollutants (5 nmol/mol level) and their analytical methods

  • Kang, Ji Hwan;Kim, Yong Doo;Lee, Jinhong;Lee, Sangil
    • 분석과학
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    • 제34권5호
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    • pp.202-211
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    • 2021
  • Volatile organic compounds (VOCs) in hazardous air pollutants (HAPs) have been regulated by the Air Pollution Control Act (1978) and their atmospheric concentrations have been monitored in 39 monitor sites in Korea. However, measurement standards of volatile organic compounds (VOCs) in HAPs at ambient levels have not been established in Korea. Primary reference gas mixtures (measurement standards) at ambient levels are required for accurately monitoring atmospheric VOCs in HAPs and managing their emissions. In this study, primary reference gas mixtures (PRMs) at 5 nmol/mol were developed in order to establish primary national standards of VOCs in HAPs at ambient levels. Primary reference gas mixtures (PRMs) were prepared in pressurized aluminum cylinders with special internal surface treatment using gravimetric method. Analytical methods using gas chromatography-flame ionization detector (GC-FID) coupled with a cryogenic preconcentrator were also developed to verify the consistency of gravimetrically prepared HAP VOCs PRMs. Three different columns installed in the GC-FID were evaluated and compared for the retention times and separation of eighteen target components in a chromatogram. Results show that the HAP VOCs PRMs at 5 nmol/mol were consistent within a relative expanded uncertainty (k=2) of less than 3 % except acrylonitrile (less than 6 %) and the 18 VOCs were stable for 1 year within their associated uncertainties.

브리넬 경도 표준 시험기 및 압입 자국 자동 측정장치의 특성 평가에 대한 연구 (A Study on the Evaluation of Brinell Standard Hardness Tester and Automatic Indentation Measurement System)

  • 방건웅;탁내형
    • 열처리공학회지
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    • 제12권4호
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    • pp.294-302
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    • 1999
  • Evaluation of Brinell standard hardness tester was carried out to secure its application as a national standard for Brinell hardness. Accuracies and reliabilities in load application, indenter diameter and indentation measurement were tested through evaluation of these components. The accuracies of load application for various loading conditions were within the limit of ISO and KS specifications. Errors in the indentation measurement due to the difference in personnel characters were successfully removed by utilising automatic indentation measurement system. In overall, the tester and the indentation measuring system were found to be eligible as a national standard of Brinell hardness.

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Comparison of Test Standards for the Performance and Safety of Agricultural Tractors: A Review

  • Kabir, Md. Shaha Nur;Chung, Sun-Ok;Kim, Yong-Joo;Shin, Sung-Hyun
    • Journal of Biosystems Engineering
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    • 제39권3호
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    • pp.158-165
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    • 2014
  • Purpose: The objective of this paper was to compare test standards regarding the performance and safety of agricultural tractors to identify the differences in test conditions, measurement tolerances, and test procedures. Based on the comparison, some recommendations were proposed for possible revisions or improvements to current tractor test standards. Methods: The test standards and codes of major standards development organizations (SDOs), such as the Organization for Economic Cooperation and Development (OECD), the International Organization for Standardization (ISO), the American Society of Agricultural and Biological Engineers (ASABE), EC type approval, and the board of actions of the Nebraska Tractor Test Laboratories (NTTL), were selected and analyzed. Comparison of the test standards: The ISO provides references for fuel and lubricants for tractor tests, and the OECD provides additional measurements for calculating fuel consumption characteristics during the power take-off (PTO) tests. The ISO, EC type approval, and the ASABE provide PTO protective device and the safety requirements. During drawbar power tests, seven transmission ratios are selected for fully automatic transmissions, according to the OECD. In case of hydraulic lift tests, ISO 789-2 and OECD Code 2 advise the use of a static lift force, while SAE J283 advises the use of additional dynamic lift capacity tests for a better representation of in-field operations. The OECD, the ISO, and EC type approval determine the seat index point (SIP), whereas the ASABE determines the seat reference point (SRP) for roll-over protective structure (ROPS) tests. Diversified measurement tolerances were among the braking performance test standards. The European Union (EU) has developed daily limits for vibration exposures with adaptations from ISO 2631-1. Electromagnetic compatibility evaluations are emerging of high-efficiency tractors due to the long-term conformance to electromagnetic emissions and interferences. Comparisons of tractor test standards discussed in this paper are expected to provide useful information for tractor manufacturers and standards development personnel to improve the performance and safety test standards of tractors.

Infrared Thermography Characterization of Defects in Seamless Pipes Using an Infrared Reflector

  • Park, Hee-Sang;Choi, Man-Yong;Park, Jeong-Hak;Lee, Jea-Jung;Kim, Won-Tae;Lee, Bo-Young
    • 비파괴검사학회지
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    • 제32권3호
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    • pp.284-290
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    • 2012
  • Infrared thermography uses infrared energy radiated from any objects above absolute zero temperature, and the range of its application has been constantly broadened. As one of the active test techniques detecting radiant energy generated when energy is applied to an object, ultrasound infrared thermography is a method of detecting defects through hot spots occurring at a defect area when 15~100 kHz of ultrasound is excited to an object. This technique is effective in detecting a wide range affected by ultrasound and vibration in real time. Especially, it is really effective when a defect area is minute. Therefore, this study conducted thermography through lock-in signal processing when an actual defect exists inside the austenite STS304 seamless pipe, which simulates thermal fatigue cracks in a nuclear power plant pipe. With ultrasound excited, this study could detect defects on the rear of a pipe by using an aluminium reflector. Besides, by regulating the angle of the aluminium reflector, this study could detect both front and rear defects as a single infrared thermography image.

교류-직류 변환오차 자동 측정시스템 (An Automatic AC-DC Transfer Error Measurement System)

  • 권성원;조용명;김규태;강전홍;박영태
    • 센서학회지
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    • 제7권6호
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    • pp.401-408
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    • 1998
  • 교류전압표준기인 열전형 전압변환기의 교류-직류 변환오차를 비교평가하기 위하여 이중채널방식 자동측정시스템을 개발하였다. 비교측정되는 2대의 변환기출력을 동시에 측정하여 드리프트의 영향을 감소시켰고, 또 저열기전력 이중채널 스캐너를 사용하여 변환기 출력을 순방향-역방향으로 측정하여 그 평균값을 취함으로서 전압측정기의 ���V전압이 제거되도록 하였다. 정격전압이 동일한 4 V인 변환기끼리 비교 측정한 결과, 주파수 $40\;Hz{\sim}100\;kHz$에서는 외국표준기관에서의 측정값과 약 ${\pm}2\;ppm$ 이내에서 일치하였으며, $200\;kHz{\sim}1\;MHz$ 범위에서는 약 ${\pm}4\;ppm$ 이내에서 일치하였다. 본 시스템의 개발로 변환기의 교류-직류 변환오차의 측정능력을 기존수동방식의 약 ${\pm}15\;ppm$에서 ${\pm}\;3ppm$(100 kHz 이하)로 크게 향상시켰으며, 표준유지 및 산업체 지원의 효율을 크게 높일 수 있게 되었다.

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So, You Need Reliable Magnetic Measurements You Can Use With Confidence? How the Magnetic Measurement Capabilities at NPL Can Help

  • Hall, Michael;Harmon, Stuart;Thomas, Owen
    • Journal of Magnetics
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    • 제18권3호
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    • pp.339-341
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    • 2013
  • The magnetic field standards, facilities and capabilities available at NPL for the calibration of magnetometers and gradiometers and the measurement of the magnetic properties of materials will be introduced. The details of the low magnetic field facility will be explained and the capabilities this facility enables for the characterisation and calibration of ultra-sensitive room temperature magnetic sensors will be presented. Building on core material capabilities that are compliant with the IEC 60404 series of written standards, the example of a standard permeameter that has been modified for the measurement of strips for real world conditions is discussed. This was incorporated into a stress machine to measure the DC properties of the soft magnetic materials used by the partners of a collaborative industry led R&D project at stress levels of up to 700 MPa. The results for three materials are presented and the changes in the properties with applied stress compared to establish which material exhibits favourable properties.

석유정제산업에서의 유기성 유해대기오염물질의 비산배출량 산정 (Estimation of Fugitive Emission of Organic Hazardous Air Pollutants from Oil Refinery Industry)

  • 양성봉;유미선;이영준;유은진;최성헌
    • 한국대기환경학회지
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    • 제24권2호
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    • pp.229-237
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    • 2008
  • Hazardous air pollutants emitted from the oil refinery plant were surveyed from 1993 US and 2005 Korean TRI data. Toluene, xylene, methanol, MTBE and n-hexane, relatively large in amount of fugitive emission, are considered as candidates of newly designated HAPs in Korea. The sealed oil pump, one of equipments among fugitive sources in the crude oil distillation tower was examined for the estimation of amounts of annual HAPs emissions according to several calculation methods using registered emission factors. Emission rates showed to be decreased with following calculation factors; average emission factor>pegged emission factor>concentration emission factor>correlation equation. Annual emission amounts of benzene, toluene, xylene. ethyl benzene and nhexane from the distillation tower were estimated and amounts of these HAPs calculated with TVOC concentrations obtained from LDAR program and correlation equations showed only 6% of those from using concentration factors.