• Title/Summary/Keyword: Nano-pit

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Electrophoretic Deposition of Ni Nano-particles for Self-repairing of Heat Exchanger Tubes

  • Lee, Gyoung-Ja;Pyun, Su-Il;Rhee, Chang-Kyu
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1211-1212
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    • 2006
  • The electrophoretic deposition process of Ni nano-particles was employed for self-repairing of heat exchanger tubes. For electrophoretic deposition of Ni nano-particles on pitted Ni alloy specimen, a constant electric field of 100 V $cm^{-1}$ was applied to the specimen for 180 s in Ni-dispersed solution. It was found that as electrophoretic deposition proceeded, the size of the pit remarkably decreased due to the agglomeration of Ni nano-particles at the pit. This strongly suggests that the electrophoretic mobility of the charged particles is larger for the pit with a higher current value rather than outer surfaces with a lower current value.

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Effectiveness and Preparation of Nano-emulsion of a Rapeseed Oil Extract Originated from Jeju with PIT Emulsifying System (PIT유화시스템을 이용한 제주산 유채씨앗 오일추출물의 나노에멀젼의 제조 및 효과)

  • Joo, Se-Jin;Kim, Hack-Soo;Lee, Jeong-Koo;Lee, Min-Hee;Kim, In-Young
    • Journal of the Korean Applied Science and Technology
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    • v.29 no.3
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    • pp.486-494
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    • 2012
  • Nano-emulsion with phase inversion temperature (PIT) emulsifying system was prepared to use rapeseed oil from originating Jeju in order to apply various cosmetic applications. Natural rape seed oil (NRSO) extraction was extracted using n-hexane as a solvent. NRSO extract showed a light yellowish color of viscous liquid as well as yield was $43{\pm}2.5%$. Acid value was $2.76{\pm}0.5$ and gravity was $0.89{\pm}0.05$. Droplet size of PIT-Yuche-NE with 20wt% of rapeseed oil was 50-120nm (average: $82{\pm}5.8nm$) and zeta potential was -29.5mV. It was thermodynamically good stable emulsion due to $(PEG)_{5-30}$fattyacidether. Some conclusions from the result of characteristic experiment were obtained as follows. First, the anti-oxidative activity was measured by free radical scavenging activity using DPPH (1,1-diphenyl-2-picrylhydrazyl radical). Anti-oxidative activity of PIT-Yuche-NE was $37.2{\pm}6.7%$ on 10mg/mL compared with PIT-Toco-NE (Natural tocopherol nano-emulsion, $28.8{\pm}6.5%$ on 10 mg/mL) and PIT-Nokcha-NE (Green tea extract nano-emulsion, $29.6{\pm}7.2%$ on 10mg/mL). Second, the collagen synthesis activity of PIT-Yuche-NE was $148{\pm}15.2%$ compared with PIT-Toco-NE (Natural tocopherol nano-emulsion, $121{\pm}13.5%$ on 10mg/mL) and PIT-Nokcha-NE (Green tea extract nano-emulsion, $95{\pm}12.7%$ on 10mg/mL). Third, the effectiveness of moisturizing activity of Yuche-CRM with Aramo-TS after 6 hours increase $47{\pm}3.9%$ (*p-value£0.05, n=7) whereas Both Toco-CRM was $30{\pm}5.2%$ (*p-value£0.05, n=7) and Nokcha-CRM was $35{\pm}4.5%$. Therefore, Yuche-CRM has higher moisturizing effect than other two creams. Finally, Nano-emulsion stabilizing rapeseed oil using PIT emulsifying system of this study can be used to apply cosmetics industry and pharmaceutical industry.

Physical Properties and Cytotoxicity of Dental Pit and Fissure Sealants Containing Cerium Oxide Nano Particles(CNPs) (세륨옥사이드나노입자(Cerium Oxide Nano Particles; CNPs)를 첨가한 치면열구전색재의 물리적 특성 및 세포독성)

  • Jeong, Mi-Ae;Kim, Dong-Ae
    • The Journal of the Korea Contents Association
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    • v.22 no.3
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    • pp.586-592
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    • 2022
  • In this study cerium nano particles(CNPs) with 0-4.0 wt% was incorporated to the conventional dental pit and fissure sealant(ConciseTM) to produce new pit and fissure sealant the physical properties and cytotoxicity. The physical properties were measured for polymerizing depth the degree of water absorption and solubility. The cytotoxicity of cell viability was analyzed by MTT assay using immortalized human oral keratinocyte(IHOK). As a result of this preceding study the polymerizing depth was decreased by the increasing of the amount of CNPs. The solubility degree of the sealant added CNPs with 2.0 wt% showed was the lower and the water absorption showed no significantly difference with the control groups(p>0.05). The cytotoxicity test results showed high survival rates in all experimental groups. Therefore, pit and fissure sealant by the addition of CNPs excellent cell viability be produced without weaken the physical property of the cell viability fissure sealant containing CNPs does not weaken physical properties and has no cytotoxic effects biocompatibility. Considering its properties effect of CNPs, further studies are required for distribution technology application.

Changes in the amount of adhesion of Streptococcus mutans to pit and fissure sealant incorporating cerium oxide nano particles(CNPs) (세륨옥사이드나노입자(Cerium oxide nano particles: CNPs)를 함유한 치면열구전색재의 Streptococcus mutans 부착량 변화)

  • Lee, Seong-Sook;Park, Young-Min;Kim, Dong-Ae
    • Journal of Korean society of Dental Hygiene
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    • v.20 no.4
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    • pp.535-543
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    • 2020
  • Objectives: The aim of this study was to investigated the surface roughness and change in the amount of adhesion of Streptococcus mutans to the commercial pit and fissure sealant containing cerium oxide nano particles(CNPs). Methods: The CNPs was incorporated into a commercial pit and fissure sealant at 0-4.0 wt%. Disk Specimens (ϕ 10 mm × 2 mm) were prepared by light polymerization the front and back for 40s. Average surface roughness was measured and Streptococcus mutans adhesion was observed under confocal laser scanning microscopy (CLSM) after 24 hour. Data were statistically analyzed by one-way ANOVA and Tukey HSDa post-hoc test. Results: Difference of the surface roughness(Ra) between groups was not statistically significant in both non CNPs group and CNPs group(p>0.05). In CNPs group, the amount of S. mutans adhesion was significantly different between control group and decreased in order of CNPs 4.0, CNPs 0.5, CNPs 1.0 and CNPs 2.0(p<0.05). Conclusions: Within the limitation of this study, these aspects of oral bacteria performances suggest potential usefulness of the CNPs incorporation, especially CNPs 1% and 2%, in pit and fissure sealant for inducing antibacterial effect.

Skin compatible Microemulsions obtained by a new PIT -Nano- Technology Approach

  • Jorg Schreiber;Ulrich Kux;Anja Eitrich;Wittern, Klaus-Peter;Yvonne Cierpisz
    • Proceedings of the SCSK Conference
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    • 2003.09b
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    • pp.392-404
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    • 2003
  • A new technology to achieve o/w microemulsions allows the formulation of transparent products with low surfactant content. The PIT Nanotechnology approach gives cosmetic/pharmaceutical o/w microemulsions in one step with a broad variety of surfactants, cosurfactants and oil phases.

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Effects of Cerium Oxide Nano Particles(CNP) Containing on The Mechanical of Pit and Fissure Sealant (세륨옥사이드나노입자(CNP)첨가가 치면열구전색재 기계적 성질에 미치는 영향)

  • Jeong, Mi-Ae;Kim, Dong-Ae
    • The Journal of the Korea Contents Association
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    • v.20 no.6
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    • pp.433-438
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    • 2020
  • The aim of this study was to investigate the mechanical properties of pit and fissure sealant containing cerium oxide nano particles(CNP). Used to mix with pit and fissure sealant (ConciseTM, USA). CNP was added into liquid (0- 4.0 wt%) of pit and fissure sealant. The specimens for the vickers hardness (VHN; 10 × 2 mm), Three-point flexure (FS; 2 × 2 × 25 mm) with flexure modulus (FM) were obtained from cements at 1, 7, and 14 days after storing in (37±1)℃ distilled water. All mechanical strength tests were conducted using machine (Instron 3344) with a cross-head speed of 1 mm/min. Data were statistically analyzed by one-way ANOVA and Duncan posthoc test(p<0.05). Mechanical properties of conventional pit and fissure sealant could be enhanced by addition of CNP. Three-point flexure and modulus of pit and fissure sealant containing CNP were showed a slightly higher value not significantly with the group(p>0.05). The vickers hardness values were increase significantly with incubation time(p<0.05). Results indicated that CNP can be used considered as potential reinforcing agent for increasing mechanical properties for conventional pit and fissure sealant. Therefore, it was suggest that the additional effects of CNP and research on a wide range of substances.

Self-repairing Technology by Electrophoresis of Ni Nano-Particles for Heat Exchanger Tubes (Ni 나노입자의 전기영동 코팅에 의한 전열관 자가보수 기술 개발)

  • Lee, Gyoung-Ja;Lee, Min-Ku;Rhee, Chang-Kyu
    • Journal of Powder Materials
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    • v.14 no.4
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    • pp.238-244
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    • 2007
  • The electrophoretic deposition process of Ni nano-particles in organic suspension was employed for self-repairing of heat exchanger tubes. For this purpose, Ni nano-particles prepared by levitational gas condensation method were dispersed into the solution of ethanol with the addition of dispersant Hypermer KD2. For electrophoretic deposition of Ni nano-particles on the Ni alloy specimen, constant electric fields of 20 and 100 V $cm^{-1}$ were applied to the specimen in Ni-dispersed solution. It was found that as electrophoretic deposition proceeds, the size of the pit or crack remarkably decreased due to the agglomeration of Ni nano-particles at the pit or crack. This strongly suggests that the electrophoretic mobility of the charged particles is larger for the damaged part with a higher current value rather than outer surfaces with a lower current value.

Influence of Magnesium Powder and Heat Treatment on the Superconducting Properties of $MgB_2/Fe$ Wires ($MgB_2/Fe$ 선재의 초전도성에 대한 열처리 조건과 Mg 분말의 영향)

  • Tan, Tan Kai;Kim, N.K.;Kim, Y.I.;Jun, B.H.;Kim, C.J.
    • Progress in Superconductivity
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    • v.9 no.1
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    • pp.1-4
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    • 2007
  • The most common technique to fabricate $MgB_2$ superconducting wire is by powder-in-tube (PIT) technique. Therefore, the starting powder for the processing of $MgB_2$ superconductors is an important factor influencing the superconducting properties and performance of the conductors. In this study, the influence of magnesium precursor powders and annealing temperatures on the transition temperatures ($T_c$) and critical current densities ($J_c$) of $MgB_2/Fe$ wires was investigated. All the $MgB_2/Fe$ wires were fabricated by in situ PIT process. It was found that higher $J_c$ was obtained for $MgB_2$ wires with smaller particle size of magnesium precursor powders. The $J_c$ also increases with decreasing annealing temperatures.

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