• Title/Summary/Keyword: Nano powder synthesis

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THERMAL PLASMA SYNTHESIS OF NANO-SIZED POWDERS

  • Seo, Jun-Ho;Hong, Bong-Guen
    • Nuclear Engineering and Technology
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    • v.44 no.1
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    • pp.9-20
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    • 2012
  • A brief review on the thermal plasma synthesis of nano-sized powders is presented according to the application materials, such as, metals, ceramics, glasses, carbonaceous materials and other functional composites, such as, supported metal catalyst and core-shell structured nano materials. As widely adopted plasma sources available for thermal plasma synthesis of nanosized powders, three kinds of plasma torches, such as transferred and non-transferred DC and RF plasma torches, are introduced with the main features of each torch system. In the basis of the described torch features and the properties of suggested materials, application results including synthesis mechanism are reviewed in this paper.

Synthesis and Characteristics of W-Ni-Fe Nanocomposite Powder by Hydrogen Reduction of Oxides (산화물 수소환원에 의한 W-Ni-Fe 나노복합분말의 합성과 특성)

  • 이창우;윤의식;이재성
    • Journal of Powder Materials
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    • v.8 no.1
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    • pp.49-54
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    • 2001
  • The synthesis and characteristics of W-Ni-Fe nanocomposite powder by hydrogen reduction of ball milled W-Ni-Fe oxide mixture were investigated. The ball milled oxide mixture was prepared by high energy attrition milling of W blue powder, NiO and $Fe_2O_3$ for 1 h. The structure of the oxide mixture was characteristic of nano porous agglomerate composite powder consisting of nanoscale particles and pores which act as effective removal path of water vapor during hydrogen reduction process. The reduction experiment showed that the reduction reaction starts from NiO, followed by $Fe_2O_3$ and finally W oxide. It was also found that during the reduction process rapid alloying of Ni-Fe yielded the formation of $\gamma$-Ni-Fe. After reduction at 80$0^{\circ}C$ for 1 h, the nano-composite powder of W-4.57Ni-2.34Fe comprising W and $\gamma$-Ni-Fe phases was produced, of which grain size was35nm for W and 87 nm for $\gamma$-Ni-Fe, respectively. Sinterability of the W heavy alloy nanopowder showing full density and sound microstructure under the condition of 147$0^{\circ}C$/20 min is thought to be suitable for raw material for powder injection molding of tungsten heavy alloy.

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Microstructure and Synthesis of Nano Palladium Spot Coated Activated Carbon Powders by Hydrothermal Attachment Method (수열흡착법을 이용한 나노팔라듐 점코팅 활성탄 분말의 합성 및 미세조직)

  • Kim, Hyeong Chul;Han, Jae Kil
    • Journal of Powder Materials
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    • v.19 no.6
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    • pp.424-428
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    • 2012
  • Nano Pd spot-coated active carbon powders were synthesized by a hydrothermal-attachment method (HAA) using PVP capped Pd colloid in a high pressure bomb at $250^{\circ}C$, 450 psi, respectively. The PVP capped Pd colloid was synthesized by the precipitation-redispersion method. PVP capped Pd nano particles showed the narrow size distribution and their particle sizes were less than 8nm in diameter. In the case of nano Pd-spot coated active carbon powders, nano-sized Pd particles were adhered in the active carbon powder surface by HAA method. The component of Pd was homogeneously distributed on the active carbon surface.

Microstructure and Synthesis of Ag Spot-coated Cu Nanopowders by Hydrothermal-attachment Method using Ag Colloid (수열흡착법을 이용한 은 점코팅된 구리 나노분말의 합성과 미세조직)

  • Kim, Hyeong-Chul;Han, Jae-Kil
    • Journal of Powder Materials
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    • v.18 no.6
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    • pp.546-551
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    • 2011
  • Ag spot-coated Cu nanopowders were synthesized by a hydrothermal-attachment method (HA) using oleic acid capped Ag hydrosol. Cu nano powders were synthesized by pulsed wire exploding method using 0.4 mm in diameter of Cu wire (purity 99.9%). Synthesized Cu nano powders are seen with comparatively spherical shape having range in 50 nm to 150 nm in diameter. The oleic acid capped Ag hydrosol was synthesized by the precipitation-redispersion method. Oleic acid capped Ag nano particles showed the narrow size distribution and their particle size were less than 20 nm in diameter. In the case of nano Ag-spot coated Cu powders, nanosized Ag particles were adhered in the copper surface by HAA method. The components of C, O and Ag were distributed on the surface of copper powder.

Synthesis and Densification of Nanostructured $Al_2O_3-(Zro_2+3%Mol\;Y_2O_3)$ Bioceramics by High-Frequency Induction Heat Sintering

  • Kim, Sug-Won;Khalil, Khalil Abdel-razek
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.527-528
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    • 2006
  • Nanostructured Alumina - 20 vol% 3YSZ composites powder were synthesized by wet-milling technique. The starting materials were a mixture of Alumina micro-powder and 3YSZ nano-powders. Nano-crystalline grains were obtained after 24 h milling time. The nano-structured powder compacts were then processed to full density at different temperatures by high-frequency induction heat sintering (HFIHS). Effects of temperature on the mechanical and microstructure properties have been studied. $Al_2O_3-3YSZ$ composites with higher mechanical properties and small grain size were successfully developed at relatively low temperatures through this technique.

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A Study on the Nano Alloy Powders Synthesized by Simultaneous Pulsed Wire Evaporation (S-PWE) method II - Synthesis of Ee-Al Nano Alloy Powders (동시 전기 폭발법에 의한 나노 합금 분말 제조에 관한 연구 II - Fe-Al alloy 분말 제조)

  • ;;;O. M.;Yu. A. Kotov
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.105-110
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    • 2004
  • In this study the possibility to obtain a homogeneous mixture and to produce solid solutions and intermetallic compounds of Fe and Al nano particles by simultaneous pulsed wire evaporation (S-PWE) have been investigated. The Fe and Al wires with 0.45 mm in diameter and 35 mm in length were continuously co-fed by a special mechanism to the explosion chamber and simultaneously exploded. The characteristics, e.g., phase composition, particle shape, and specific surface area of Fe-Al nano powders have been analyzed. The synthesized powders, beside for Al and $\alpha$-Fe, contain significant amount of a high-temperature phase of $\gamma$-Fe, Fe Al and traces of other intermetallics. The phase composition of powders could be changed over broad limits by varying initial explosion conditions, e.g. wire distance, input energy, for parallel wires of different metals. The yield of the nano powder is as large as 40 wt % and the powder may include up to 46 wt % FeAl as an intermetallic compound.