• Title/Summary/Keyword: ND2

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The Analysis of Lanthanides Using UV-VIS Spectrometer (UV-VIS 흡광광도법으로 란탄족원소들의 정량분석에 관한 연구)

  • Ji, Bong Il;Kim, Ha Seok;Ha, Yeong Gu
    • Journal of the Korean Chemical Society
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    • v.34 no.6
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    • pp.616-621
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    • 1990
  • The spectrophotometric methods for the determination of Nd, Pr, Sm, Eu, Ho, Er were developed, using the multicomponent method of absorption spectra cointerference. The absorption spectra of individual Nd, Pr, Sm, Eu, Ho, Er, mixture of Sm, Eu, Ho, Er in hydrochloric acid solutions were investigated, and also a band register which includes the molar absorptions for all trivalent Nd, Pr, Sm, Eu, Ho and Er absorption band maxima were measured. The spectrophotometric determination of Nd, Pr, Sm, Eu, Ho and Er were investigated using the analytically significant absorption bands at 444.2, 575.1, 401.7, 394.2, 416.6, and 379.7 nm, respectively.

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Effect of Ca-doping on the superconducting properties of Nd-Ba-Cu-O bulks (Nd-Ba-Cu-O 벌크 초전도체의 초전도 특성에 미치는 Ca첨가제의 영향)

  • 이훈배;위성훈;유상임
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2002.02a
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    • pp.346-350
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    • 2002
  • The effect of Ca-doping on the superconducting properties of Nd-Ba-Cu-O bulk superconductors, fabricated by the oxygen-controlled melt growth process, has been systematically investigated. Various c-axis textured bulk samples were grown using precursors with the nominal compositions of N $d_{1.8-x}$C $a_{x}$B $a_{2.4}$C $u_{3.4}$ $O_{y}$ (x = 0.00, 0.02, 0.05, 0.10, 0.15) in a reduced oxygen atmosphere of 1% $O_2$ in Ar. Magnetization measurements revealed that the critical temperatures( $T_{c}$) were almost linearly depressed from 95K to 86K with increasing the Ca dopant from x = 0.0 to 0.15, respectively, and thus critical current densities( $J_{c}$) at 77K and for H//c-axis of specimens were gradually degraded with increasing x. Compositional analyses revealed that although the amounts of the Ca dopant both in NdB $a_2$C $u_3$ $O_{y}$(Nd123) and N $d_4$B $a_2$C $u_2$ $O_{10}$(Nd422) were increased with increasing x, only less than half of the initial Ca compositions were detected in melt-grown Ca-doped Nd-Ba-Cu-O bulk crystals. The supression of $T_{c}$ is attributed to an increased Nd substitution for the Ba site in the Nd123 superconducting matrix with increasing the amount of the Ca dopant.t.opant.t.t.t.t.t.

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Effect of Swine Liquid Manure and Phosphorus Application on Chemical Properties and Microbial Population of Italian (제주화산회토지역에서 돈분액비와 인산시용이 이탈리안 라이그라스 재배 토양의 화학적 특성 및 미생물상에 미치는 영향)

  • 김문철;현해남;최대진;문봉춘;고용구;강태숙
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.21 no.4
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    • pp.181-190
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    • 2001
  • This study was conducted to investigate the effect of swine liquid manure(SLM) and phosphorus fertilizer from September, 1998 to July, 1999 on the soil fertility on Italian ryegrass field, Cheju volcanic ash soil. pH(lst investigated), Mg (2nd investigated) and Cu content (2nd investigated) on soil grown by Italian ryegrass were significantly increased by an increase of fertilizer P(P

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Nd1+XBa2-XCu3O7-δ Bulk Superconductor by Zone-melt Process

  • Soh, Dea-Wha;Guo, Fan-Zhan
    • Transactions on Electrical and Electronic Materials
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    • v.3 no.3
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    • pp.21-24
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    • 2002
  • Two kinds of $Nd_{1+X}Ba_{2-X}Cu_3O_{7-{\delta}}$, the sintering samples and zone melting samples, were heat-treated under pure Ar at 950$^{circ}C$. The substitution of Nd ion for Ba ion in the $Nd_{1+X}Ba_{2-X}Cu_3O_{7-{\delta}}$ before and after the heat treatment was investigated by XRD. In order to confirm the effects of the heat treatment, the Tc and Jc of samples with/without the heat treatment under Ar were comparatively studied. $Nd_{1+X}Ba_{2-X}Cu_3O_{7-{\delta}}$ samples were oxygenated under pure oxygen at $300^{circ}C$. From the XRD pattern it was found that the sample with x<0.4 was transferred from tetragonal phase to orthorhombic phase after the oxygenation, while the sample with x>0.4 did not show the phase transition even after a long time oxygenation. Therefore, the low oxygen partial pressure (Ar+1 % O$_2$) was used for the ambient atmosphere of the zone-melting samples, which could reduce the melting temperature and depress the substitution of Nd for Ba. After the improvement in the zone-melting process, the Jc value was increased to 2 x $10^4$A/$cm^2$ (0 T, 78 K). The particle orientation and the structure of zone-melted NdBaCuO were studied by the XRD and SEM analysis.

Consideration of Cause of Recent Severe Outbreaks of Newcastle Disease in Korea and a Brief Review of Virological Differences, Serological Diagnosis and Administration of a Vaccine (최근의 닭 뉴캣슬병 만연에 따른 원인과 바이러스의 성상, 진단 및 백신 운용에 관한 고찰)

  • 김재흥;송창선
    • Korean Journal of Poultry Science
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    • v.19 no.2
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    • pp.65-76
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    • 1992
  • Since the first outbreaks of Newcastle disease ( ND) in Korea was reported in 1927, the disease has been a major problem in Korean poultry industry. Several attempts related ND prevention and controls have been tried and significantly reduced the ND outbreaks. However, recently frequencies of ND outbreaks have been increased throughout the country since 1988. Many assumptions such as variances of ND virus pathogenicity, decreased efficacy of ND vaccine, incorrect vaccination program etc, has been issued and discussed. Therefore, to clearly understand this recent situation of ND outbreaks in Korea, we reviewed all available past informations related with ND outbreaks in Korea and compared the virulence of recently isolated ND viruses with that of a reference one. Also, we discussed about some problems related with serological diagnosis. administration methods of vaccine and vaccination program.

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A STUDY ON THE COMPARISONS BETWEEN DENTAL CALCIFICATION AND SKELETAL MATURITY (치아 석회화과정과 골성숙단계의 상호연관성에 관한 연구)

  • Cha, Dae-Sik;Cha, Kyung-Suk
    • The korean journal of orthodontics
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    • v.24 no.4 s.47
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    • pp.841-849
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    • 1994
  • This study was conducted on 342 patients(male 157, female 185)aged 8 to 15 years old, who visited Dankook University Dental Hospital. Pre-orthodontic treatment orthopantomograms were used to assess the dental calcification stages of mandibular 3rd molar, 2nd molar, 2nd premolar and 1st premolar by 8 stages.(by Demirjian) Hand-wrist radiogrms were used to evaluate the skeletal maturity in 11 stages.(by Fishman) Following results were obtained after investigating the correlationship between dental calcification and skeletal maturity 1. Chronologic age showed high correlation to dental calcification and skeletal maturity. 2. Dental calcification and skeletal maturity showed high correlation and no statistical difference was observed between male and female. 3. SMI stages 1 to 4 showed high statiscal significance to mandibular 2nd molar, 2nd premolar and 1st premolar. SMI stages 5 to 8 showed high stastical significance to mandibular 2nd molar, 2nd premolar. SMI stages 9 to 11 showed high statistical significance to mandibular 3rd molar.

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A Scanning Electron Microscopic Study on the Effect of Nd:YAG Laser Irradiation on the Sclerotic Dentin (Nd:YAG레이저조사가 경화상아질에 미치는 영향에 관한 주사전자현미경적 연구)

  • Kim, Moon-Hyeon;Shin, Keum-Back
    • Journal of Oral Medicine and Pain
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    • v.24 no.4
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    • pp.397-410
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    • 1999
  • In order to obtain the basic data concerning the optimal parameters in using Nd:YAG laser as a therapeutic modality to dentinal hypersensitivity, the author prepared 3 sections of sound dentin and 10 sections of sclerotic dentin with thickness of $0.5mm{\pm}0.1mm$ from human extracted teeth of anteriors and premolars, and applied the laser energy from a fiberoptic delivered, free running, pulsed Nd:YAG laser (wavelength 1064nm, pulse duration $120{\mu}sec$, fiber diameter $320{\mu}m$) to surfaces of sound and sclerotic dentin sections for 1 second with contact/unidirectional moving mode of the fiber under speed of 3mm~4mm/sec and parameters of 0.5W/10Hz, 1.0W/10Hz, 1.5W/10Hz, 2.0W/10Hz: $62J/cm^2$, $124J/cm^2$, $187J/cm^2$, $249J/cm^2$. The author comparatively evaluated the characteristics of ultrastructural changes on surfaces of sound and sclerotic dentin sections irradiated by the pulsed Nd:YAG laser using the scanning electron microscopy. A fairly ill-defined bordered surface of partially closed and melted dentinal tubules can be seen on the scanning electron microscopic feature of the sound dentin surface irradiated by the pulsed Nd:YAG laser with energy density of $62J/cm^2$. The physical modification of sound dentin surface extensively occurred depended on the increase of energy density from $62J/cm^2$ to $124J/cm^2$, $187J/cm^2$, $249J/cm^2$. While, a fairly well-defined bordered surface of partially closed and melted dentinal tubules with thickened peritubular dentin can be seen on the scanning electron microscopic feature of the sclerotic dentin surface irradiated by the pulsed Nd:YAG laser with energy density of $62J/cm^2$. The physical modification of sclerotic dentin surface of a fairly rough, shallow depression with many cracks, thickened peritubular dentin and structureless dentinal tubules extensively occurred depended on the increase of energy density from $62J/cm^2$ to $124J/cm^2$, $187J/cm^2$, $249J/cm^2$ compared to those of sound dentin surface irradiated by the pulsed Nd:YAG laser under the same parameters. Therefore, it is recommended that the pulsed Nd:YAG laser as a therapeutic modality to dentinal hypersensitivity should be applied with the less energy density than $62J/cm^2$ on the sound dentin surface, and its energy density on the partially sclerotic dentin surface should be lower than that on the sound dentin surface to preserve tooth from unnecessary excessive structural destruction.

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Islanding Detection Method for Inverter-Based Distributed Generation through Injection of Second Order Harmonic Current

  • Lee, Yoon-Seok;Yang, Won-Mo;Han, Byung-Moon
    • Journal of Power Electronics
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    • v.18 no.5
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    • pp.1513-1522
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    • 2018
  • This paper proposes a new islanding detection method for inverter-based distributed generators by continuously injecting a negligible amount of 2nd order harmonic current. The proposed method adopts a proportional resonant (PR) controller for the output current control of the inverter, and a PR filter to extract the 2nd order harmonic voltage at the point of common coupling (PCC). The islanding state can be detected by measuring the magnitude ratio of the 2nd order harmonic voltage to the fundamental voltage at the PCC by injecting a 2nd order harmonic current with a 0.8% magnitude. The proposed method provides accurate and fast detection under grid voltage unbalance and load unbalance. The operation of the proposed method has been verified through simulations and experiments with a 5kW hardware set-up, considering the islanding test circuit suggested in UL1741.