• 제목/요약/키워드: Morphologies

검색결과 1,146건 처리시간 0.025초

철도차량 부쉬용 방진 천연고무의 카본블랙 강화제에 의한 피로수명과 파단 모폴로지 변화 연구 (A study on the change of the fatigue life and the fracture morphology due to the carbon black on the Natural rubber for vibration-proof)

  • 김재훈;허현무
    • 한국철도학회논문집
    • /
    • 제8권1호
    • /
    • pp.21-26
    • /
    • 2005
  • The effects of carbon black on the fatigue lift and the fracture morphology and the carbon black dispersion of the carbon-black filled natural rubbers, for the vibration-proof, were investigated. Different kinds of carbon blacks resulted in different fatigue lift and fracture morphologies, which are classified by micro-scale and macro-scale fracture morphologies. These results be related to the size distribution of carbon black particles, the development of the carbon black agglomerate and the combine forces between the carbon black and the natural rubber.

Nanoscale Morphology of Bis(1-anthraquinoxy)glycols

  • Kwon, Soon-Sik;Liang, Hui;Kim, Jong-Pil;Lee, Young-A;Jung, Ok-Sang
    • Bulletin of the Korean Chemical Society
    • /
    • 제28권11호
    • /
    • pp.2065-2068
    • /
    • 2007
  • The nanoscale morphologies on a series of new anthraquinone substitutes have been carried out. Among the substitutes, only bis[2-(1-anthraquinonoxy)-ethyl]ether in a mixture of dichloromethane/acetone (1/1) slowly forms uniform nanowires with 80-120 nm diameters. The same compound in a mixture of dichloromethane/tetrahydrofuran (1/1) slowly produces uniform nanobelts with 400-600 nm widths. Thus, both the spacer lengths and the solvent effects of the compounds are important factors for the formation of nanoscale morphologies. The nano patterns seem to be formed by the π-π interactions between the anthraquinone moieties.

Effect of Calcination Temperature on the Structure and Electrochemical Performance of LiMn1.5Ni0.5O4 Cathode Materials

  • Ju, Seo Hee;Kim, Dong-Won
    • Bulletin of the Korean Chemical Society
    • /
    • 제34권1호
    • /
    • pp.59-62
    • /
    • 2013
  • Spinel $LiMn_{1.5}Ni_{0.5}O_4$ cathode powders with different morphologies were synthesized by a co-precipitation method using oxalic acid. The calcination temperature affected the morphologies, crystalline structure and electrochemical properties of the $LiMn_{1.5}Ni_{0.5}O_4$ powders. The $LiMn_{1.5}Ni_{0.5}O_4$ powders obtained at a calcination temperature of $850^{\circ}C$ exhibited the highest initial discharge capacity with good capacity retention and high rate capability.

Hot Filament Chemical Vapor Deposition of Crystalline Boron Films

  • Soto, Gerardo
    • 한국세라믹학회지
    • /
    • 제56권3호
    • /
    • pp.269-276
    • /
    • 2019
  • This article reports on the conditions required for the growth of crystalline boron films on silicon substrates by hot filament chemical vapor deposition method. The reactive gas was 3% diborane diluted in hydrogen. The films were characterized by optical, electronic, and atomic force microscopies; x-ray diffraction; and energy dispersive, electron energy loss, Raman, x-ray photoelectron, and Auger spectroscopies. The parameters that affect the morphologies of the films have been investigated. It was concluded that faceted crystals are produced at low B2H6 flows and working pressures below 200 mT. α-boron is produced between 530 and 600℃. Deposition outside this range produces thin films with a wide variety of morphologies. This result indicates that the films crystallize through a process called "abnormal or discontinuous grain growth." It is assumed that this is due to the anisotropic surfaces of boron allotropes.

Shannon Entropy as an Indicator of the Spatial Resolutions of the Morphologies of the Mode Patterns in an Optical Resonator

  • Park, Kyu-Won;Kim, Jinuk;Moon, Songky
    • Current Optics and Photonics
    • /
    • 제5권1호
    • /
    • pp.16-22
    • /
    • 2021
  • We present the Shannon entropy as an indicator of the spatial resolutions of the morphologies of the resonance mode patterns in an optical resonator. We obtain each optimized number of mesh points, one of minimum size and the other of maximum one. The optimized mesh-point number of minimum size is determined by the identifiable quantum number through a chi-squared test, whereas the saturation of the difference between Shannon entropies corresponds to the other mesh-point number of maximum size. We also show that the optimized minimum mesh-point increases as the (real) wave number increases and approximates the proportionality constant between them.

Characteristics in Size Distributions and Morphologies of Wear Particles Depending on Types of Abrasion Testers

  • Eunji Chae;Seong Ryong Yang;Sung-Seen Choi
    • Elastomers and Composites
    • /
    • 제58권2호
    • /
    • pp.87-94
    • /
    • 2023
  • Abrasion tests of an SBR compound were conducted using four different types of abrasion testers (cut and chip, Lambourn, DIN, and LAT100). The abrasion test results were analyzed in terms of size distributions and morphologies of the wear particles. Most wear particles were larger than 1000 ㎛. The wear particle size distributions tended to decrease as the particle size decreased. Except for the Lambourn abrasion test, the wear particles smaller than 212 ㎛ were rarely generated by the other three abrasion tests, implying that small wear particles were produced through friction by introducing talc powder. Shapes of the wear particles varied depending on the abrasion testers. The wear particles generated from the Lambourn abrasion tester had stick-like shapes. The cut and chip abrasion test showed a clear abrasion pattern, but the DIN abrasion test did not show any specific abrasion pattern. The Lambourn and LAT100 abrasion tests showed irregular abrasion patterns.

Sn-Ag 범프의 조성과 표면 형상에 영향을 미치는 도금 인자들에 관한 연구 (The Effect of Electroplating Parameters on the Compositions and Morphologies of Sn-Ag Bumps)

  • 김종연;유진;배진수;이재호
    • 마이크로전자및패키징학회지
    • /
    • 제10권4호
    • /
    • pp.73-79
    • /
    • 2003
  • Sn-Ag 전해도금시 도금욕의 Ag 이온의 농도, 전류밀도, 펄스 주기, 첨가제등의 인자들이 솔더의 조성과 표면형상에 미치는 영향에 관하여 연구하였다. Ag 이온의 농도와 시편에 가해지는 전류밀도를 변화시킴으로써 Sn-Ag 솔더내의 Ag 조성을 조절하는 것이 가능하였고 또한 전류밀도를 증가시키면 솔더의 미세조직의 크기가 감소되는것을 관찰하였다. 펄스 인가 주기와 첨가제의 양등을 변화시키면 솔더내 Ag의 조성이 달라지고 솔더의 표면 거칠기가 감소하면서 표면 형상이 변화됨을 확인하였다. 이러한 과정을 통하여 30 $\mu\textrm{m}$의 미세피치와 15$\mu\textrm{m}$의 범프 높이를 가지는 공정 Sn-Ag 솔더 범프를 형성하였다. 도금된 솔더의 조성은 EDS와 WDS 분석을 통하여 확인하였고 표면형상은 SEM과 3D surface analyzer를 사용하여 분석하였다.

  • PDF