• Title/Summary/Keyword: Monodispersed silica cap-ZnO powders

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Preparation of Monodispersed $SiO_2/ZnO$ Composite Fine Powders by Sol-Gel Method (졸-겔법엔 의한 단분산 $SiO_2/ZnO$ 복합미립자의 졔조)

  • Lee, Chang-Woo;Shim, Won;Hahm, Yeong-Min;Hur, Yun-Haeng
    • Journal of environmental and Sanitary engineering
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    • v.13 no.3
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    • pp.58-65
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    • 1998
  • Monodispersed $SiO_2/ZnO$ composite fine powders were prepared by Sol-Gel processing and their surface electrical and UV absorbance properties were investigated. Pseudomorph ZnO fine powders were microcapsuled by $SiO_2/ZnO$ sol fabricated using TEOS[tetraethylorthosilicate, purity 98% and ethanol as a solvent with $NH_3$ catalyst. The effects of experimental parameters such as molar ratio of starting materials on the final particle size and shape of $SiO_2/ZnO$ composite fine powder were discussed. As a result, we could controlled the size of monodispersed $SiO_2/ZnO$ composite fine powders without agglomeration, as well as the good dispersibility in aquous solution. The prepared powders were observed to have the mean particle sizes of $0.26-0.78{\mu}m$ with standard deviations of $0.020-0.063{\mu}m$.

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