• Title/Summary/Keyword: Modulus Measurement

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Measurement of Tensile Properties for Thin Aluminium Film by Using White Light Interferometer (백색광간섭계를 이용한 알루미늄 박막의 인장 물성 측정)

  • Kim, Sang-Kyo;Oh, Chung-Seog;Lee, Hak-Joo
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.5
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    • pp.471-478
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    • 2010
  • Thin films play an important role in many technological applications including microelectronic devices, magnetic storage media, MEMS and surface coatings. It is well known that a thin film's material properties can be very different from the corresponding bulk properties and thus there has been a strong need for the development of a reliable test method to measure the mechanical properties of a thin film. We have developed an alternative and convenient test method to overcome the limitations of previous membrane deflection experiment and uniaxial tensile test by adopting a white light interferometer having sub-nanometer out-of-plane displacement resolution. The freestanding aluminium specimens are tested to verity the effectiveness of the test method developed and get the tensile properties. The specimens are 0.5 rum wide, $1{\mu}m$ thick and fabricated through MEMS processes including sputtering. 1 to 5 specimens are fabricated on Si dies. The membrane deflection experiments are carried out by using a homemade tester consisted of a motor-driven loading tip, a load cell, and 6 DOF alignment stages. The test system is compact enough to set it up beneath a commercial white light interferometric microscope. The white light fringes are utilized to align a specimen with the tester. The Young's modulus and yield point stress of the aluminium film are 62 GPa and 247 MPa, respectively.

Data Reduction and Analysis of the Resonant Column Testing Based on the Equation of Motion (운동방정식에 기초한 공진주 실험의 자료분석 및 해석)

  • 조성호;강태호
    • Journal of the Korean Geotechnical Society
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    • v.19 no.4
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    • pp.133-144
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    • 2003
  • The resonant column testing is a laboratory testing method to determine the shear modulus and material damping factor of soils. The method has been widely used for many applications and its importance has increased. Since the first use of the testing method in 1960's, the low-technology electronic devices fir testing and data acquisition have limited the measurement only to the amplitude of the linear spectrum. The limitations of the testing method are also attributed to the assumption of linear-elastic material in the theory of the resonant column testing and also to the incomplete understanding of the dynamic behaviour of the resonant column testing device. Recently, Joh et al. proposed a theory to overcome the limitations of the resonant column testing by deriving the equation of motion and providing its solution for the resonant column testing device. This study proposed the improved data reduction and analysis method for the resonant column testing, thanks to the advanced data acquisition system and the new theoretical solution for the resonant column testing system. For the verification of the proposed data reduction and analysis method, the numerical simulation of the resonant column testing was performed by the finite element analysis. Also, a series of resonant column testing were performed fir Joomunjin sand, which verified the feasibility of the proposed method and revealed the limitations of the conventional data reduction and analysis method.

Hybrid Analysis of Displacement Behavior and Numerical Simulation on Tunnel Design (터널 변위 거동 및 수치 모의실험의 결합 해석)

  • Jeong, Yun-Young;Han, Heui-Soo;Lee, Jae-Ho
    • The Journal of Engineering Geology
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    • v.20 no.1
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    • pp.47-60
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    • 2010
  • This study is focused on the analysis of tunnel behavior to estimate the stability on tunnel design. An estimation method was proposed as a hybrid consideration, which contains the displacement analysis by 3D numerical simulation, the maximum displacement obtained after field measurement, and an assessment of tunnel stability using a deformation analysis proposed by Sakurai(1988, 1997). The points of case study by Sakurai(1988, 1997) were replotted considering his analysis. From the new analysis of the tunnel case study, the trend line for analyzed points is analogized, which curve is divided into stable, unstable and failure zone. To evaluate the estimation method, a special shape of railway tunnel was selected, which are the Inchon international airport rail way connected to subway line 9 in Gimpo, Korea. The point s of upper and below track on the Inchon international airport rail way were satisfied to the stability of tunnel after reinforcing. Also the points shows the higher apparent Young's modulus, which resulted from improvement on shear strength by the micro silica grouting and the supporting of umbrella method. Therefore, if new analysis used, proper tunnel reinforcing method could be selected according to tunnel strain and geological property.

Self-Sensing and Interfacial Property of Carbon Nanofiber/Epoxy Composites with Different Aspect Ratios (형상비가 다른 탄소나노섬유/에폭시 복합재료의 자체 감지능 및 계면특성)

  • Jang, Jung-Hoon;Kim, Pyung-Gee;Kim, Sung-Ju;Wang, Zuo-Jia;Park, Joung-Man;Yoon, Dong-Jin
    • Journal of Adhesion and Interface
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    • v.9 no.1
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    • pp.3-8
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    • 2008
  • Self-sensing was evaluated for carbon nanofiber (CNF)/epoxy composites with two different aspect ratios via electro-micromechanical technique and wettability test. Volumetric electrical resistance was measured to evaluate the comparative dispersion degree indirectly and it decreased due to the increase of electric contacts with increasing CNF concentration. The dispersion degree was evaluated indirectly by calculating coefficient of variation (COV) of volumetric electrical resistance. The CNF type A with a high aspect ratio showed better self-sensing than the case of CNF type B with a short aspect ratio. The CNF type B/epoxy composite showed little self-sensing at a concentration higher than 2 vol% probably due to poor dispersion. The apparent modulus of CNF type B was higher than that of CNF type A due to the orientation effect and the high surface area. The thermodynamic work of adhesion was consistent with the result of apparent modulus.

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Estimation of Deformation Modulus of Basaltic Rock Masses in Northeastern and Northwestern Jeju Island (제주도 북동부 및 북서부 현무암반의 변형계수 추정)

  • Yang, Soon-Bo;Boo, Sang-Pil
    • Journal of the Korean Geotechnical Society
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    • v.35 no.1
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    • pp.5-15
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    • 2019
  • In this study, the in situ deformation moduli, which were measured by borehole loading tests at basaltic rock masses located in the northeastern onshore and offshore and the northwestern onshore of Jeju Island, were examined in relation to RQD and RMR. The measured deformation moduli were also compared with the estimated deformation moduli from conventional empirical formulas using RQD and RMR. In addition, the measured deformation moduli were analyzed with respect to both the velocity ratio ($V_P/V_S$) and dynamic Poisson's ratio, which were obtained from the elastic wave velocities measured by velocity logging tests. As results, with only RQD, it was inappropriate to evaluate the quality of the Jeju island basaltic rock masses, which are characterized by vesicular structures, to select a measurement method of in situ deformation moduli, and to estimate the deformation moduli. On the other hand, it was desirable to evaluate the quality of the Jeju Island basaltic rock masses, and to estimate the deformation moduli by using RMR. The conventional empirical formulas using RMR overestimated the deformation moduli of the Jeju Island basaltic rock masses. There was qualitative consistency in the relation between velocity ratio and deformation moduli. To estimate appropriately the deformation moduli of the Jeju Island basaltic rock masses, empirical formulas were proposed as the function of RMR and velocity ratio, respectively.

Analysis of Perceived Weight According to Temperature and Weight of Stainless Steel Cup (스테인리스 컵의 온도와 무게에 따른 무게감 분석)

  • Ryu, Taebeum;Park, Jaehyun
    • Science of Emotion and Sensibility
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    • v.25 no.2
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    • pp.23-30
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    • 2022
  • The weight of an object is an important research topic in terms of sense, and objects have size-weight, color-weight, and material-weight illusions due to the influence of size, color, and material and the weight of the object. Although temperature is a very important environmental factor in our daily life, there is a dearth of studies on how the temperature of an object affects its perceived weight. This study analyzed the effect of an object's temperature on the perceived weight. A stainless steel cup, in which weight and temperature are easily adjustable, was selected as a perceived weight measurement object; 5 temperature levels (0, 9, 20, 40, 70 degrees) and 2 weight levels (250, 400 g) were set. A total of 40 healthy men and women in their 20s participated in the experiment. The weight of the given cup compared to the reference cup was evaluated according to the modulus method. The study revealed that both temperature and weight significantly affected the perceived weight. The effect of temperature on the weight was different depending on the weight of the object. When the cup's weight was small (250 g), the temperature of the cup did not affect the weight. However, the perceived weight of a large cup (400 g) increased at a low temperature. This result suggests that the effect of temperature on the weight of an object depends on the size-weight illusion.

Self-Sensing and Interfacial Evaluation of Ni Nanowire/Polymer Composites Using Electro-Macromechanical Technique (전기적 미세역학적 시험법을 이용한 Ni nanowire강화 고분자 복합재료의 자체 감지능 및 계면 물성평가)

  • Kim, Sung-Ju;Yoon, Dong-Jin;Hansen George;DeVries K. Lawrence;Park, Joung-Man
    • Composites Research
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    • v.19 no.5
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    • pp.20-27
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    • 2006
  • Self-sensing and interfacial evaluation of Ni nanowire/polymer composites were investigated using electro-macromechanical technique, which can be used fur a feasible sensing measurement on tensile and compressive loading/consequent unloading, temperature, and humidity. Mechanical properties of Ni nanowire with different aspect ratio and adding contents in either epoxy or silicone composites were measured indirectly using electro-pullout test under uniform and non-uniform cyclic loadings. Comparing apparent modulus with the conventional mechanical tensile modulus of Ni nanowire/epoxy composites, the trends were consistent with each other. Ni nanowire/epoxy composites showed the sensing response on humidity and temperature. Self-sensing on applied tensile and compressive loading/unloading was also responded for Ni nanowire/silicone composites via electrical contact resistivity showing the opposite trend between tension and compression. It can be due to the different electrically-interconnecting mechanisms of dispersed Ni nanowires embedded in silicone matrix.

Material Properties Depending on the Maximum Aggregate Size and Fineness Modulus for Concrete Repair Materials (콘크리트 단면복구용 보수재료의 굵은 골재 최대치수 및 조립률에 따른 재료적 특성)

  • Sun-Mok Lee;Byung-Je Lee;Yun-Yong Kim
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.27 no.6
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    • pp.62-69
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    • 2023
  • Re-damage is frequently occurring for various reasons, including material factors, external factors, and factors caused by poor construction in concrete cross-section restoration work, so it is necessary to identify the cause and improve it. Cement-based materials are the most commonly used maintenance materials for concrete structures, and in particular, additional cross-sectional restoration work may be carried out due to re-damage such as cracks and excitement due to dry contraction of the repair material. In this study, a basic study was conducted to identify the characteristics of concrete while diversifying the maximum dimensions and assembly rate of thick aggregates to examine the effects of using thick aggregates in repair materials. As a result, the slump of concrete increased as the maximum size of thick aggregates increased, and the amount of air content was measured 1.88 to 2.35 times higher in the mixing using aggregates with a maximum aggregate size of 5 mm or more compared to the mixing group with a maximum aggregate size of 10 mm or more. It was found that compressive strength was greatly affected by the performance rate of thick aggregates. The compressive strength was measured the highest in the mixture using thick aggregates with the highest performance rate of 20 mm, and the compressive strength of the mixture with the lowest performance rate was more than 45%. As a result of the dry shrinkage measurement, the dry shrinkage was the lowest as the performance rate of the thick aggregate increased according to the change in the maximum dimensions and assembly rate of the thick aggregate, and the lowest performance rate was the largest in the mix. Through this study, it was confirmed that adjusting the particle size by diversifying the maximum dimensions and assembly rate of thick aggregates used in concrete structure repair materials can improve strength and workability and reduce dry shrinkage.

Electronic state calculation of ceramics by $DV-X\;{\alpha}$ cluster method

  • Adachi, Hirohiko
    • Proceedings of the Materials Research Society of Korea Conference
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    • 1994.11a
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    • pp.1-1
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    • 1994
  • ;The electronic state calculations for various types of ceramic materials have beell performed by the use of $DV-X\;{\alpha}$ cluster method. The molecular orbital levels and wave functions for model clusters have been computed to study the electronic properties ami chemical bonding of the ceramics. For ${\beta}-sialon(Si_{6-z}Al_zO_zN_{8-z})$ which is a high temperature structural material based on ${\beta}-Si_3N_4$, we have made model cluster calculations to estimate the strength of chemical bonding between atoms by the Mulliken population analysis. It is found that the covalent bonding between Si and N atoms is very strong in pure ${\beta}-Si_3N_4$, but the covalency around solute atom is considerably weakened when Si atom is substituted by AI. This tendency is enhanced by an additional substitution of oxygen atom for N. The result calculated can well explain the experimental data of changes in mechanical properties such as the reductions of Young's modulus and Vickers hardness with increment of z-value in ${\beta}-sialon$. Various model clusters for transition metal oxides which show many interesting physical and chemical properties have also been calculated. High-valent perovskite-type iron oxides EMFe0_3E(M=Ca and Sr) possess very interesting magnetic and chemical properties. In these oxides, iron exists as $Fe^{4+}$ state, but the experimental measurement of Mossba~er effect suggests that disproportionation $2Fe^{4+}=Fe^{3+}+Fe^{5+}$ takes place for $CaFe0_3$ at low temperatures. The model cluster calculations for these compounds indicated the existence of considerably strong covalent bonding of Fe-O. The calculations of hyperfine interaction at iron neucleus show very good agreement with the experimental Mossbauer measurements. The result calculated also implies that the disproportionation reaction is strongly possible by assuming the quenching of breathing phonon mode at low temperatures.tures.

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Effect of Sintering Temperature and Sb/Bi Ratio on Microstructure and Grain Boundary Properties of ZnO-Bi2O3-Sb2O3-Co3O4 Varistor (소결온도와 Sb/Bi 비가 ZnO-Bi2O3-Sb2O3-Co3O4 바리스터의 미세구조와 입계 특성에 미치는 영향)

  • Hong, Youn-Woo;Shin, Hyo-Soon;Yeo, Dong-Hun;Kim, Jin-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.12
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    • pp.969-976
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    • 2011
  • In this study we aims to evaluate the effects of 1/3 mol% $Co_3O_4$ addition on the reaction, microstructure development, resultant electrical properties, and especially the bulk trap and grain boundary properties of $ZnO-Bi_2O_3-Sb_2O_3$ (Sb/Bi=2.0, 1.0, and 0.5) system (ZBS). The samples were prepared by conventional ceramic process, and characterized by XRD, density, SEM, I-V, impedance and modulus spectroscopy (IS & MS) measurement. In addition of $Co_3O_4$ in $ZnO-Bi_2O_3-Sb_2O_3$ (ZBSCo), the phase development, density, and microstructure were controlled by Sb/Bi ratio. Pyrochlore on cooling was reproduced in all systems. The more homogeneous microstructure was obtained in ZBSCo (Sb/Bi=1.0) system. In ZBSCo, the varistor characteristics were improved drastically (non-linear coefficient ${\alpha}$=23~50) compared to ZBS. Doping of $Co_3O_4$ to ZBS seemed to form $V^{\cdot}_o$(0.33 eV) as dominant defect. From IS & MS, especially the grain boundary of Sb/Bi=0.5 system is composed of electrically single barrier (0.93 eV) and somewhat sensitive to ambient oxygen with temperature.