• The Korean Journal of Nuclear Medicine
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• v.30 no.3
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• pp.361-366
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• 1996

This study was to determine the effect of $Al^{3+}$ in $^{99m}Tc$ eluate from $^{99}Mo-^{99m}Tc$ generator on labeling efficiency and biodistribution of $^{99m}Tc$-MDP. The chromatographic analysis of $^{99m}Tc$-MDP preparations containing $Al^{3+}(0-62.5{\mu}g/ml)$ showed decreased labeling efficiency $^{99m}Tc$ pertechnetate and hydrolyzed reduced $^{99m}Tc$ fraction increased with increasing concentrations of aluminum. However, the chromatography system could not discern between hydrolyzed reduced $^{99m}Tc$ and $^{99m}Tc$ labeled colloid. $^{99m}Tc$-MDP preparations containing aluminum were relatively stable. Chromatographic analysis also confirmed that no significant differences were observed in the radiochemical purity of the filtered and the unfiltered $^{99m}Tc$-MDP preparations containing aluminum by $0.22{\mu}m$ syringe filter. In biodistribution data of ICR-mice, blood and heart uptake were increasing with increasing concentrations of aluminum, because of decreasing labeling efficiency of $^{99m}Tc$-MDP and increasing of $^{99m}Tc$ pertechnetate. However, liver and bone uptake were not significantly increased. In rat images no difference were observed at $5{\mu}g/ml\;Al^{3+}$ compare with at $0{\mu}g/ml\;Al^{3+}$, but at $10{\mu}g/ml\;Al^{3+}$ lumbar uptake was increased. As a practical conclusion, a concentration below $10{\mu}g/ml\;Al^{3+}$($10{\mu}g/ml\;Al^{3+}$ is the maximum allowed in pertechnetate eluate from $^{99}Mo-^{99m}Tc$ generator by USP.) in $^{99m}Tc$-MDP radiopharmaceutical result in low labeling efficiency. Radiochemical purity 90% of $^{99m}Tc$-MDP is the minimum allowed by USP. Therefore, when soft tissue uptake is observed in $^{99m}Tc$-MDP bone scan and labeling efficiency is above 90%, we can expect that $Al^{3+}$ in pertechnetated eluate is not the cause of soft tissue uptake.

• Journal of Korean Society for Atmospheric Environment
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• v.9 no.2
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• pp.140-146
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• 1993

CoMo, NiMo/ZSM-5 catalysts were prepared at Si/Al ratios of 100, 200 and characterized by TGA, XRD and SEM. Simultaneous hydrocracking of n-heptane and hydrodesulfurization of DBT were studied over these catalysts at the ranges of temparatures between 400$^\circ$C and 500$^\circ$C, pressure of 30 $\times 10^5$ Pa and contact time of 0.02g cat. hr/ml feed in a fixed bed flow reactor. It was shown that the hydrocracking activity of n-heptane increased in the order of NM 100, CM 100, NM 200 and CM 200 catalysts. It was also shown that the Hydrodesulfurization activity of DBT increased in the order of CM 200, NM 200, CM 100 and NM 100 catalysts and these results were thought to be that the increase of acidity of catalysts might increase hydrocracking activity of these catalysts but deactive those simultaneously. In this study it was shown that CM 100 and NM 200 were active catalysts in simultaneous hydrodesulfurization of DBT and hydrocracking of n-heptane reactions.

• Economic and Environmental Geology
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• v.49 no.2
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• pp.89-95
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• 2016

Mo isotope, one of highly redox-sensitive isotopes, has been shown to be useful tracers of geochemical processes. Many studies for Mo isotope have documented with the help of recently developed analysis tools, but it has not yet been documented in the Korea. In this study, we introduce two-stage column separation method of Mo using column tube (BioRad PolyPrep(R) column, 10 ml) and anion exchange resin (BioRad Resin AG(R) 1-X8, 200-400 mesh). Mo isotope ratios in the solid SRMs (BHVO-2, SDO-1, PACS-2) and liquid SRM (IAPSO) were measured on MC-ICP-MS (Multi-collector Inductively Coupled Plasma Mass Spectrometer) and then compared with reference Mo isotope ratios. Mo isotope ratios in our study overlap with reference Mo isotope ratios within analytical error.

• Applied Chemistry for Engineering
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• v.7 no.6
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• pp.1174-1180
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• 1996

Potassium hexatitanate whisker was effectively prepared with calcination and flux method by using industrial $TiO_2$, $K_2CO_3$ and $K_2MoO_4$ as the starting materials. When it was synthesized by the calcination method, the filtrate after boiling water treatment was required a neutralization, as the pH of filtrate was higher than 9. Because K component was very small, recovery of K component was not economically suitable. In case of flux method, flux was recovered 96.1% of Mo component and 91.8% of K component at $K_2MoO_4$, for 10th treatment in boiling water of 100ml to 10g.

• Journal of KIISE:Computing Practices and Letters
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• v.8 no.1
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• pp.62-70
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• 2002

The purpose of this paper in that users can use mobile device applications more easily and efficiently through MoDAM (Mobile Device Application Management) system. MoDAM automates the process of web retrieval for obtaining mobile device applications and the process of installing or updating it on mobile devices and then supply users with these automated services in a step form by combining two separated processes. We implement a web agent conforming to OSD (Open Software Description) specification for automating software retrieval and downloading and also a mobile device based software management module conforming to SyncML (Synchronization Markup Language) specification for synchronizing common data between server and client. The method of automated software retrieval and management for mobile devices using these standard specifications minimizes users' interrupts and also can be applied to traditional several different mobile devices, operating systems or downloading web sites without platform dependent considerations.

• Applied Chemistry for Engineering
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• v.4 no.4
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• pp.701-708
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• 1993

Hydrodemetallation(HDM) of VO-tetraphenylporphyrin(VO-TPP) was studied over $CoMo/{\gamma}-Al_2O_3$ catalyst at emperatures between $300^{\circ}C$ and $400^{\circ}C$, the total pressure between $15{\times}10^5$ and $30{\times}10^5$ Pa and the contact times between 0.008 and 0.020gcat. hr./ml teed. HDM of VO-TPP was inhibited by pyridine because the increase of pyridine concentration(up to 4mole%) caused the decrease of HDM conversion. The reaction rate of VO-TPP was found to be apparently 1st order over $350^{\circ}C$ and its activation energy was determined to be about 23kca1/mo1e by Arrhenius plot. Pore mouth-plugging phenomena were shown by ad/desorption isotherm and pore size distribution of fresh and aged catalysts.

• Korean Journal of Veterinary Research
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• v.27 no.1
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• pp.153-155
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• 1987

Determination of cholinesterase activity is a routine practice in many laboratories to detect the influence of cholinesterase inhibiting drugs such as organophosphate and carbamate insecticides. Among many different methods to determine the cholinesterase activity, the present method was the most recent, simple and accurate one for routine test in clinics. The results obtained in sera of human and the different species of animals by means of the present method were as follows: $5.76{\pm}1.12U/ml$ in human, $3.37{\pm}0.83U/ml$ in german shepherd, $0.61{\pm}0.18U/ml$ in rat, $14.91{\pm}3.10U/ml$ in mouse, $1.55{\pm}0.51U/ml$ in chicken, $0.28{\pm}0.11U/ml$ in slaughtered cattle and $0.50{\pm}0.10U/ml$ in slaughtered pig.

• Journal of The Korean Society of Inherited Metabolic disease
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• v.11 no.1
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• pp.88-98
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• 2011

Lesch-Nyhan syndrome is a X-linked recessive disorder caused by a deficiency of the enzyme hypoxanthine-guanidine phosphoribosyltransferase (HPRT), enzyme to recycle purines. Case history: born induced vaginal delivery at 40 weeks complicated by premature membrane ruputure, body weight 2.820 gm. He showed failure to thrive showing severe protein aversion like milk products and pink daper. Developmental delay revealing rolling over at 10.5 month, followed by regression. Seizure at 2 months, His poor oral feeding was lifelong problem. Weak crying, spastic, choreoathetoid movement. Self mutilating behavior noted and diagnosed at age 3 years. No family history of consanguinity and neurological disorders. Method: Laboratory test, physical exam, imaging study and molecular. Clinical follow up Treat ment with allopurinol. Result: uric acid 10.5 mg/dL (N 3.5-7.9), APRT 151.1uM/ min/ml pro(25.7-101), HPRT 7.6 (N 233.5-701) and c.151C>T hemizygote (p,Arg51X). Abdominal sonogram showed staghorn calculi in both kidneys, brain MRI brain atrophy. Clinical follow up showed, seizure at 2 mo, developmental delay (head control and, rolling over at at 11mo, pointing body part at 2 yr 7 mo, eye hand coordination at 2 y 11mo,creeping at 3 y 7 mo, speaking words at 6 y 6 mo ),and developmental regression at 3 yr of age. Sleeping problem including insomnia and severe constipation. Self mutilating behavior (lip bite) started at 2.5 yr, neurologic sx including intermittent upward gaze accompanied by swallowing difficulty at 3 y 7 mo grand mal seizure at 4.5 yr and spastic extremity and trunchal hypotonia and choleoathetoid movement and ataxia at 6.5 yr. Scoliosis with severe spasticity at 9 yr 9 mo. Acute life threatening episode with irregular breathing at 9 yr and 9 mo, Emaciation and nephrolithiasis and recurrent pneumonia. Died suddenly at 10 yr 3 mo. Conclusion: life long feeding problem, chronic gut motility dysfunction, sleeping difficulty and progressing neurologic deterioration and nephrolithiasis despite normal serum uric acid maintence by allopurinol treatment.

• 제어로봇시스템학회:학술대회논문집
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• 2002.10a
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• pp.61.5-61
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• 2002

1. Introduction 2. Development of the Proposed Identification Method 2.1 MlMO Hammerstein nonlinear process 2.2 Process activation 2.3 Identification of the linear dynamic subsystem 2.4 Identification of the nonlinear static function 3. Simulation Study 4. Conclusion. Acknowledgment. References

• Asian-Australasian Journal of Animal Sciences
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• v.18 no.2
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• pp.221-225
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• 2005

An in vitro study was conducted to examine the effect of monensin or fish oil addition on bio-hydrogenation of $C_{18^-} unsaturated fatty acids and CLA production by mixed ruminal bacteria when incubated with safflower oil. Commercially manufactured concentrate (1%, w/v) with safflower oil (0.2%, w/v) were added to mixed solution (600 ml) of strained rumen fluid and McDougalls artificial saliva (control). Monensin $Rumensin^{(R)}$, 10 ppm, w/v, MO), mixed fish oil (0.02%, w/v, absorbed to 0.2 g alfalfa hay, FO) or similar amounts of monensin and fish oil (MO+FO) to MO and FO was also added into the control solution. All the culture solutions prepared were incubated in the culture jar anaerobically at $39^{\circ}C$ up to 12 h. Higher pH (p<0.047) and ammonia concentration (p<0.042) were observed from the culture solution containing MO at 12 h incubation than those from the culture solutions of control or FO. The MO supplementation increased (p<0.0001-0.007) propionate proportion of culture solution but reduced butyrate proportion at 6 h (p<0.018) and 12 h (p<0.001) of incubations. Supplementation of MO or MO+FO increased (p<0.001) the proportions of $C_{18:2}$. The MO alone reduced (p<0.022-0.025) the proportion of c9,t11-CLA compared to FO in all incubation times. The FO supplementation increased the proportion of c9,t11-CLA. An additive effect of MO to FO in the production of c9,t11-CLA was observed at 6 h incubation. In vitro supplementation of monensin reduced hydrogenation of $C_{18^-}$UFAs while fish oil supplementation increased the production of CLA.