• 제목/요약/키워드: Mixed Compound

검색결과 400건 처리시간 0.023초

Al-Ti 혼합 분말 슬러리를 이용한 강의 알루미나이징처리 방법 (Convenient Aluminizing Process of Steel by Using Al-Ti Mixed Powder Slurry)

  • 이영기;김정열;이유기
    • 한국재료학회지
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    • 제19권4호
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    • pp.207-211
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    • 2009
  • In this study, we attempted to develop a convenient aluminizing process, using Al-Ti mixed slurry as an aluminum source, to control the Al content of the aluminized layer as a result of a one-step process and can be widely adopted for coating complex-shaped components. The aluminizing process was carried out by the heat treatment on disc and rod shaped S45C steel substrates with Al-Ti mixed slurries that were composed of various mixed ratios (wt%) of Al and Ti powders. The surface of the resultant aluminized layer was relatively smooth with no obvious cracks. The aluminized layers mainly contain an Fe-Al compound as the bulk phase. However, the Al concentration and the thickness of the aluminized layer gradually decrease as the Ti proportion among Al-Ti mixed slurries increases. It has also been shown that the Al-Ti compound layer, which formed on the substrate during heat treatment, easily separates from the substrate. In addition, the incorporation of Ti into the substrate surface during heat treatment was not observed.

Transformation of Ginsenosides to Compound K(IH-901) by Lactic Acid Bacteria of Human Intestine

  • Bae, Eun-Ah;Kim, Na-Young;Han, Myung-Joo;Choo, Min-Kyung;Kim, Dong-Hyun
    • Journal of Microbiology and Biotechnology
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    • 제13권1호
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    • pp.9-14
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    • 2003
  • When ginsenosides Rbl, Rb2, and Rc were anaerobically incubated with commercial and human intestinal lactic acid bacteria, most commercial lactic acid bacteria did not metabolize these ginsenosides to compound K. However, lactic acid bacteria, B. minimum KK-1, Bifidobacterium cholerium KK-2, and B. cuniculi K-513, isolated from human intestinal microflora transformed these ginsensosides to compound K. When the bacterial mixtures of commercial lactic acid bacteria were incubated with these ginsenosides, these compounds were not transfformed to compound K. However, when Bzfidobacterium KK-1 and KX-2 were miked, these ginsenosides were synergistically transformed to compound K. When water extract of ginseng was incubated with these mixed bifidobacteria, compound K was potently produced. Therefore, it is suggested that, if ginseng with these mixed bifidobacteria is fermented, compound K-enforced ginseng materials could be produced that show cytotoxicity against tumor cell lines.

PARABOLIC MARCINKIEWICZ INTEGRALS ASSOCIATED TO POLYNOMIALS COMPOUND CURVES AND EXTRAPOLATION

  • Liu, Feng;Zhang, Daiqing
    • 대한수학회보
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    • 제52권3호
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    • pp.771-788
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    • 2015
  • In this note we consider the parametric Marcinkiewicz integrals with mixed homogeneity along polynomials compound curves. Under the rather weakened size conditions on the integral kernels both on the unit sphere and in the radial direction, the $L^p$ bounds of such operators are given by an extrapolation argument. Some previous results are greatly extended and improved.

딸기의 고설수경재배에서 배지의 종류가 생육, 수량 및 과실의 품질에 미치는 영향 (Effect of Substrates on the Growth, Yield and Fruit Quality of Strawberry in Elevated Hydroponic System)

  • 전하준;황진규;손미자;최문환;조문수
    • 생물환경조절학회지
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    • 제15권4호
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    • pp.317-321
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    • 2006
  • 본 실험은 딸기의 고설수경재배에 이용 가능한 적정한 배지를 조사하기 위하여 수행하였다. 코코피트 배지에서 엽수가 가장 많았으며, 원예용 상토배지에서 엽장과 엽폭이 가장 우수했다. 과중은 통계적인 유의성은 없었지만 원예용 상토배지에서 25.8g으로 가장 높게 나타났고 과장, 과경, 당도 등도 처리 간에 유의한 차이는 없었지만 원예용 상토배지에서 가장 좋은 결과를 나타내었다. 주당 수확과수는 원예용 상토와 코코피트 배지 모두 왕겨 혼합배지보다 유의하게 높은 수치를 나타내었다. 주당 수량은 원예용 상토배지가 545.9g으로 가장 많았으며, 그 다음으로 코코피트 배지에서 높았으며 왕겨 혼합배지에서 가장 낮았다. 본 연구에서는 딸기의 수경재배에 적합한 고형배지로서 생산자가 구입과 작업이 편리하고 물리성이 좋은 원예용 상토의 우수성을 입증하여, 딸기 재배농가에게 유용한 정보로 활용될 수 있을 것으로 기대되며 타 작물의 고형배지 재배에서도 유용하게 이용될 것으로 생각된다.

X-선 회절법에 의한 철-질소 화합물층의 ε과 γ'상 분율 해석 (Fraction Analysis of ε and γ'-iron Nitride in Compound Layer Using X-ray Diffraction)

  • 김윤기
    • 한국재료학회지
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    • 제16권2호
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    • pp.85-91
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    • 2006
  • The fraction of $\varepsilon\;and\;\gamma$'-iron nitride in compound layer is predicted by x-ray diffraction using direct comparison method. The validity of formulation models was checked by comparing calculated results with metallographic analysis of iron nitride compound layer grown on steel S45C by gas nitriding. The fraction of $\varepsilon$ calculated by the three phase model, porous-$Fe_3N$/ dense-$Fe_3N$/ mixed layer with $Fe_3N\;and\;Fe_4N$, is 80 percent of that analyzed by etching technique. The $\varepsilon$ fraction predicted by mixed layer model is 122 percent of that measured by microscope.

공액사슬로 연결된 이핵금속착체의 전자적 상호작용에 관한 연구 (A Study on Electronic Interaction in Dimetallic Complexes with Conjugated Chain)

  • 정민철
    • 한국전기전자재료학회논문지
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    • 제17권6호
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    • pp.652-660
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    • 2004
  • The cis-hex-3-ene-1,5-diynyl-bridged diiron compound 3, [(η$^{5}$ - $C_{5}$ M $e_{5}$ ) Fe(dppe)]$_2$($\mu$-C≡C-CH=CH-C≡C), have been prepared and characterized by cyclic voltammetry(CV), and electronic spectroscopy (UV-VIS and near-IR, NMR). From the results, compound 3 show two well resolved, single-electron, reversible oxidation waves by CV, and comproportionation constant(Kc) calculated from the CV data for compound 3. The Mixed-valence (MV) radical cation 3$^{+}$ show strong absorptions in the near IR, 1586 nm, and this band is more readily assigned as MV $\pi$-$\pi$ band of delocalized complex (Robin-Day Mixed-valence Class III), and the $H_{ab}$ , effective coupling parameter are most consistent with electronic delocalization.

Effect of 1,3-Diphenyl-guanidine (DPG) Mixing Step on the Properties of SSBR-silica Compounds

  • Lim, Seok-Hwan;Lee, Sangdae;Lee, Noori;Ahn, Byeong Kyu;Park, Nam;Kim, Wonho
    • Elastomers and Composites
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    • 제51권2호
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    • pp.81-92
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    • 2016
  • 1,3-Diphenylguanidine (DPG) is commonly used as a secondary accelerator which not only acts as booster of cure but also activating silanization reaction. The aim of this study is to increase the interaction between silica and rubber by using DPG. In this study, mixing was proceeded in two steps. The T-1 compound is mixed DPG with silica and silane coupling agent in the kneader at high temperature which is named as $1^{st}$ mixing step. T-3 compound is mixed DPG with curatives in the two-roll mill at low temperature which is named as $2^{nd}$ mixing step. The T-2 compound is mixed a half of DPG in $1^{st}$ mixing step and the remainder is mixed in $2^{nd}$ mixing step. Total DPG content was equal for all compounds. When DPG is mixed with silica, silane coupling agent during the $1^{st}$ mixing step, a decrease in cure rate and an increase in scorch time can be seen. This indicates that DPG is adsorbed on the surface of silica. during rubber processing. However, bound rubber content is increased and dynamic properties are improved. These results are due to the highly accelerated silanization reaction. However, there are no significant difference in 100%, 300% modulus.

혼합제제중 Methylephedrine Hydrochloride와 Ephedrine Hydrochloride의 분리정량에 관한 연구 (Study on Isolative Determination Methylephedrine Hydrochloride and Ephedrine Hydrochloride in the Mixed Preparation)

  • 고인석
    • 생약학회지
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    • 제1권3호
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    • pp.93-99
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    • 1970
  • There have been reported by several workers for the isolation and determination of the amine derivatives as Metbylephedrine Hydrochloride and Ephedrine Hydrochloride adopting neutralization method, steam distillation method, non-aqous titration method, ion-exchange resin method, titration method after acetylation, colorimetric method, gravimetric method, iodine titration method and gas chromatography. Those methods mentioned in above, can be practically applied for the sample which is not mixed one mith the other amine compounds. Presently, it has not shown on the isolative determination of the mixed sample of amine derivatives. In this paper, it is discussed on the isolative determination of Methylephedrine Hydrochloride as the tertiary amine compound and Ephedrine Hydrochloride as the secondary amine compound. According to the results of the experiment, it could be summarized as follows: 1. There is no time-variation on the color reaction of Methylephedrine Hydrochloride and Ephedrine Hydrochloride with the color reagent, bromcresolgreen. And Methylephedrine Hydrochloride and Ephedrine Hydrochloride, respectively, can be determined spectrophotometrically by means oft his color reaction. 2. For the isolation of Methylephedrine Hydrochloride and Ephedrine Hydrochloride from the mixed sample, Methylephedrine Hydrochloride can be eluted by chloroform, while Ephedrine Hydrochloride by the mixed solvent of chloroform and ethylalcohol (2:1), from the celite column adsorbed at pH6.4 followed by extraction with ether undersodium hydroxide alkali re action. 3. When the sample is mixed with quinine hydrochloride, dihydrocodeine bitartate, and noscapine, these mixed compounds can be eliminated by means of stram distillation. 4. When the sample is mixed with chlorpheniramine maleate, dextromethorphan hydrobromide and diphenhydramine hydrochloride, the mixed compounds can be eliminated by means of steam distillation and celite adsorption column chromatography, In conclusion, the isolative determination method for Methylephedrine Hydrochloride and Ephedrine Hydrochloride studied in this paper, indicates with the excellent reproducibility and accuracy.

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Fenbufen-Acetaminophen Ester의 합성 및 항염 작용 (Synthesis and Anti-inflammatory Activity of Fenbufen-Acetaminophen Ester)

  • 서정진;이종욱
    • 약학회지
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    • 제28권1호
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    • pp.17-20
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    • 1984
  • Synthetic procedures to synthesize fenbufen-acetaminophen ester were searched by acid chloride method, DCC method and mixed acid anhydride method. The compound was synthesized by DCC method and mixed acid anhydride method but could not be synthesized by acid chloride method. Its anti-inflammatory activity was superior to acetaminophen and similar to fenbufen.

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NH3-Air-C3H8 분위기에서 Nitrocarburisng시 형성된 Compound Layer의 조직제어 (Structural Control of the Compound Layers formed during Nitrocarburising in NH3-Air-C3H8 Atmospheres)

  • 김영희;최광웅
    • 열처리공학회지
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    • 제8권4호
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    • pp.289-301
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    • 1995
  • The effect of Air/$C_3H_8$ gas addition on the compound layer growth of steels nitrocarburised in $NH_3+Air+C_3H_8$ mixed gas atmospheres was investigated. It is considered that amount of residual $NH_3$ was varied according to alternation of Air/$C_3H_8$ mixing ratio and volume content. The compound layer formed from nitrocarburising was composed of ${\varepsilon}-Fe_{2-3}$(C, N) and ${\gamma}^{\prime}-Fe_4$(C, N). According as Air/$C_3H_8$ mixing ratio increased, the superficial content of ${\gamma}^{\prime}-Fe_4$(C, N) within the compound layer was increased, at the same time the growth rate of compound layer and porous layer was increased. In the case of alloy steel at the fixed gas composition, the growth rate of compound layer and porous layer was worse than carbon steel and compound layer phase composition structure primarily consisted of E phase. As the carbon content of materials was increasing in the given gas atmospheres, the growth rate of compound layer and porous layer was increased and the superficial content of ${\varepsilon}-Fe_{2-3}$(C, N) within the compound layer was increased.

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