• Title/Summary/Keyword: Mix-Method

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Mixed Micellizations of TTAB with Other Surfactants (DTAB, CTAB, Tween-20, Tween-40, and Tween-80) (TTAB와 다른 계면활성제(DTAB, CTAB, Tween-20, Tween-40 및 Tween-80)와의 혼합미셀화에 대한 연구)

  • Lee, Nam-Min;Lee, Byung-Hwan
    • Journal of the Korean Chemical Society
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    • v.56 no.5
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    • pp.556-562
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    • 2012
  • The critical micelle concentration (CMC) and the counter-ion binding constant (B) for the mixed micellizations of TTAB (tetradecyltrimethylammonium bromide) with other surfactants (DTAB, CTAB, Tween-20, Tween-40, and Tween-80) in aqueous solution of 4-chlorobenzoic acid (0.5 mM) at $25^{\circ}C$ were determined as a function of ${\alpha}_1$ (the overall mole fraction of TTAB) by using the spectrophotometric method and the conductivity method. Various thermodynamic parameters ($X_i$, ${\gamma}_i$, $C_i$, $a_i^M$, ${\beta}$, and ${\Delta}H_{mix}$) were calculated for each mixed surfactant system and compared with the other mixed surfactant systems by means of the equations derived from the nonideal mixed micellar model. The results show that TTAB/DTAB mixed system has a great positive deviation from the ideal mixed micellar model and the other mixed systems have great negative deviations from the ideal mixed model.

Performance Evaluation of Nitrogen Oxide Removal by Air Purification Blocks with Titanium Dioxide (이산화티타늄을 이용한 대기정화 블록의 질소산화물 제거 성능 평가)

  • Oh, Ri-On;Kim, Hwang-Hee;Park, Sung-Ki;Cha, Sang-Sun;Park, Chan-Gi
    • Journal of The Korean Society of Agricultural Engineers
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    • v.62 no.5
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    • pp.39-46
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    • 2020
  • This study evaluated the nitrogen oxide (NOx) removal efficiency by air purification concrete blocks with titanium dioxide (TiO2). The concrete in the mixtures had a 30% water:cement ratio, to which TiO2 was added at 0%, 5%, and 10% of cement weight. The compressive strength reduction rate and removal efficiency of NOx were investigated. The result of the compressive strength test in the study indicated that addition rate of TiO2 did not lead to signifcant effect. In terms of the average removal efficiency of NOx, mix No. 1 using a TiO2 mixing ratio of 0% had a removal efficiency of 0.57% on average; thus, the removal effect w as not significant. For the other samples prepared by mixing, the average removal efficiencies for mix No. 2 (5% TiO2) were 58.86% and 62.05% for normal and washing surface treatments, respectively, and those of sample No. 3 (10% TiO2) were 59.94% and 67.61%. mixs No. 4 (5%) and No. 5 (10%), in which TiO2 diluted with distilled water was sprayed onto the block surface, had an average NOx removal efficiency of 61.72% and 68.48%, respectively. In terms of NOx removal efficiency, Mixs No. 3 and No. 5 with 10% TiO2 were better than Mixs No. 2 and No. 4 with 5% TiO2. In addition, analyzing the NOx removal efficiency results from the fixing method, it was capable to apply mixing (washing) and the diluted spray methods. Therefore, it was found that the diluted spray method applied in this study can be employed in any manufacture of air purification concrete blocks.

The Fundamental Study of Strength and Drying Shrinkage on Alkali-activated Slag Cement Mortar with Different Entering Point of Fine Aggregate (잔골재의 투입시점에 따른 알칼리 활성화 슬래그 모르타르의 강도와 건조수축에 대한 기초적 연구)

  • Kim, Tae-Wan;Eom, Jang-Sub;Seo, Ki-Young;Park, Hyun-Jae
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.18 no.2
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    • pp.117-125
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    • 2014
  • This paper examines the fundamental properties of alkali-activated slag cement (AASC) activated by sodium hydroxide (NaOH). The water to binder (W/B) ratio was 0.4 and 0.5. And concentration of activator were 2M and 4M. Five mix design of each W/B ratios was considered. The N0 mixture was KS L 5109 method and N1~N4 were varied in different mixing time, mix step and entering points of fine aggregate. Test results clearly showed that the flow value, strength and drying shrinkage development of AASC were significantly dependent on the entering point of fine aggregate. The flow value tended to decreases with delaying entering point of fine aggregate. The compressive strength and flexural strength increases with delaying entering point. Moreover, the XRD analysis confirmed that there were sustain these results. The drying shrinkage increases with delaying entering point of fine aggregate. Futhermore, a modified mixing method incorporating all hereby experimentally derived parameters, is proposed to improvement the physical properties of AASC.

Experimental Study on Reduced Amount of Rebound in Wet Process Shotcrete Works by Upon Accelerator Contents (급결제 함유량에 따른 습식 Shotcrete 리바운드 감소량에 대한 실험적 연구)

  • Jeon, Jun Tai;Park, Hong Tae;Lee, Yang Kyu
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.32 no.6D
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    • pp.615-622
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    • 2012
  • The aim of shotcrete is to increase the bearing capacity and to protect the excavated surface from erosion by preventing falling of rock mass. Shotcreting method is divided into two types as dry process and wet process. Since 1997, wet process method has been used more frequently than dry process method in field works. The failure to bond, so called rebound, occurs in many case during shotcrete works. The excess amount of rebound has a significant effect on the total construction cost. For example, material and craft-man cost increases, the shooting time delays due to deceleration of work execution stage, work efficiency of craft-man decreases and additional cost to remove the muck generates. In this study, therefore, the experimental analysis of rebound amount and strength was conducted by analyzing the actual construction data for wet process type of shotcreting method upon accelerator contents. Also, the effective and rational method was suggested, which can be actually implemented in the Korea construction sites.

Development of an UPLC-DAD Method for Simultaneous Analysis of Eight Marker Compounds of Bulhwangeumjeonggi-san (UPLC-DAD를 이용한 불환금정기산의 다성분 동시분석법 개발)

  • Lee, Kyung-hee;Lamichhane, Ramakanta;Kumar, Sharma Dipak;Raj, Pandeya Prakash;Kim, Se-Gun;Jung, Hyun-Ju
    • Korean Journal of Pharmacognosy
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    • v.47 no.4
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    • pp.366-373
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    • 2016
  • Bulhwangeumjeonggisan (BHGJGS) is a traditional herbal formulation generally used in the treatment of cold and gastritis. BHGJGS consists of eight herbal plants; Atractylodis Rhizoma, Magnoliae Cortex, Citri Pericarpium, Glycyrrhizae Radix, Agastachis Herba, Pinelliae Rhizoma, Zingiberis Rhizoma and Zizyphi Fructus. Complete standardization of this formulation has not been done yet. So, a simple and accurate method was developed and validated using Ultra Performance Liquid Chromatography (UPLC) with Diode Array Detector (DAD) for the standardization of BHGJGS. UPLC conditions were optimized using a c18 RP-Amide column with mobile phase; 0.1% phosphate buffer and acetonitrile, detection wavelength; 210 and 325 nm. The linearities of calibration curves were acceptable ($R^2$>0.9994), and the limit of detection and quantification were within the ranges of 0.011-0.091 and $0.034-0.277{\mu}g/ml$ respectively. The relative standard deviation (RSD) of intra- and inter-day precisions were under 3.61%. The RSD of repeatability was under 0.68 %. The results of recovery test were 94.4-107.9%, and the RSD were under 4.6%. The developed method was used to find the contents of standard constituents in BHGJGS mix extract powder, and two commercial formulation (A and B). The data show that the developed method was specific, sensitive, accurate, and precise for analysis of BHGJGS components.

Resin Bond Strength of Lithium Disilicate Glass-Ceramic by Surface Cleansing Method after Temporary Cementation (임시접착 후, 치면세마에 따른 Lithium Disilicate Glass-Ceramic의 레진결합강도에 대한 연구)

  • Chung, Seung-Hwa;Lee, Jin-Han;Oh, Sang-Chun
    • Journal of Dental Rehabilitation and Applied Science
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    • v.23 no.3
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    • pp.259-268
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    • 2007
  • purpose: This study was to evaluate the shear bond strength of Lithium Disilicate Glass-Ceramic by removable method of temporary cement on the abutment tooth. Material and Method: Sixty molar teeth of human with the occlusal surface up were mounted in acrylic resin blocks. The 45 specimens were prepared to exposure dentin by diamond bur and the eugenol-containing temporary cement($Cavitec^{TM}$ ($KERR^{(R)}$, U.S.A)was applied to the dentin surfaces. After initial removal of the cement with a dental explorer, the specimens were divided into 4 groups of 15 specimens each. The dentin surfaces of the specimens were treated by rotary instrument with as follow pastes: $Zircate^{(R)}$ prophy paste(Dentsply, U.S.A), Radent Prophy Paste(Pascal company,inc. U.S.A), and Dental pumice(Wip mix corporation,U.S.A). An adhesive resin luting agent(Variolink $II^{(R)}$, Ivoclar Vivadent, Leichtenstein) including Monobond-S and $Excite^{(R)}$ was applied to all specimens. The ceramic specimens were made with an A1 ingot of IPS Empress $II^{(R)}$ (Ivoclar Vivadent, Leichtenstein). After the specimens were stored in distilled water for 48hr, the shear bond strength(MPa) was measured by a Universal testing machine(Zwick 145641, Zwick, Germany) at a 1mm/min cross-head speed. The data were statistically analyzed by one-way ANOVA and Duncan's multiple range test. Results: In all group, there were no significant differences in comparison with the control group(p>0.05). The pattern of most failure showed the mixed type of cohesive and adhesive failure. Conclusion: Resin bond strength of IPS Empress $II^{(R)}$ was not affected by removal method of the temporary cement.

Real-Time Traffic Information Collection Using Multiple Virtual Detection Lines (다중 가상 검지선을 이용한 실시간 교통정보 수집)

  • Kim, Eui-Chul;Kim, Soo-Hyung;Lee, Guee-Sang;Yang, Hyung-Jeong
    • The KIPS Transactions:PartB
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    • v.15B no.6
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    • pp.543-552
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    • 2008
  • ATIS(Advanced Traveler Information System) is the system to offer a real-time traffic information or traffic situation for the benefit of the client. One of traffic information collection methods for ATIS research is the method of image analysis. The method is divided into two : one is the method to set two loop detectors at the area and the other is the method detecting the vehicle through an image analysis. In this paper, we propose a real-time traffic information collection system to mix two methods. The system installs multiple virtual detection lines and traces the location of the vehicle. Use of multiple virtual detection lines supplements the defect of the method of loop detectors. And we drew a representative pixels in the detecting area and used it for image analysis. This is to solve the problem of time delay which increases as the image size increases. We gathered traffic images and experimented using the system and got 92.32% of detection accuracy.

Initial Control of Microorganism in Kimchi by the Modified Preparation Method of Seasoning Mixture and the Pretreatment of Electrolyzed Acid-Water (전해산화수 전처리 및 양념류 제조방법에 따른 김치의 초기 미생물 제어)

  • Park, Kee-Jai;Jung, Sung-Won;Park, Byoung-In;Kim, Young-Ho;Jeong, Jin-Woong
    • Korean Journal of Food Science and Technology
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    • v.28 no.6
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    • pp.1104-1110
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    • 1996
  • To lessen the initial level of microorganism in kimchi, the preparation method of seasoning mixture was modified and electrolyzed acid-water was substitute for washing water and brine water. Changes in the microbial counts of the red pepper powder-garlic mixture prepared with red pepper powder, garlic and 4.8% (w/w) water (tap water and electrolyzed acid-water) of manufactured kimchi showed that coliform count and E. coli count were reduced to 93% and 98%, of the initial level in the tap water added red pepper powder-garlic mixture and 97% and 99% in the electrolzed acid-water added mixture after 6 hours of mix. After 24 hours of mix, no E. coli was recovered in borth mixtures. Microbial levels were revealed as $2.4{\times}10^5\;CFU/g$ for total count, $2.3{\times}10^5\;CFU/g$ for Lactobacillus count. $1.0{\times}10^2{\;}CFU/g$ of coliform count and $10^1\;CFU/g$ of E. coli count in the seasoning mixture prepared by the general method, and $4.2{\times}10^5\;CFU/g$ of total count, $4.0{\times}10^5CFU/g$ of Lactobacillus count, $1.0{\times}10^3\;CFU/g$ of coliorm count and $4.0{\times}10^2\;CFU/g$ of E. coli count in the mixture propared by the modified method. During fermentation at $10^{\circ}C$, the levels of total and Lactobacillus counts in kimchi prepared by the modified method were significantly lower than those of kimchi were recovered in kimchi prepared by the modified method, whereas there were at the level of $10^1\;CFU/g$ in kimchi prepared by the general method. The pH and acidity of kimchi prepared by the modified method were 4.66 and 0.54%, respectively, whereas those in kimchi prepared b the general method were 4.51 and 0.70%, respectively. But after 14 days of fermentation significant differences were not observed in the changes of microbial, pH and acidity for both kimchi.

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Setting Time Evaluation of High Flowable Ternary Concrete Mix Using Durometer (듀로미터를 이용한 3성분계 고유동 콘크리트의 응결시간 추정)

  • Han, Min-Cheol;Lee, yuk-Ju
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.8 no.1
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    • pp.33-38
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    • 2020
  • The aim of the research is to evaluate the feasibility of durometer for assessing setting time of the concrete by comparing it with the currently used proctor penetration test method to improve the surface finishing timing determining method generally determined based on the experience of the worker. As a research result, the correlation between suggesting method using durometer with currently used proctor penetration test method was high enough. Hence, on the surface of the concrete, the initial setting time and the final setting time could be designated as 41 HD with C-type, and 11 HD with D-type, respectively. Therefore, the durometer can be used as a portable setting time evaluation device with the easiness of handling and measuring for determining concrete surface finishing timing quantitatively.

Fashion Coordination of Black Color in Fashion Collection -Focused on 2005~2007 Collection- (패션 컬렉션에 나타난 블랙컬러의 패션 코디네이션 연구 -2005~2007년 컬렉션을 중심으로-)

  • Je, Gi-Yeon;Lee, Kyoung-Hee
    • Journal of the Korean Society of Clothing and Textiles
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    • v.33 no.7
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    • pp.1003-1013
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    • 2009
  • This study offers data that can be used to direct the styles of black dresses by looking into the characteristics of coordination in black fashion, which is continuously appearing at modem. fashion collections with a unique aesthetic value and image. This study examined the characteristic of fashion coordination of black color: First, to look at the fashion image of black color, second, to look at the characteristic of black color coordination appearing in black fashion, and third, to look at the method of coordination appearing in black color. This study collected and selected 560 black pictures that showed the fashion collections from 2005 S/S until 2007 F/W. As for data analysis, the researcher made a content analysis by classifying the pictures by item, material, accessory, and a coordination method. The research results are as follows: First, the fashion image of black color was expressed as sexy feminine, modern chic, modern future, genderless, and avant-garde images. Second, the fashion coordination of black color has the characteristics of sexiness and dignity by the use of body exposure, concealment, and a subdued line that expresses a modern, minimal atmosphere. The mix & match of materials expressed the monotony of one color as refined beauty and the use of accessories appeared to bring the image into relief. Third, as for the coordination method, pants on skirts, pants on dresses, piece coordination of code matching, plus- one coordination through vivid colors and accessories, and cross-over coordination relying on shape, material, and sense were prominent.