• Title/Summary/Keyword: Mineral Detection

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Luminescence Identification Characteristics for Irradiated Dried Fishery Products (조사처리한 건조수산품의 전처리 방법에 따른 Luminescence 판별 특성)

  • Kim, Moon-Young;Ahn, Jae-Jun;Kim, Gui-Ran;Kwak, Ji-Young;Park, Kun-Sang;Lee, Kyung-Jin;Kwon, Joong-Ho
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.42 no.11
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    • pp.1837-1842
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    • 2013
  • Photostimulated luminescence (PSL) and thermoluminescence (TL) analyses were conducted for the detection of different gamma-irradiated dried fishes (mussel, squid, beka squid, mitra squid, plaice, and saury) at 0, 1, 5 and 10 kGy. For TL analysis, the contaminating silicate minerals were obtained by density separation or acid hydrolysis treatment. PSL determinations indicated that all the non-irradiated samples showed PSL photon counts/60 s (PCs) lower than 700 PCs (negative), but the irradiated mussel sample at 5 and 10 kGy were only possibility identified showing higher than 5000 PCs (positive). Irrespective of sample kinds and methods of mineral separation, all the non-irradiated samples showed TL glow curves in low-intensity with a maximum peak only after $250^{\circ}C$. However, all the irradiated samples produced TL glow curves in high intensity with a maximum peak particularly in the temperature range of 1$150{\sim}250^{\circ}C$. In conclusion, more distinguishable TL results [glow curve, TL ratio ($TL_1/TL_2$)] were obtained from the marker minerals separated by acid hydrolysis rather than density method.

Effect of Agrichemicals during Cultivation on Quality and Shelf-life of Fresh-cut Lettuce (재배과정 중 농약살포 정도가 신선편이 양상추의 품질 및 저장성에 미치는 영향)

  • Youn, Aye-Ree;Kwon, Ki-Hyun;Kim, Byeong-Sam;Kim, Sang-Hee;Noh, Bong-Soo;Cha, Hwan-Soo
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.38 no.2
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    • pp.217-224
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    • 2009
  • This study investigated the effect of agrichemicals (A) and low-agrichemicals (LA) during cultivation on the quality characteristics of minimally processed lettuce (Lactuca sativa L.) during storage at $4{\pm}1^{\circ}C$. After 10 days of storage, the sugar content analysis showed that LA-treated lettuce ($4.57^{\circ}Brix$) was higher than A-treated lettuce ($3.57^{\circ}Brix$). The major minerals were K, P and Na, and mineral contents were high in A-treated lettuce during 0, 5 and 10 days. However, the sample with LA treatment had higher chlorophyll and vitamin C contents compared with A-treated lettuce. The degree of color was more stable in samples kept at LA treatment than those kept at A treatment. The polyphenol oxidase (PPO) activity of the LA-treated lettuce was 475.90 unit/g, while the A-treated sample had almost 1.5-fold higher activity. The detection of 48 residual pesticides in samples were not detected on storage 0 day.

Physicochemical and Archaeometric Characteristics of Goryeo Period Potteries from the Sandongri in Seosan, Korea (서산 산동리 고려시대 도기의 물리화학적 및 고고과학적 특성)

  • Lee, Chan Hee;Jin, Hong Ju
    • Journal of Conservation Science
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    • v.32 no.2
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    • pp.123-139
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    • 2016
  • The excavated potteries of Goryeo Period from the Sandongri archaeological site in Seosan were studied on physicochemical analyses. Surface color of the samples are mainly grayish blue, and showed the natural glaze by melting the body soils during the burning. Partly, swelling surface are observed bloated marks because of blow out gas by burning. The potteries are some possibility of making the similar source clay on the basis of magnetic susceptibilities (about $1{\times}10^{-3}SI\;unit$) and general occurrences. Values of specific gravity, apparent porosity and absorption ratio are divided two groups as highly different cases of bloating surface samples. The source clay of the potteries used mainly microcrystalline clay, the mineral compositions are quartz and some colored minerals. Based on the analysis, the burning temperature of the potteries are assumed that they were around $1,100^{\circ}C$ because detection of quartz and mullite within hard and compact matrices. As geochemical variations of the samples, evolution trends of rare earth, compatible and incompatible elements showed very similar patterns excepting the some major elements, that means the potteries are interpreted to making by elutriation processes using the same raw clays from very similar basement rocks of genetically.

Interpretation on Raw Material Characteristics and Manufacturing Techniques of Brown-glazed Stonewares and Roof Tiles from Hong Nang Sida Temple, Laos (라오스 홍낭시다 유적 출토 갈유도기와 기와의 원료특성과 제작기술 해석)

  • Jin, Hong Ju;Jang, Sungyoon;Kim, Su Kyoung;Lee, Myeong Seong;Moon, Dong Hyeok;Chun, Yu Gun
    • Journal of the Mineralogical Society of Korea
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    • v.32 no.4
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    • pp.273-285
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    • 2019
  • This study is aimed to interpret the raw material characteristics and manufacturing technology through physical, mineral and geochemical analysis of the brown-glazed stonewares and roof tiles excavated from the Hong Nang Sida temple in Laos, which was built in the 12th century. The glaze of brown-glazed stoneware is a typical lime serial with CaO content of more than 15 % and they were vitrified. The body is the combination of quartz, mullite and cristobalite, but had not vitrified texture, and therefore, which is assumed to have been fired more than 950 ℃. Meanwhile, The roof tiles are unglazed and its outer color is reddish brown, whitish grey and bluish grey. The bluish gray tiles has sandwich structure, which seem to experience imperfect reducing environment. The tile samples with a number of amorphous iron oxide nodule had a very similar chemical composition. In conclusion, it is assumed that the clay source was made from raw material produced from the same bedrock. The firing temperature of roof tiles were divided into less than 900 ℃, 900~950 ℃ and greater than 950 ℃ according to detection of micas, hercynite and mullite.

COMPARATIVE STUDY ON THE RATE OF DENTAL ENAMEL DEMINERALIZATION USING A QLF (Quantitative Light-induced Fluorescence를 이용한 법랑질 탈회 속도에 관한 비교 연구)

  • Lee, Chang-Keun;Yoo, Seung-Hoon;Kim, Jong-Soo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.31 no.3
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    • pp.506-515
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    • 2004
  • The objective of this study was to compare the rate of in vitro demineralization of bovine permanent (BP), human deciduous (HD) and human permanent (HP) enamel. Twenty aye flattened and polished enamel samples for each group (BP, HD, HP) were immersed in a demineralizing solution (0.1 mol/L lactic acid, 0.2% Carbopol 907, and 50% saturated hydroxyapatite) for 1, 2, 4 or 8 days. All 25 samples from each group were subjected to Quantitative light induced fluorescence analysis (QLF) and 5 samples from each group were randomly selected for Transverse Microradiography analysis (TMR). Integrated mineral loss (IML) and lesion depth (LD) were determined by TMR. The fluorescence radiance (FR) of sound enamel $(FR_S)$, demineralized enamel $(FR_D)$ were determined by QLF and FR ratio $(FR_D/FR_S)$ was calculated. Bovine enamel samples showed significant correlation between FR ratio and lesion depth(p<0.05) and deciduous enamel samples does not showed significant correlation between FR ratio and lesion depth(p>0.05). Permanent enamel samples showed significant correlation between FR ratio and lesion depth(p<0.05) The constant of demineralization time between FR ratio from regression analysis were as follows: bovine enamel was -4.643(p<0.05) deciduous enamel was -5.421(p<0.05) and permanent enamel was -4.435(p<0.05).

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Characteristics of Thermoluminescence and Electron Spin Resonance and Organoleptic Quality of Irradiated Raisin and Dried Banana During Storage (건포도와 건바나나의 감마선 조사와 저장기간에 따른 열발광 및 전자스핀공명 특성과 관능적 품질)

  • Jo, Deok-Jo;Kwon, Joong-Ho
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.31 no.4
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    • pp.609-614
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    • 2002
  • The characteristics of thermoluminescence (TL) and electron spin resonance (ESR) and organoleptic qualities of gamma-irradiated raisin and dried banana were investigated during storage at 4$^{\circ}C$ for 6 months. The minerals separated from non-irradiated raisins showed TL glow curve (TL$_1$) with very low intensity around 200~30$0^{\circ}C$, while the irradiated samples at 1 kGy or more showed glow curves with higher intensity around 18$0^{\circ}C$, with linear increase by irradiation dose ($R^2$=0.9684), which made it possible to identify irradiated samples during 6 months. Moreover, TL ratios (TL$_1$/TL$_2$) through the reirradiation step at 1 kGy enhanced confidence in the identification of irradiated raisins. The ESR signals of multicomponent lines resulted from crystalline sugar radicals were shown in irradiated banana, identifying irradiated samples. The ESR signal intensity was dependent on irradiation doses ($R^2$=0.8977) and the signals were stable enough to be detected by 6th month after storage. Considering tile marketability of irradiated dried fruits during 6 months at low temperature TL and ESR analyses were shown suitable for the identification of irradiated raisins and dried banana, respectively.

Characteristics of proteolytic microorganisms and their effects on proteolysis in total mixed ration silages of soybean curd residue

  • Hao, Wei;Tian, Pengjiao;Zheng, Mingli;Wang, Huili;Xu, Chuncheng
    • Asian-Australasian Journal of Animal Sciences
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    • v.33 no.1
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    • pp.100-110
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    • 2020
  • Objective: The objective of this study was to isolate proteolytic microorganisms and evaluate their effects on proteolysis in total mixed ration (TMR) silages of soybean curd residue. Methods: TMRs were formulated with soybean curd residue, alfalfa or Leymus chinensis hay, corn meal, soybean meal, a vitamin-mineral supplement, and salt in a ratio of 25.0: 40.0:30.0:4.0:0.5:0.5, respectively, on a basis of dry matter. The microbial proteinases during ensiling were characterized, the dominate strains associated with proteolysis were identified, and their enzymatic characterization were evaluated in alfalfa (A-TMR) and Leymus chinensis (L-TMR) TMR silages containing soybean curd residue. Results: Both A-TMR and L-TMR silages were well preserved, with low pH and high lactic acid concentrations. The aerobic bacteria and yeast counts in both TMR silages decreased to about 105 cfu/g fresh matter (FM) and below the detection limit, respectively. The lactic acid bacteria count increased to 109 cfu/g FM. The total microbial proteinases activities reached their maximums during the early ensiling stage and then reduced in both TMR silages with fermentation prolonged. Metalloproteinase was the main proteinase when the total proteinases activities reached their maximums, and when ensiling terminated, metallo and serine proteinases played equally important parts in proteolysis in both TMR silages. Strains in the genera Curtobacterium and Paenibacillus were identified as the most dominant proteolytic bacteria in A-TMR and L-TMR, respectively, and both their proteinases were mainly with metalloproteinase characteristics. In the latter ensiling phase, Enterococcus faecium strains became the major sources of proteolytic enzymes in both TMR silages. Their proteinases were mainly of metallo and serine proteinases classes in this experiment. Conclusion: Proteolytic aerobic bacteria were substituted by proteolytic lactic acid bacteria during ensiling, and the microbial serine and metallo proteinases in these strains played leading roles in proteolysis in TMR silages.

Detection of Long Period Seismic Events by Using a Portable Gravity Meter, gPhone (이동식 중력계(gPhone)를 활용한 장주기 지진 이벤트 관측)

  • Lee, Won Sang;Seo, Ki-Weon;Eom, Jooyoung;Sheen, Dong-Hoon;Lee, Choon-Ki;Park, Yongcheol;Yun, Sukyoung;Yoo, Hyun Jae
    • Geophysics and Geophysical Exploration
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    • v.18 no.1
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    • pp.31-34
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    • 2015
  • A gravity meter has been used for exploring subsurface mineral resources and monitoring long-period events such as Earth tides. Recently, researchers found several other intriguing features that we could even detect large teleseismic earthquakes and monitor seismic ambient noise using gravimeters. The zero-length spring suspension technology gives the gPhone (Micro-g LaCoste) excellent low frequency sensitivity, which may have implications for investigating much longer-period natural events (e.g., Earth's hum, tsunami waves, etc.). In this study, we present preliminary results through temporary operation of the gPhone at Geumsan in South Korea for 9 months (Nov. 2008-Jul. 2009). The gPhone successfully recorded large teleseismic events and showed a clear seasonal variation of the Double frequency microseisms during its operation period.

Determination of Uranium Concentration in Solid- and Liquid-state Geological Materials by Fission Track Registration Technique and its Applicability (피션트랙 검출기법에 의한 고체 및 액체상태 지질물질의 우라늄 정량과 그 적용성)

  • Shin, Seong-Cheon
    • The Journal of the Petrological Society of Korea
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    • v.24 no.2
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    • pp.77-90
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    • 2015
  • The fission track registration techniques for accurate determinations of uranium in solid- and liquid-state geological materials were recommended and their applicability were examined. The determination of uranium can be achieved by optical counting of neutron-induced fission tracks of $^{235}U$ registered on solid-state track detectors under high magnification. In a dry registration method using powdered pellets of rocks (e.g., granite and coal) showing good uranium-affinity, it was not easy to decide an overall mean concentration over the total sample owing to track-clusters caused by frequent presence of uranium-bearing minerals. Separate scanning for homogeneous and track-clustered parts may be an alternative choice. Assuring the homogeneity over the whole sample, high reproducibilities were confirmed both from duplicate detections using mica and Lexan polycarbonate detectors and from multiple measurements at different thermal neutron fluences. The wet registration method using sealed quartz tubes is recommended to overcome the common heterogeneity in uranium concentrations of $10^1ppm$ and more. Adopting the wet registration, the uranium homogeneity was recovered below the $10^0ppm$ level and the lower detection limit was proved to reach without difficulty the $10^2ppb$ (i.e. $ng\;g^{-1}$) level.

Application of Geophysical Survey to the Geological Engineering Model for the Effective Detection in Foundation of Stone Relics (석조문화재 기초지반 파악을 위한 모형지반에서의 탐사기법 적용)

  • Kim, Man-Il;Lee, Chang-Joo;Kim, Jong-Tae;Kim, Ji-Soo;Kim, Sa-Dug;Jeong, Gyo-Cheol
    • The Journal of Engineering Geology
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    • v.18 no.4
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    • pp.537-543
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    • 2008
  • To effectively delineate the foundation of stone relics by GPR and seismic refraction methods, a geological engineering model was constructed with alternating layer of soil and gravel to a depth of 3 m. This study was aimed at mapping the boundaries of model ground structure and interfaces of alternating layer using the various frequency antenna in GPR survey and seismic velocities. Compared to the resolution from the high frequency antenna, the image resolution from the survey using 100 Hz antenna is the lower, but with the deeper image coverage. On the contrast, the deeper structure was not mapped in the higher frequency data due to higher absorption effect, but the shallow layered zone was distinctively resolved. Therefore subsurface images were effectively provided by integrating the data with 100 MHz and 450 MHz antennas for the deep and shallow structures, respectively. Regarding the seismic refraction data, the boundaries of the model and interface of the alternating layers were not successfully mapped due to the limit of the survey length. However, the equivalent contours of low velocity extended deep as considerable velocity contrasts with surrounding ground.