• Title/Summary/Keyword: Microstructure development

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Some Physical and Electrical Properties of Zirconia Solid Electrolyte Contained Yttria (이트리아를 함유한 지르코니아 고체전해질의 물리적, 전기적 특성)

  • 정형진;오영제
    • Journal of the Korean Ceramic Society
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    • v.23 no.1
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    • pp.13-20
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    • 1986
  • Zirconia soild electrolytes containing 4~10mol% of yttria were prepared by wet-blending of oxides and rea-ction-sintering, Sinterbility and degree of stabilization were optimized for the development of oxygen sensor. Fracture strength thermal expansion coefficient electrical conductivity and galvanic potential were measured and discussed with respect to the amount of ytria addition phase transformation microstructure and degree of stabilization. It was found that sintering and stabilization occurred when the composition was designed to be near the boundary region of $ZrO_2-Y_2O_3$ binary system. In such away a good zirconia solid electrolyte suitable for oxygen sensor could be developed.

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Development of New Semi-solid Method and Practical Application to Bearing Bracket (신 반응고 슬러리의 개발과 베어링 브라켓에 대한 적용)

  • Sim, Jae-Gi;Moon, Jun-Young;Kim, Jae-Min;Hong, Chun-Pyo
    • Journal of Korea Foundry Society
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    • v.27 no.4
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    • pp.173-178
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    • 2007
  • The bearing bracket, which has produced by the squeeze casting for the high strength in lightweight part of automobile, was developed by the rheocasting process using the H-NCM slurry. Compared with the squeeze casting, the rheocasting process has some merits such as shortening cycle-time, reducing total weight, and increasing productivity. In this study, partial feeding test was carried out by controlling plunger stroke length and compared with semisolid simulation. Optimal casting parameters such as injection speed and stroke variations were established. Sound products with integral microstructure were obtained by the H-NCM slurry and X-ray analysis also showed the integral condition throughout the entire parts.

A Study on the Synthesis and Mechanical Characteristics of NATM Resin (HATM 수지의 합성 및 기계적 특성에 관한 연구)

  • Kim, Ki-Jun
    • Journal of the Korean Applied Science and Technology
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    • v.22 no.4
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    • pp.355-361
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    • 2005
  • The physical characteristics of polyurethane were examined by SEM, FT-IR tensile strength and mole % [NCO/OH]. Growing concerns in the environment-friendly architecture and public works have led to the development of solvent-free formulations that can be cured and foamed in air. Compared with general packing materials, this resin is much stronger in intensity and much longer in durability. Polyurethane foam resins were mainly composed of polyol, MDI, silicone surfactant, fillers, catalyst and blowing agent. The rigid foam of polyurethane in mechanical characteristics were due to chain extender and the increase of mole % [NCO/OH]. The change in the microstructure of polyurethane should be taken into account when considering the process of construction and durability through the polyurethane polymer resin in lots of industries.

Development of Multi-Components Model of Cement Hydration

  • WangXiaoYong
    • Cement Symposium
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    • s.34
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    • pp.129-137
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    • 2007
  • This paper presents a numerical model which can predict degree of cement mineral component, such as $C_3S$, $C_2S$, $C_3A$, $C_4AF$ and microstructure of hydrating cement as a function of water to cement ratio, cement particle size distribution, cement mineral components and temperature. In this model cement particles are parked randomly in cell space and hydration process is described using a multi-component intergrated kinetic model. The simulation result of degree of hydration of cement mineral component agrees well with experiment result. The content of cement hydration product, such as CSH and CH can be obtained as an accompanied result during hydration process. By introducing of equal-area projection method, water withdrawl mechanism and contact area among cement particles can be considered in detail. By using proposed method, pore size distribution of hydrating cement is predicted.

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The softening behavior of Mg-Li-Al(-Zr) alloys (Mg-Li-Al(-Zr) 합금의 연화현상)

  • Kim, Y.W.;Kwang, Y.H.;Lim, Y.J.;Kim, D.H.;Hong, C.P.
    • Journal of the Korean Society for Heat Treatment
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    • v.11 no.1
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    • pp.10-16
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    • 1998
  • The softening behavior of squeeze cast Mg-Li-Al and Mg-Li-Al-Zr alloys have been investigated. The highest hardness values of Mg-Li-Al and Mg-Li-Al-Zr alloys were obtained after solution treatment at $400^{\circ}C$ for 1 hour. The hardness value, however, decreased as the aging temperature and time increased. Microstructural and calorometric analyses showed that quenched-microstructure changed from primary (${\alpha}$ and ${\beta}$)+secondary ${\alpha}$ to primary(${\alpha}$ and ${\beta}$)+secondary ${\alpha}+{\theta}$ after aging. The softening during aging was due to the coarsening of ${\theta}$ precipitates.

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The Effects of Thermo-mechanical Treatment on the Thixoforming Process of Cu-Ca Alloys for High Efficiency Electrical Motors (고효율 전동기용 Cu-Ca 합금의 반응고 성형공정에 미치는 가공열처리의 영향)

  • Lee, E.Y.;Kang, B.M.;Lee, S.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.16 no.5
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    • pp.267-274
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    • 2003
  • The effect of the thermo-mechanical treatment on the microstructural development and the electric conductivity of Cu-Ca alloys are studied for the thixoforming processed rotor of the induction motor The Cu-Ca alloys containing Ca less than 1.0wt% show the electrical conductivity higher than 80% IACS They also show broad melting range over $150^{\circ}C$ which is desirable for the thixoforming process The semi-solid microstructure of cast alloy changes from the dendrite structure to globular structure by prior deformation before reheating. The details of microstructural changes by the thermo-mechanical treatment are discussed.

A Study on the Squeeze Casting of Al-7.0Si-0.4Mg Alloy for Fuel System Parts (Al-7.0Si-0.4Mg 합금 자동차 연료계 부품의 스퀴즈 캐스팅에 관한 연구)

  • 김순호
    • Journal of the Korean Society for Precision Engineering
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    • v.20 no.12
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    • pp.48-54
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    • 2003
  • Alumium alloys casting are gaining increased acceptance in the automotive and electronic industeries and squeeze casting is the most efficient method of manufacturing such mass produced parts. This study has been investigated the microstructures and mechanical properties of Al-7.0Si-0.4Mg (AC4C) alloy fabricated by squeeze casting process for development of Fuel system Parts (Fuel rail). The microstructure of squeeze casted specimen were composed of eutectic structure Alumimim solid solution and $Mg_2$Si precipitates. The tensile strength of as-solid solution treatment Al-7.0Si-0.4Mg ahoy revealed 298.5MPa. It was found that Al-7.0Si-0.4Mg alloy have good corrosion resistance in electrochemical polarization test.

Manufacturing and Properties of Metal Based Composite Produced By Friction Stir Processing (마찰교반프로세스를 이용한 금속기 복합소재 제조 및 특성)

  • Choi, Don-Hyun;Yeon, Yun-Mo;Jung, Seung-Boo
    • Journal of Welding and Joining
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    • v.30 no.5
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    • pp.27-33
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    • 2012
  • Friction stir processing (FSP), developed based on the basic principles of friction stir welding(FSW), a solid-state joining process originally developed for various metal alloys, is an emergingmetalworking technique that can provide localized modification and control of microstructures in near-surface layers of processed metallic components. The FSP causes intense plastic deformation, material mixing, and thermal exposure, resulting in significant microstructural refinement, densification, and homogeneity of the processed zone. The FSP technique has been successfully used for producing the fine-grained structure and surface composite, modifying the microstructure of materials, and synthesizing the composite and intermetallic compound in situ. In this review article, the current state of the understanding and development of FSP is addressed.

Effects of Solid Lubricants on Microsteucture and Mechanical Proerties of Sintered Valve Seats for Automobile Engine (자동차 엔진용 소결 밸브시트의 미세조직과 기계적 성질에 미치는 고체윤활제의 영향)

  • 최재기
    • Journal of Powder Materials
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    • v.6 no.2
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    • pp.163-170
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    • 1999
  • Engine valve seat is a functionally important part for maintaining engine performance. The progress of automotive technology has increased the severity of conditions to which it is exposed, especially as regards LPG fuel engines and turbocharger. Therefore, it requires excellent heat and wear resistance to meet the severe condition inside the engine. In the present study, effects of solid lubricants such as CaF$_2$, MnS and MoS$_2$ on microstructure and mechanical properties of sintered Fe alloys for valve srats have been investigated for the development of valve seat material with high temerature wear resistance. As a results of engine simulation test, 0.5 wt% CaF$_2$ specimen showed the most excellent property, but in the overall aspect of view valve recession has increased with increasing the amount of solid lubricants.

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Effect of Reverse Transformation on the Microstructure and Retained Austenite Formation of 0.14C-6.SMn Alloy Steel (0.14C-6.5Mn 합금강의 미세조직과 잔류오스테나이트 형성에 미치는 역변태처리의 영향)

  • Song, K.H.;Lee, O.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.4
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    • pp.253-258
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    • 2000
  • The present study aimed to develop the TRIP(transformation induced plasticity) aided high strength low carbon steel sheets using reverse transformation process. The cold-rolled 0.14C-6.5Mn steel was reverse-transformed by slow heating to intercritical temperature region and air cooling to room temperature. An excellant combination of tensile strength and elongation of $98.3kgf/mm^2$ and 44.4% appears. This combination comes from TRIP phenomena of retained austenite during deformation. The stability of retained austenite Is very Important for the good ductility and it depends on diffusion of carbon and manganese during reverse transformation. The air cooling after holding at intercritical temperature retards the formation of pearlite and provides the carbon enrichment in retained austenite, resulting the increase of elongation in cold-roiled TRIP steel.

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