• 제목/요약/키워드: Microstructure development

검색결과 655건 처리시간 0.024초

Properties of artificial lightweight aggregates made from waste sludge

  • Chiou, I.J.;Chen, C.H.
    • Computers and Concrete
    • /
    • 제8권6호
    • /
    • pp.617-629
    • /
    • 2011
  • In this investigation, reservoir sediment and municipal sewage sludge were sintered to form the artificial lightweight aggregates. The sintered aggregates were compared with the commercialized lightweight aggregates to in terms of potential alkali-silica reactivity and chemical stability based on analyses of their physical and chemical properties, leaching of heavy metal, alkali-silica reactivity, crystal phase species and microstructure. Experimental results demonstrated that the degree of sintering of an aggregate affected the chemical resistance more strongly than did its chemical composition. According to ASTM C289-94, all potential alkali-silica reactivity of artificial lightweight aggregates were in the harmless zone, while the potential reactivity of artificial lightweight aggregates made from reservoir sediment and municipal sewage sludge were much lower than those of traditional lightweight aggregates.

Development of Tungsten Dispersed Copper Based Alloy and its Physical Property

  • Mishima, Akira;Sakaguchi, Shigeya
    • 한국분말재료학회지
    • /
    • 제5권4호
    • /
    • pp.329-333
    • /
    • 1998
  • Copper-10 wt. % tungsten alloyed powder was obtained by co-reduction of mixed tungsten-trioxide and copper oxide powders at 973 K for 7.2 Ks. In the alloy obtained by pressure-assisted sintering of this co-reduced powder, ultra fine tungsten particles (about 100nm) were dispersed uniformly in the copper matrix. At room temperature, the hardness of this alloy was Hv151 and the electrical conductivity was 85% IACS. After annealing at 1173 K for 3.6 Ks, the hardness and electrical conductivity were Hv147 and 84% IACS, respectively, and were same as before annealing. It was confirmed that the hardness and electrical conductivity of this alloy were hardly influenced by annealing condition since the microstructure of this alloy is highly stabilized.

  • PDF

Sustainable use of mine waste and tailings with suitable admixture as aggregates in concrete pavements-A review

  • Gayana, B.C.;Chandar, Karra Ram
    • Advances in concrete construction
    • /
    • 제6권3호
    • /
    • pp.221-243
    • /
    • 2018
  • Utilization of mine waste rocks and tailings in concrete as aggregates will help in sustainable and greener development. The literature shows the potential use of iron ore tailings as a replacement of natural fine aggregates. As natural sand reserves are depleting day by day, there is a need for substitution for sand in concrete. A comprehensive overview of the published literature on the use of iron ore waste and tailings and other industrial waste in concrete is being presented. The effect of various properties such as workability, compressive strength, split tensile strength, flexural strength, durability and microstructure of concrete have been presented in this paper.

특수 가공된 셀룰로오스섬유보강 콘크리트의 초기 특성 (Properties of Specialty Cellulose Fiber Reinforced Concrete at Early Ages)

  • 원종필;박찬기
    • 한국콘크리트학회:학술대회논문집
    • /
    • 한국콘크리트학회 1999년도 봄 학술발표회 논문집(I)
    • /
    • pp.349-354
    • /
    • 1999
  • Specialty cellulose fibers processed for the reinforcement of concrete offer relatively high levels of elastic modulus and bond strength. The hydrophilic surfaces of specialty cellulose fibers facilitate their dispersion and bonding in concrete. Specialty cellulose fibers have small effective diameters which are comparable to the cement particle size, and thus promote close packing and development of dense bulk and interface microstructure in the matrix. The relatively high surface area and the close spacing of specialty cellulose fibers when combined with their desirable mechanical characteristic make them quite effective in the suppression and stabilization of microcracks in the concrete matrix. The properties of fresh mixed specialty cellulose fiber reinforced concrete and the contribution of specialty cellulose fiber to the restrained shrinkage crack reduction potential of cement composites at early age and theirs evaluation are presented in this paper. Results indicated that specialty cellulose fiber reinforcement showed an ability to reduce the total area significantly (as compared to plain concrete and polypropylene fiber reinforced concrete.

  • PDF

기체분리용 세라믹 복합분리막의 개발: I. 극미세 입자 실리카 졸의 코팅 특성 (Development of Ceramic Composite Membranes for Gas Separation: I. Coating Characteristics of Nanoparticulate SiO2 Sols)

  • 현상훈;;윤성필
    • 한국세라믹학회지
    • /
    • 제29권6호
    • /
    • pp.496-504
    • /
    • 1992
  • Alumina tubes suitable for the support of gas separation membranes have been prepared by the slipcasting technique. These supports have the average pore size of 0.1 ${\mu}{\textrm}{m}$ within the narrow distribution. The sol-gel dipcoating process of nanoparticulate sols is very sensitive to microstructure of the support, and the coating on the inside surface of the tube is found to be more successful than on the outside surface. Nanoparticulate silica sols (0.82 mol/ι) have been synthesized by an interfacial hydrolysis reaction between TEOS and high alkaline water. When coating an alumina tube with these sols, the minimum limits of the particle size and the aging time required for forming the coated gel layer at the given pH are provided. It is optimum to coat the support with less concentrated sols stabilized through aging for the appropriate time (more than 22 days) at the lower pH (pH 2.0) for producing a reproducible crack free thin film coating in composite membranes.

  • PDF

Microstructural Evolution and Dielectric Response Characteristics During Crystallization of Amorphous Pb(Fe2/3W1/3)O3

  • Kim, Nam-Kyung;David A. Payne
    • The Korean Journal of Ceramics
    • /
    • 제1권2호
    • /
    • pp.75-80
    • /
    • 1995
  • Development of phases, evolution of microstructures, and dielectric response characteristics of amorphous lead iron tungstates during crystabllization were investiageted. A series of mircographs showing the evolution sequence of microstructures is presented. Crystallization was observed to initiate from inside of the amorphous material. A cubic perovskite phase developed fully at $760^{\circ}C$ from amorphous state via intermediate metastable crystalline structures. Dielectric constant of amorphous PFM was totally insensitive to the temperature change around the Curie temperature of crystalline material. Sintered pellet, with relative density of 96% and an almost pore-free dense internal microstructure, could be prepared from amorphous powder.

  • PDF

반응결합 질화규소의 제조의 있어서 초기 질소분압의 영향 (The Effect of Initial Partial Pressure of Nitrogen on the Manufacturing of Reaction-Bonded Silicon Nitride)

  • 이근예;이준근;오재희
    • 한국세라믹학회지
    • /
    • 제21권1호
    • /
    • pp.51-59
    • /
    • 1984
  • In this paper mechanical properties of reaction-bonded silicon nitride are studied with the variation of initial nitrogen partial pressure. At 1, 25$0^{\circ}C$ the amount of nitridation and the nucleation of nitride increase linearly with the nitrogen partial pressure increase. After the nitridation is completed the density of nitride and modulus of rupture at room temperature are increased with the amount of nitridation. When the partial pressure of nitrogen is 0.5 atm the specimen show the optimum properties that is the highest density of nitride and modulus of rupture. Also the microstructure of $\alpha$-matte is deveoped very well at that pressure of nitrogen which contributes to the strength development of specimen. It is shown that with proper control of initial partial pressure of nitrogen high strength silicon nitride body can be manufactured for dynamic applications.

  • PDF

Texture Development in Liquid-Phase-Sintered β -SiC by Seeding with β -SiC Whiskers

  • Kim, Won-Joong;Roh, Myong-Hoon
    • 한국세라믹학회지
    • /
    • 제43권3호
    • /
    • pp.152-155
    • /
    • 2006
  • Silicon carbide ceramics seeded with 10-30 wt% SiC whiskers are fabricated by hot pressing and annealing. A quantitative texture analysis including calculation of the Orientation Distribution Function (ODF) is used for obtaining the degrees of preferred orientation of the fabricated samples. The microstructure and crystallographic texture are discussed with respect to the effect of ${\beta}-SiC$ whisker seeds on the resulting fracture toughness values. The SEM microstructures and the texture data reveal a correlation between texture and fracture toughness anisotropy.

증기 및 가열 조합양생에 의한 에폭시수지 혼입 모르타르의 강도 및 세공구조 (Strength Properties and Pore Structure of Epoxy-Modified Mortars under Steam and Steam/Heat Combined Curing)

  • 이재화;김완기
    • 한국건축시공학회:학술대회논문집
    • /
    • 한국건축시공학회 2011년도 추계 학술논문 발표대회
    • /
    • pp.107-108
    • /
    • 2011
  • The purpose of present study is to examine the application of effective curing to hardener-free epoxy-modified mortars. The epoxy-modified mortars are prepared with polymer-cement ratios, subjected to two types of curing conditions, and tested for compressive, flexural and tensile strengths. As a result, hardener-free epoxy-modified mortars with steam curing is markedly improved with increasing air-dry curing period. High strength development of the epoxy-modified mortars may be achieved by the dense microstructure by cement and the hardener of the epoxy resin in the mortars.

  • PDF

Mechanical Properties of Carbon/Carbon Composites Densified by HIP Technique

  • Manocha, L.M.;Warrier, Ashish;Manocha, S.;Banerji, S.;Sathiyamoorthy, D.
    • Carbon letters
    • /
    • 제6권1호
    • /
    • pp.6-14
    • /
    • 2005
  • The study of mechanical properties and fracture behaviour of carbon/carbon composites is significant to its application and development. These are dependent on microstructure and properties of reinforcing fibers and matrix, fiber/matrix interface and porosity/cracks present in the composites. In the present studies high-density carbon/carbon composites have been prepared using PAN and various pitch based carbon fibers as reinforcements and pitch as matrix with repeated densification cycles using high-pressure impregnation and carbonization technique. Scanning electron microscopy has been used to study the fracture behaviour of the highly dense composites and correlated with structure of the composites. The geometry of reinforcement and presence of unfilled voids/cracks was found to influence the path of crack propagation and thereby the strength of composites. The type of stresses (tensile or compressive) accumulated also plays an important role in fracture of composites.

  • PDF