• Title/Summary/Keyword: Microstructure development

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Development of high performance hybrid fiber reinforced concrete using different fine aggregates

  • Gupta, Hitesh;Bansal, Prem Pal;Sharma, Raju
    • Advances in concrete construction
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    • v.11 no.1
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    • pp.19-32
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    • 2021
  • In the present experimental study, the high performance hybrid fiber reinforced concrete (HPHFRC) is prepared using the Modified Andreasen and Andersen (A&A) particle packing model. Total of 16 trial mixes of HPHFRC with Indian standard sand (SS) and natural river sand (NS) are prepared to achieve the selection criteria (flow percent>150 and compressive strength>80 MPa). Based on the flow percent and compressive strength criteria, the selected mixes evaluated to study the effect of usage of natural river sand (NS) and the expensive Indian standard sand (SS) on the mechanical, durability, and microstructure property of designed HPHFRC. It has been found that the Modified A&A model is reliable to design the mix for HPHFRC with excellent mechanical, durability, and microstructure properties. In addition to that, a moderate difference in the mechanical and durability properties of NS contained HPHFRC and SS contained HPHFRC is found. Based on the obtained results of NS contained HPHFRC, it can be concluded that the use of natural river sand (NS) can be successfully adopted for the production of HPHFRC, resulted in a reduction of the production cost without compromising the excellent performance of HPHFRC.

Microscopic damping mechanism of micro-porous metal films

  • Du, Guangyu;Tan, Zhen;Li, Zhuolong;Liu, Kun;Lin, Zeng;Ba, Yaoshuai;Ba, Dechun
    • Current Applied Physics
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    • v.18 no.11
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    • pp.1388-1392
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    • 2018
  • Metal thin films are used widely to solve the vibration problem. However, damping mechanism is still not clear, which limits the further improvement of the damping properties for film and the development of multi-functional damping coating. In this paper, Damping microscopic mechanism of porous metal films was investigated at both macroscopically and microscopically mixed levels. Molecular dynamics simulation method was used to model and simulate the loading-unloading numerical experiment on the micro-pore and vacancy model to get the stress-strain curve and the microstructure diagram of different defects. And damping factor was calculated by the stress-strain curve. The results show that dislocations and new vacancies appear in the micro-pores when metal film is stretched. The energetic consumption from the motion of dislocation is the main reason for the damping properties of materials. Micro-mechanism of damping properties is discussed with the results of in-situ experiment.

Microstructural Evolution of a Cold Roll-Bonded Multi-Layer Complex Aluminum Sheet with Annealing

  • Jo, Sang-Hyeon;Lee, Seong-Hee
    • Korean Journal of Materials Research
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    • v.32 no.2
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    • pp.72-79
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    • 2022
  • A cold roll-bonding process using AA1050, AA5052 and AA6061 alloy sheets is performed without lubrication. The roll-bonded specimen is a multi-layer complex aluminum alloy sheet in which the AA1050, AA5052 and AA6061 sheets are alternately stacked. The microstructural evolution with the increase of annealing temperature for the roll-bonded aluminum sheet is investigated in detail. The roll-bonded aluminum sheet shows a typical deformation structure in which the grains are elongated in the rolling direction over all regions. However, microstructural evolution of the annealed specimen is different depending on the type of material, resulting in a heterogeneous microstructure in the thickness direction of the layered aluminum sheet. Complete recrystallization occurs at 250 ℃ in the AA5052 region, which is lower by 100K than that of the AA1050 region. Variation of the misorientation angle distribution and texture development with increase of annealing temperature also differ depending on the type of material. Differences of microstructural evolution between aluminum alloys with increase of annealing temperature can be mainly explained in terms of amounts of impurities and initial grain size.

Recent Progress in Dielectric Materials for MLCC Application (MLCC용 유전체 소재의 연구개발 동향)

  • Seo, Intae;Kang, Hyung-Won;Han, Seung Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.35 no.2
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    • pp.103-118
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    • 2022
  • With the recent increase in demand for electronic devices, multi-layer ceramic capacitors (MLCCs) have become the most important core component. In particular, the next-generation MLCC with extremely high reliability is required for the 4th industrial revolution and electric vehicle applications. Therefore, it is necessary to develop dielectric ceramic materials with high dielectric properties and reliability. During the decades, electrical properties of BaTiO3 based dielectric ceramics, which have been widely used in MLCC industrial field, have been improved by microstructure and defect chemistry control. However, electrical properties of BaTiO3 have reached their limits, and new types of dielectric materials have been widely studied. Based on these backgrounds, this report presents the recent development trends of BaTiO3-based dielectric materials for the next-generation MLCCs, and suggests promising candidates to replace BaTiO3 ceramics.

Strength and microstructure of composites with cement matrixes modified by fly ash and active seeds of C-S-H phase

  • Golewski, Grzegorz Ludwik;Szostak, Bartosz
    • Structural Engineering and Mechanics
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    • v.82 no.4
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    • pp.543-556
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    • 2022
  • Fly ash (FA) is the main additive to concretes currently produced. This substitute of ordinary Portland cement (OPC) have a positive effect on the structure and mechanical parameters of mature concrete. Unfortunately, the problem of using FA as the OPC replacement is that it significantly reduces the performance of concretes in the early stages of their curing. This limits the possibility of using this type of concrete, e.g., in the prefabrication, where it is required to obtain high strength composites after short periods of their curing. In order to minimize these negative effects, research has been undertaken to increase the early strength of the concretes with FA through the application of a specially dedicated chemical nanoadmixture (NA) in the form of seeds of the C-S-H phase. Therefore, this paper presents results of tests of modified concretes both with the addition of FA and with NA. The analyses were carried out based on the results of the macroscopic and microstructural tests in 5 time periods, i.e. after: 4, 8, 12, 24 and 72 hours. The greatest increase in mechanical strength parameters and rapid development of the basic matrix phases in composites in the first 12 hours of composites curing was observed.

Development of thermal conductivity model with use of a thermal resistance circuit for metallic UO2 microcell nuclear fuel pellets

  • Heung Soo Lee;Dong Seok Kim;Dong-Joo Kim;Jae Ho Yang;Ji-Hae Yoon;Ji Hwan Lee
    • Nuclear Engineering and Technology
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    • v.55 no.10
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    • pp.3860-3865
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    • 2023
  • A metallic microcell UO2 pellet has a microstructure where a metal wall is connected to overcome the low thermal conductivity of the UO2 fuel pellet. It has been verified that metallic microcell fuel pellets provide an impressive reduction of the fuel centerline temperature through a Halden irradiation test. However, it is difficult to predict the effective thermal conductivity of these pellets and researchers have had to rely on measurement and use of the finite element method. In this study, we designed a unit microcell model using a thermal resistance circuit to calculate the effective thermal conductivity on the basis of the microstructure characteristics by using the aspect ratio and compared the results with those of reported metallic UO2 microcell pellets. In particular, using the thermal conductivity calculated by our model, the fuel centerline temperature of Cr microcell pellets on the 5th day of the Halden irradiation test was predicted within 6% error from the measured value.

Disintegration process and micro mechanism of mudstone under dry-wet cycles

  • Ji Chen;Ruyu Huang;Xinyu Luo;Xin Liao;Qiang Tang
    • Geomechanics and Engineering
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    • v.36 no.1
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    • pp.9-18
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    • 2024
  • With the rapid development of highways and railways, series of traffic safety issues emerged because of mudstone disintegration. To research on the mechanism and further guarantee the stability and safety of transportation infrastructure built on or near mudstone formations, the mudstone disintegration test of mudstone was carried out based on mudstone and sandy mudstone. The element types, cementation characteristics and pore characteristics of the tested specimens were studied by means of Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD) and Image Pro Plus (IPP). The disintegration index of mudstone was approximately 1%, and even some specimens were difficult to be calculated, while the disintegration index of sandy mudstone is approximately 8.7%. According to the results, the two mudstones belong to grade II and III disintegration respectively, of which the sandy stone presents more extensive disintegration than mudstone. This phenomenon was distinguished that, the clay minerals of mudstone are approximately 25% more abundant than those of sandy mudstone, and the unit pore area is 20 ㎛2 larger, which result in different microstructure and water absorption capacities. In the liquid phase, the ions in the mudstone specimens were exchanged and combined with water molecules in the environment during the whole disintegration process. This results in continuous spalling and fragmentation of clay minerals, the emergence of secondary fractures, and the deepening of primary fractures.

Failure Analysis of a Ball in the Nuclear Fuel Exchanger

  • Kim, H.P.;Kim, D.J.;Hwang, S.S.;Joung, M.K.;Lim, Y.S.;Kim, J.S.
    • Corrosion Science and Technology
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    • v.4 no.5
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    • pp.211-216
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    • 2005
  • Failure analysis of the latch ram ball and the C-ram ball with the trade name AFBMA Gr. 50 Colmonoy No. 6, has been performed to identify the root cause of the failure. The study required the extraction of the both failed and normal balls from the nuclear fuel exchanger. Microstructures of both balls were examined after polishing and etching. Breaking tests of both the ball revealed similarity in cleavage surfaces. Fracture surfaces of both failed ball and normal ball after breaking test were examined with SEM and EDX. Microstructure of the ball revealed an austenite phase with coarse Cr rich precipitate. Indented marks observed on the surface of the failed ball are believed to be produced by overloading. In the light of the afore mentioned observations and studies, the failure mechanism of the ball in nuclear fuel exchanger seem to be caused by impact or mechanical overloading on ball.

The Effect of Uni-nanoadditive Manufactured Using RF Plasma Processing on Core-shell Structure in MLCC

  • Song, Soon-Mo;Kim, Hyo-Sub;Park, Kum-Jin;Sohn, Sung-Bum;Kim, Young-Tae;Hur, Kang-Heon
    • Journal of the Korean Ceramic Society
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    • v.46 no.2
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    • pp.131-136
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    • 2009
  • Radio frequency (RF) plasma treatment is studied for the size reduction and the spheroidization of coarse particles to change them into nano-sized powders of spherical shape in MLCC fields. The uni-nanoadditives manufactured by RF plasma processing for high dispersion have been investigated for the effect on core-shell structure in dielectrics of MLCC. Microstructures have been characterized using scanning electron microscope (SEM), transmission electron microscope (TEM) and Electron Probe Micro Analyzer (EPMA). We compared the distribution of core-shell grains between specimens manufactured using uni-nanoadditive and using mixed additive. In addition, the uniformity of rare earth elements in the core-shell structured grains was analyzed. It was shown, from TEM observations, that the sintered specimen manufactured using uni-nanoadditives had more dense small grains with well-developed core-shell structure than the specimen using mixed additives, which had a homogeneous microstructure without abnormal grain growth and shows broad temperature coefficient of capacitance (TCC) curves in all temperature ranges because of well dispersed additives.

Enhancement of Microstructural Homogeneity of W-Cu Pseudo-alloy by Adding W-Cu Composite Powder in Infiltration Process

  • Hong, Moon-Hee;Choi, Jae-Ho;Lee, Seong;Kim, Eun-Pyo;Noh, Joon-Woong;Lee, Sung-Ho;Kim, Young-Moo
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.948-949
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    • 2006
  • An infiltration technique using W-Cu composite powder has been developed to enhance microstructural uniformity of W-Cu pseudo-alloy. W-Cu composite powder, manufactured by reduction from $WO_3$ and CuO powder mixtures, were blended with W powder and then cold iso-statically pressed into a cylindrical bar under 150 MPa. The pressed samples were pre-sintered at $1300^{\circ}C$ for 1 hour under hydrogen to make a skeleton structure. This skeleton structure was more homogeneous than that formed by using W and Cu powder mixtures. The skeleton structures were infiltrated with Cu under hydrogen atmosphere. The infiltrated W-Cu pseudo-alloy showed homogeneous microstructure without Cu rich region

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