• Title/Summary/Keyword: Microstructure control

검색결과 504건 처리시간 0.057초

분산계 특성이 질화규소 미분의 과립특성 및 충진거동에 미치는 영향 (Effect of Suspension Property on Granule Characteristics and Compaction Behavior of Fine Si3Na4 Powder)

  • 이해원;오성록
    • 한국세라믹학회지
    • /
    • 제32권4호
    • /
    • pp.462-470
    • /
    • 1995
  • The characteristics of spray-dried granules are important for dry pressing operation since they have great influences on die-filling, compaction ratio, and resulting green microstructure. An attempt was made to control granule morphology and the packing structure of fine Si3N4 particles in granules by adjusting suspension property. Mercury porosimetry was used to characterize the pore structures of both granules and green compacts. Finally, the effects of particle packing structure in granules and green microstructure on sintering behavior were investigated.

  • PDF

Seed 첨가에 의한 Sr-Ferrite의 미세구조 제어 (Microstructure Control of Sr-Ferrite by Seed Addition)

  • 박준홍;신효순;이병교
    • 한국세라믹학회지
    • /
    • 제32권1호
    • /
    • pp.90-94
    • /
    • 1995
  • In Sr-ferrite system, it has been attempted to inhibit the abnormal grian growth using Sr-ferrite powders synthesized by molten salt method as the matrix and the seeds, respectively. At each sintering temperature, the addition of seed more than 15% suppressed the abnormal grain growth, and the uniform microstructure resulted. Particularly, at 12$25^{\circ}C$, it was observed that the maximum number of the abnormal grain growth nuclei was achieved since the abnormal grain growth was suppressed even by the addition of 10% seed.

  • PDF

Performance of self-curing concrete as affected by different curing regimes

  • El-Dieb, A.S.;El-Maaddawy, T.A.
    • Advances in concrete construction
    • /
    • 제9권1호
    • /
    • pp.33-41
    • /
    • 2020
  • In this study, polyethylene glycol (PEG) and polyacrylamide (PAM) have been used as self-curing agents to produce self-curing concrete (SC). Compressive strength, ultrasonic pulse velocity (UPV), bulk electrical resistivity, chloride ion penetrability, water permeability, and main microstructural characteristics were examined under different curing regimes, and compared to those of the control concrete mixture with no self-curing agents. One batch of a control mixture and one batch of a SC mixture were air-cured in the lab to act as non-water-cured samples. The water curing regimes for the control mixture included continuous water curing for 3, 7, and 28 days and periodical moist curing using wetted burlap for 3 and 7 days. Curing regimes for the SC mixtures included 3 days of water curing and periodical moist curing for 3 and 7 days. SC mixtures showed better microstructure development and durability performance than those of the air-cured control mixture. A short water curing period of 3 days significantly improved the performance of the SC mixtures similar to that of the control mixture that was water cured for 28 days. SC concrete represents a step towards sustainable construction due to its lower water demand needed for curing and hence can preserve the limited water resources in many parts of the world.

순 티타늄 박판의 파이버 레이저 용접시 결함 억제를 위한 연속의 출력 파형제어 특성(II) - 중첩부 길이변화에 따른 영향 - (The Characteristics of Continuous Waveshape Control for the Suppression of Defects in the Fiber Laser Welding of Pure Titanium Sheet (II) - The Effect According to Control of Overlap Weld Length -)

  • 김종도;김지성
    • Journal of Welding and Joining
    • /
    • 제34권6호
    • /
    • pp.69-74
    • /
    • 2016
  • Because the pure titanium has superior corrosion resistance and formability compared with different material, it is widely used as material of welded heat exchanger. When the welding of heat exchanger is carried out, certain area in which welding start and end are overlapped occurs. The humping of back bead is formed in the overlap area due to partial penetration. Thus in this study, the experiments were carried out by changing the length and wave shape of overlap area, and then the weldabiliay was evaluated through the observation of microstructure, the measurement of hardness and tensile-shear strength test in the overlap area. When overlap length was 9.8mm, humping bead was suppressed. The microstructure of overlap area coarsened and its hardness increased due to remelting. As a result of tensile-shear strength test in the overlap area according to applying the wave shape control, it was confirmed that the overlap area applied wave shape control had more excellent yield strength and ductility.

소형가스터빈 디스크의 얼간단조 (The Hot Forging of Small Size Gas Turbine Disks)

  • 차도진;송영석;김영득;김동권
    • 한국소성가공학회:학술대회논문집
    • /
    • 한국소성가공학회 2008년도 추계학술대회 논문집
    • /
    • pp.370-373
    • /
    • 2008
  • Small size gas turbine disk requires good mechanical strength and creep properties at high temperature. In this study, Waspaloy was used as a superalloy to satisfy these specifications. The control of microstructure was needed to satisfy material properties at high temperature. In order to do this, we studied forging conditions and material analysis. Therefore die and preform design conducted so that hot forged gas turbine disk could have a good microstructure. The die and preform shapes are designed with consideration of the predefined hydraulic press capacity and the microstructure of forging product. Also we carried out the hot compression test for Waspaloy in various test conditions. From these results, we obtained the forging conditions as material temperature, die velocity etc. To verify these forging conditions, we conducted FE simulations by means of the DEFORM 2D-HT. In this study, the hot closed die and preform designs were completed to offer high temperature material properties of a small size gas turbine.

  • PDF

Processing and Microstructure of Alumina Coated with $Al_2O_3$/SiC Nanocomposite

  • Ha, Jung-Soo;Kim, C-S.;D-S. Cheong
    • 한국결정성장학회:학술대회논문집
    • /
    • 한국결정성장학회 1997년도 Proceedings of the 12th KACG Technical Meeting and the 4th Korea-Japan EMGS (Electronic Materials Growth Symposium)
    • /
    • pp.19-22
    • /
    • 1997
  • The surface modificaion of alumina by $Al_2$O$_3$/SiC nanocomposite coating was studied in terms of processing and microstructure. A powder slurry of 5 vol% SiC composition was dipcoated onto presintered alumina bodies and pressurelessly sintered at 1$700^{\circ}C$ for 2 h in $N_2$. The used of organic binder and plasticizer in the slurry preparation, and the control of the density of presintered alumina body were found to be necessary to avoid cracking and warping during processing. The nanocomposite coating well bonded to the alumina body with thickness about 110 ${\mu}{\textrm}{m}$. The average grain size of coating (2 ${\mu}{\textrm}{m}$) was much finer than that of alumina body (13 ${\mu}{\textrm}{m}$). Fracture surface observations revealed mostly transgranular fracture for the coating, whereas intergranular fracture for the alumina body. Some pores (about 6%) were observed in the coating layer, although the alumina body showed fully dense microstructure.

  • PDF

SKH51의 반응고 상태에서의 가열 및 성형에 의한 부품 제조 (Fabrication of a Part by Heating and Forming in the Semi-solid State of the SKH51 Material)

  • 이상용
    • 열처리공학회지
    • /
    • 제27권3호
    • /
    • pp.127-132
    • /
    • 2014
  • The semi-solid metal forming process has been applied to realize a near-net shape fabrication of a high speed tool steel. A complicatedly shaped part out of SKH51 was successfully manufactured by introducing pertinent materials, tooling and processing conditions. A SKH51 billet with globular grains was heated at temperatures between 1300 and $1350^{\circ}C$ using high frequency induction heater to get semi-solid microstructure before high rate injection of mushy metal into a die cavity for the forming process. It was necessary to control the preheating of dies between 300 and $400^{\circ}C$ to maintain the homogeneous microstructure during the semi-solid metal forming process. Significant defects such as pores, high fraction of liquid fraction and segregation could be removed from the part by using air vents.

Dual Phase 전도성 CO2 분리막: 메커니즘, 미세구조 및 전기전도도 (Dual Phase Conductive CO2 Membranes: Mechanism, Microstructure, and Electrical Conductivity)

  • 이시우;유지행;우상국
    • 한국세라믹학회지
    • /
    • 제44권8호
    • /
    • pp.424-429
    • /
    • 2007
  • Novel conductive $CO_2$ membranes composed of dual phases, molten carbonates and electronic conducting ceramics, were investigated. As the microstructure control of electronic conducting ceramic supports is extremely important to keep the molten carbonates stable in the membranes by a capillary force applied by the pore structure of the supports, we have scrutinized the microstructure of the electronic conducting supports utilizing microscopic images and gas permeability measurement. From the evaluation of the electrical conductivities of the molten carbonates and the electronic conducting ceramic supports, we found that the ionic conductivity of the molten carbonates could determine $CO_2$ flux through the dual phase membranes if the surface exchange rate were relatively high enough.

Theory of Charged Clusters as New Understanding of Thin Film Growth

  • Hwang, Nong-Moon;Kim, Doh-Yeon
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 한국정보디스플레이학회 2002년도 International Meeting on Information Display
    • /
    • pp.147-152
    • /
    • 2002
  • A new theory of thin film growth was suggested, where charged clusters of nanometer size are generated in the gas phase and are a major flux for thin films. The existence of these hypothetical clusters was experimentally confirmed in the diamond and silicon CVD processes as well as in metal evaporation. These results imply new insights as to the microstructure control of thin films. Based on this new understanding, the low temperature deposition of crystalline and amorphous silicon can be approached systematically.

  • PDF