• Title/Summary/Keyword: Microstructure and mechanical properties

Search Result 2,018, Processing Time 0.035 seconds

폴리카보네이트 임시수복재료의 물성 평가 (Evaluation of physical properties of polycarbonate temporary restoration materials)

  • 김광윤;곽영훈;김희중
    • 구강회복응용과학지
    • /
    • 제36권3호
    • /
    • pp.168-175
    • /
    • 2020
  • 목적: 현재 상용화하여 사용되는 임시 수복물 재료와 새롭게 대두되는 재료들의 기계적 성질을 실험하고, 평가하는 것이다. 연구 재료 및 방법: Polymethyl methacrylate (PMMA) 2종, polyetheretherketone (PEEK), polycarbonate 4군의 고분자 재료들을 평가하였고, 표면 경도, 굴곡강도, 저작 시 마모도, 마모 양상 4가지의 기계적 물성을 실험하였다. 시편의 3축 굽힘 강도와 비커스 경도 테스트는 각각 만능 시험기를 사용하여 측정하였고, 저작 시험기를 이용하여 100,000회의 저작 시험 후 주사 전자 현미경으로 미세구조를 관찰하고 전, 후 무게를 비교하였다. 통계적 유의성 평가를 위해 kruskal wallis test를 시행하였다. 결과: PEEK의 굽힘 강도와 비커스 경도가 가장 높게 나타났으며, PC, PMMA-H, PMMA-T 순으로 나타났다. 미세구조 표면은 PEEK 군에서 거칠기 형태가 가장 적게 나타났으며, PC, PMMA-H, PMMA-T 순으로 적게 나타났다. 결론: PC는 임시치아 제작에 적용할 수 있는 충분한 기계적 성질을 가진 것으로 사료된다. 그러나, 실제 임상 적용을 위해서는 생체 친화성과 같은 추가적인 연구가 필요할 것으로 사료된다.

SM570TMC 강재의 재료특성에 관한 연구 (A Study on the Materials Characteristics of SM570TMC Plates)

  • 임성우;김요숙;장인화
    • 한국강구조학회 논문집
    • /
    • 제17권3호통권76호
    • /
    • pp.365-373
    • /
    • 2005
  • 건축물이 고층이 될 수록 고강도 강재의 사용요구가 증대된다. 그러나 고강도 강재는 일반 강재와는 전혀 다른 기계적 특성을 갖고 있다. 고강도 강재를 건축구조물에 적용하기 위해서는 비탄성 영역에서의 거동이 일반 강재와 동등한가를 확인해야 한다. 본 연구에서는 최근 국내에서 개발된 SM570TMC 강재를 건축구조용으로 사용하기 위해서 기계적 성질 및 용접부 특성을 평가하였다. 연속항복현상을 보이는 SM570TMC 강재는 판두께가 증대되어도 강도저감이 발생되지 않았으며, 최소 항복강도가 440MPa로 나타났다. 또한 판두께 방향으로 균일한 경도분포를 보였다. -5oC에서의 Charpy 충격값도 충분한 인성을 보였다. 용접성과 관련있는 탄소당량은 기존 건축구조용 강재보다 훨씬 낮았으며, 용접부 특성도 우수하였다.

자기펄스 압축성형법에 의한 다이아몬드 공구용 세그먼트 분말 성형 (Consolidation of Segment Powder for Diamond Tool by Magnetic Pulsed Compaction)

  • 윤종수;이정구;이민구;이창규;박문석;홍순직
    • 한국분말재료학회지
    • /
    • 제15권5호
    • /
    • pp.378-385
    • /
    • 2008
  • This article presents the successful consolidation of the mixed Co and Diamond powders for a drilling segment by the combined application of magnetic pulsed compaction (MPC) and subsequent sintering, and their properties were analyzed. Homogeneous hardness (Hv 220) and density (97%) of sintered bulks fabricated by MPC were obtained by the new technique, where higher pressure has been employed for short period of time than that of general process. A fine microstructure and homogeneous hardness in the consolidated bulk were observed without cracks. Relatively higher drilling speed of 9.61 cm/min and life time of 6.55 m were found to the MPCed specimens, whereas the value of the specimens fabricated by general process was 11.71 cm/min and 7.96 m, respectively. A substantial improvement of mechanical properties of segment was achieved through this study.

RRA 처리가 AA 7039 Al 합금의 기계적 성질과 내응력 부식성에 미치는 영향 (The Effect of the Retrogression and Reaging Treatments on the Mechanical Properties and Susceptibility to Stress Cracking of AA 7039 Al Alloy)

  • 전상조;김준수;김송희
    • 산업기술연구
    • /
    • 제7권
    • /
    • pp.49-58
    • /
    • 1987
  • To investigate the effect of the Retrogression and Reaging (RRA) treatment on the strength and the stress corrosion cracking in AA 7039 the measurement of hardness, tensile properties and the time to failure in a constant rate method were measured. Transmission electron microscope was used to examine the microstructural changes within graln and grain boundary. The results show that the RRA treatment of the T6 condition results in a significant increase in the time to failure without sacrifying the original T6 strength. It is believed that high density and even distribution of precipitates in RRA condition were observed within grain so that the RRA condition could have similar strength to the T6 condition. The presence of fine dispersion of semicohernt ${\eta}^{\prime}$ transition phase is also believed to contribute to that effect. Examination of the grain boundary microstructure shows that the RRA treatments increases significantly the average size of the grain boundary preciptates. It is suggested that the benificial effect of the RRA treatment on the susceptibility to SCC be due to the increase in the size of grain boundary precipitates obtained during the retrogression treatment.

  • PDF

에너지 제어 용착을 이용한 스테인리스 316L의 적층 특성 및 기계적 물성 평가 (Deposition Characteristics and Mechanical Properties of Stainless Steel 316L Fabricated via Directed Energy Deposition)

  • 양승원;이협;심도식
    • 한국기계가공학회지
    • /
    • 제20권6호
    • /
    • pp.59-69
    • /
    • 2021
  • Directed energy deposition (DED) is an additive manufacturing technology involving a focused high-power laser or electron beam propagating over the substrate, resulting in melt pool formation while simultaneously supplying metal powder to the melt pool area to deposit the material. DED is performed to repair and strengthen parts in various applications, as it can be easily integrate local area cladding and cross-material deposition. In this study, we characterize stainless steel 316 L parts fabricated via DED based on various deposition conditions and geometries to widen the application of DED. The deposition characteristics are investigated by varying the laser power and powder feed rate. Multilayer deposition with a laser power of 362 W and a powder feed rate of 6.61 g/min indicate a height closest to the design value while affording high surface quality. The microhardness of the specimen increases from the top to the bottom of the deposited area. Tensile tests of specimens with two different deposition directions indicate that horizontally long specimens with respect to a substrate demonstrate a higher ultimate tensile strength and yield strength than vertically long specimens with lower elongation.

Hydrogen Desorption and Absorption Properties of MgH2, LiBH4, and MgH2 + LiBH4 Composite

  • Park, Hye Ryoung;Song, Myoung Youp
    • 대한금속재료학회지
    • /
    • 제50권12호
    • /
    • pp.955-959
    • /
    • 2012
  • To increase the hydrogen storage capacity of Mg-based materials, a sample with a composition of 69.7 wt% $MgH_2$ + 30.3 wt% $LiBH_4$ was prepared by planetary ball milling under hydrogen. The absorption and desorption properties of unmilled $MgH_2$, unmilled $LiBH_4$, and 69.7 wt% $MgH_2$ + 30.3 wt% $LiBH_4$ were examined. At 648 K the unmilled $MgH_2$ desorbed 5.70 wt% for 60 min. The unmilled $LiBH_4$ desorbed 6.40 wt% H for 780 min at 673 K. The 69.7 wt% $MgH_2$ + 30.3 wt% $LiBH_4$ sample desorbed 3.10 wt% H for 50 min, and 3.32 wt% H for 300 min at 623 K at the second cycle.

MnO$_2$가 첨가된 PMW-PNN-PT-PZ계 세라믹스의 유전 및 압전 특성 (Dielectric and Piezoelectric Characteristics of PMW-PNN-PT-PZ Ceramics with addiction of MnO$_2$)

  • 박석환;윤광희;박정흠;김현재;박창엽
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 1996년도 춘계학술대회 논문집
    • /
    • pp.63-67
    • /
    • 1996
  • In this paper, effect of MnO$_2$ addition(0, 0.1, 0.2, 0.3, 0.5wt%) on the microstructure, dielectric and piezoelectric properties of [xPMW - (0.15-x) PNN] - [yPT-(0.85-y)PZ] (x=0, 0.01, 0.02, 0.03, 0.05, y = 0.35, 0.40, ().425, 0.45, 0.5) were investigated. When Ti/Zr ratio was 1.0, dielectric and piezoelectric properties were highest value. With PMW 2mol%, dielectric constant, dielectric constant (d$\_$33/, d$\_$31/) and electromechanical coupling factor (kp, k$\_$31/) were highest values of 1995, 479, 186(x10$\^$-12/C/N), 0.61, 0.36, respectively. With the addition of MnO$_2$, dielectric constant, electromechanical coupling factor (kp, k$\_$31/) were decreased, but with 0.3wt% MnO$_2$, eletromechanical coupling factor was highest value of 0.63. With the addition of MnO$_2$, mechanical quality(Q$\_$m/ was increased.

  • PDF

내마모용 SUS 소결재의 미세조직과 기계적 성질 (Microstructure and Mechanical Properties of SUS Alloy for Wear Resistant Materials)

  • 조권구;김보수;안인섭;허보영;양성철;김해섭
    • 분석과학
    • /
    • 제6권2호
    • /
    • pp.181-195
    • /
    • 1993
  • SUS(Stainless Steel) 분말을 이용하여 기존의 고가 내마모 소결부품을 대체할 수 있는 새로운 내마모재의 개발 가능성을 조사하였다. SUS 조성의 분말에 Cu, ZrC, C 및 Ti 등의 합금원소를 첨가하여 소결체의 밀도, 소결시의 수축률 및 경도의 변화를 조사하였다. 이러한 첨가원소의 영향 중에서 가장 뛰어난 기계적 성질을 나타낸 것은 Ti을 첨가한 SUS재였으며, 3% Ti 첨가시 기존의 내마모 소결 부품을 대체할 수 있는 수축률(6.5%), 밀도($7.35g/cm^3$) 및 경도(43HRC)를 보여 주었다.

  • PDF

ECAP 공정을 이용한 분말의 치밀화 (Powder Densification Using Equal Channel Angular Pressing)

  • 윤승채;서민홍;홍순익;김형섭
    • 한국분말재료학회지
    • /
    • 제13권2호
    • /
    • pp.124-128
    • /
    • 2006
  • In recent years, equal channel angular pressing (ECAP) has been the subject of intensive study due to its capability of producing fully dense samples having a ultrafine grain size. In this paper, the ECAP process was applied to metallic powders in order to achieve both powder consolidation and grain refinement. In the ECAP process for solid and powder metals, knowledge of the internal stress, strain and strain rate distribution is fundamental to the determination of the optimum process conditions for a given material. The properties of the ECAP processed solid and powder materials are strongly dependent on the shear plastic deformation behavior during ECAP, which is controlled mainly by die geometry, material properties, and process conditions. In this study, we investigated the consolidation, plastic deformation and microstructure evolution behaviour of the powder compact during ECAP.

Ni-Cr-Mo과 SM45C의 마찰용접특성(摩擦熔接特性)에 관한 연구(硏究) (A Study on the Properties in Friction Weldability of Ni-Cr-Mo and SM45C)

  • 임형택;민택기
    • 한국공작기계학회논문집
    • /
    • 제16권6호
    • /
    • pp.29-36
    • /
    • 2007
  • The present study examined the mechanical properties of the friction welding of Ni-Cr-Mo to SM45C. Friction welding was conducted at welding conditions of 2,000 rpm, friction pressure of 100MPa, friction time of 0.8, 1.0, 1.2, 1.4, 1.6, 1.8, 2.0 seconds, upset pressure of 150MPa, and upset time of 3.0 seconds. When the friction time was 1.6 seconds, the maximum tensile strength of the friction weld happened to be 1,020MPa, which is 120% of the base material's tensile strength(850MPa). At the same condition, the maximum shear strength was 438MPa, which is equivalent to 103% of the base material's shear strength(425MPa). At the same condition, the maximum vickers hardness was Hv490 at Ni-Cr-Mo nearby weld interface, which is higher Hv40 than condition of the friction time 0.8 seconds, and the maximum vickers hardness was Hv305 from weld interface of SM45C, which is higher Hv12 than condition of the friction time 0.8 seconds. The results of microstructure analysis show that the structures of two base materials have fined and rearranged along a column due to heating and axial force during friction, which has affected in raising hardness and tensile strength.