• Transactions of Materials Processing
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• v.7 no.2
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• pp.168-176
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• 1998

Hot workability of the AA5083 alloy ws investigated by torsion test at temperature ranges of $350{\sim}520^{\circ}C$ and strain rates of 0.5, 1.0, and 3.0/sec. The flow stress and hot ductility of the AA5083 alloy as a function of deformation variables such as temperature and train rate were studied. The microstructural evolution of the AA5083 alloy was studied in relation to Zener-Hollomon parameter (Z=exp( /RT) Also the hot restoration mechanism of the AA5083 alloy was small when Z val-ues were higher than $1.73{\times}1016/sec(370^{\circ}C,\;0.5/sec)$ In addition the difference microstructures during hot deformation. It was found that the increase of flow curves and deformed microstructures during hot deformation. It was found that the increase of flow stress of the AA5083 alloy was small when Z val-ues were higher than $1.73{\times}1016/sec(370^{\circ}C.\;0.5/sec)$. However under the low Z values less than $1.73{\times}1016/sec(370^{\circ}C,\;0.5/sec)$ the flow stress increase with increasing the Z values. The large dispersoid particles in the matrix grain decreased the flow strain of the AA5083 alloy because it caused the stress concentration during hot deformation.

• Journal of the Microelectronics and Packaging Society
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• v.10 no.3
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• pp.37-42
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• 2003

In soldering of electronic packaging, the research on substituting lead-free solder materials for Pb-Sn alloys has become active due to environmental and health concerns over the use of lead. The reliability of the solder joint is very important in the development of solder materials and it is known that it is related to wettability of the solder over the substrate and microstructural evolution during soldering. It is also highly affected by type and extent of the interfacial reaction between solder and substrate and therefore, it is necessary to understand the interfacial reaction between solder and substrate completely. In order to predict the intermetallic compound (IMC) phase which forms first at the substrate/solder interface during the soldering process, a thermodynamic methodology has been suggested. The activation energy for the nucleation of each IMC phases is represented by a function of the interfacial energy and the driving force for phase formation. From this, it is predicted that the IMC phase with the smallest activation energy forms first. The grain morphology of the IMC at the solder joint is also explained by the calculations which use the energy. The Jackson parameter of the IMC grain with a rough surface is smaller than 2 but it is larger than 2 in the case of faceted grains.

• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.2
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• pp.170-176
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• 2002

Nonlinear acoustic effect has been considered as an effective tool for the evaluation of material degradation. In this paper, the applicability of nonlinear acoustic effect to the evaluation of degraded 2.25Cr-1Mo steel is investigated. Firstly, artificial aging was performed to simulate the microstructural degradation in 2.25Cr-1Mo steel arising from long time exposure at $540^{\circ}C$. Secondly, ultrasonic nonlinear parameter was quantitatively measured by bi-spectrum and power spectrum. Nonlinear acoustic parameter from bi-spectrum was found to be clearly sensitive to the aging time.

• Advances in nano research
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• v.16 no.3
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• pp.289-301
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• 2024

In this work, an analytical model employing a new higher-order shear deformation beam theory is utilized to investigate the bending behavior of axially randomly oriented functionally graded carbon nanotubes reinforced composite nanobeams. A modified continuum nonlocal strain gradient theory is employed to incorporate both microstructural effects and geometric nano-scale length scales. The extended rule of mixture, along with molecular dynamics simulations, is used to assess the equivalent mechanical properties of functionally graded carbon nanotubes reinforced composite (FG-CNTRC) beams. Carbon nanotube reinforcements are randomly distributed axially along the length of the beam. The equilibrium equations, accompanied by nonclassical boundary conditions, are formulated, and Navier's procedure is used to solve the resulting differential equation, yielding the response of the nanobeam under various mechanical loadings, including uniform, linear, and sinusoidal loads. Numerical analysis is conducted to examine the influence of inhomogeneity parameters, geometric parameters, types of loading, as well as nonlocal and length scale parameters on the deflections and stresses of axially functionally graded carbon nanotubes reinforced composite (AFG CNTRC) nanobeams. The results indicate that, in contrast to the nonlocal parameter, the beam stiffness is increased by both the CNTs volume fraction and the length-scale parameter. The presented model is applicable for designing and analyzing microelectromechanical systems (MEMS) and nanoelectromechanical systems (NEMS) constructed from carbon nanotubes reinforced composite nanobeams.

• Computers and Concrete
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• v.34 no.2
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• pp.213-230
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• 2024

The use of waste tires and industrial wastes such as fly ash (FA) and ground granulated blast furnace slag (GGBS) in concrete is an important issue in terms of sustainability. In this study, the effect of parameters affecting the physical, mechanical and microstructural properties of FA/GGBS-based geopolymer concretes with waste rubber fiber was investigated. For this purpose, the effects of rubber fiber percentage (0.6%, 0.9%, 1.2%), binder (75FA25GGBS, 50FA50GGBS, 25FA75GGBS) and curing temperature (75 ℃, 90 ℃ and 105 ℃) were investigated. The Taguchi-Grey Relational Analysis (TGRA) method was used to obtain optimum parameter levels of rubber fiber geopolymer concrete (RFGC). The slump, fresh and hardened density, compressive strength, flexural strength, static and dynamic modulus of elasticity, ultrasonic pulse velocity (UPV) tests and scanning electron microscopy (SEM) analysis were performed on the produced concretes. The analysis of variance (ANOVA) method was used to statistically determine the effects of the parameters on the experimental results. A confirmation test was performed to test the accuracy of the optimum values found by the TGRA method. With the increase of GGBS percentage, the compressive strength of RFGC increased up to 196%. The increase in rubber fiber percentage and curing temperature adversely affected the mechanical properties of RFGC. As a result of TGRA, the optimum value was found to be A1B3C1. ANOVA results showed that the most effective parameter on the experimental results was the binder with 99% contribution percentage. It is understood from the SEM images that the optimum concrete had a denser microstructure and less capillary cracks and voids. For this study, the use of the TGRA method in multiple optimization has proven to provide very useful and reliable results. In cases where many factors are effective on its strength and durability, such as geopolymer concrete, using the TGRA method allows for finding the optimum value of the parameters by saving both time and cost.

• Corrosion Science and Technology
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• v.12 no.2
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• pp.93-101
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• 2013

The object of this work is to establish an electrochemical noise(EN) measurement technique combined with a direct current potential drop(DCPD) method for monitoring of localized corrosion cracking of nickel-based alloy, and to analyze its mechanism. The electrochemical current and potential noises were measured under various conditions of applied stress to a compact tension specimen in a simulated primary water chemistry of a pressurized water reactor. The amplitude and frequency of the EN signals were evaluated in both time and frequency domains based on a shot noise theory, and then quantitatively analyzed using statistical Weibull distribution function. From the spectral analysis, the effect of the current application in DCPD was found to be effectively excluded from the EN signals generated from the localized corrosion cracking. With the aid of a microstructural analysis, the relationship between EN signals and the localized corrosion cracking mechanism was investigated by comparing the shape parameter of Weibull distribution of a mean time-to-failure.

• Corrosion Science and Technology
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• v.18 no.6
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• pp.258-266
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• 2019

The objective of this study was to evaluate corrosion resistance of additive manufactured 316L stainless steel and alloy 625 powders widely used in corrosion resistance alloys of marine industry in comparison with cast alloys. Directed Energy Deposition (DED) method was used in this work for sample production. DED parameter adjustment was also studied for optimum manufacturing and for minimizing the influence of defects on corrosion property. Additive manufactured alloys showed lower corrosion resistance in seawater compared to cast alloys. The reason for the degradation of anti-corrosion property was speculated to be due to loss of microstructural integrity intrinsic to the additive manufacturing process. Application of heat treatment with various conditions after DED was attempted. The effect of heat treatments was analyzed with a microstructure study. It was found that 316L and alloy 625 produced by the DED process could recover their expected corrosion resistance when heat treated at 1200 ℃.

• Journal of Powder Materials
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• v.19 no.5
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• pp.379-384
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• 2012

This paper reports the microstructures and thermal conductivities of $ZrB_2$-SiC composite ceramics with size and amount of SiC. We fabricated sintered bodies of $ZrB_2$-x vol.% SiC (x=10, 20, 30) with submicron and nanosized SiC densified by spark plasma sintering. Microstructure retained the initial powder size of especially SiC, except the agglomeration of nanosized SiC. For sintered bodies, thermal conductivities were examined. The observed thermal conductivity values are 40~60 W/mK, which is slightly lower than the reported values. The relation between microstructural parameter and thermal conductivity was also discussed.

• The Korean Journal of Ceramics
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• v.2 no.1
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• pp.43-47
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• 1996

$RuO_2$ thin films deposited directly on Si substrate by RF magnetron sputtering method using $RuO_2$ target have been investigated. Special interest was focused on the effect of process parameter on the surface roughness of $RuO_2$ films. Crystallization behavior and electrical properties of the films deposited at $300^{\circ}C$ were superior to those deposited at room temperature. Metallic Ru phase was formed in pure Ar and this phase had resulted poor adhesion after post annealing process in oxidizing ambient. Microstructural analysis reveals that the size of the $RuO_2$ crystallites gets smaller and the surface becomes smoother as the $O_2$ partial pressure or film thickness decreases. Irrespective of the $O_2/Ar$ ratio, resistivity of $RuO_2$ films ranged in $50~70 {\mu}{\Omega}-cm$. As the film thickness decreases, there is a thickness where the resistivity rises abruptly. Such an onset thickness turned out to be dependent n the $O_2$/Ar ratio.

• Coupled systems mechanics
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• v.6 no.3
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• pp.251-272
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• 2017

In this paper, the thermo-mechanical vibration characteristics of functionally graded (FG) nanobeams subjected to three types of thermal loading including uniform, linear and non-linear temperature change are investigated in the framework of third-order shear deformation beam theory which captures both the microstructural and shear deformation effects without the need for any shear correction factors. Material properties of FG nanobeam are assumed to be temperature-dependent and vary gradually along the thickness according to the power-law form. Hence, applying a third-order shear deformation beam theory (TSDBT) with more rigorous kinetics of displacements to anticipate the behaviors of FG nanobeams is more appropriate than using other theories. The small scale effect is taken into consideration based on nonlocal elasticity theory of Eringen. The nonlocal equations of motion are derived through Hamilton's principle and they are solved applying analytical solution. The obtained results are compared with those predicted by the nonlocal Euler-Bernoulli beam theory and nonlocal Timoshenko beam theory and it is revealed that the proposed modeling can accurately predict the vibration responses of FG nanobeams. The obtained results are presented for the thermo-mechanical vibration analysis of the FG nanobeams such as the effects of material graduation, nonlocal parameter, mode number, slenderness ratio and thermal loading in detail. The present study is associated to aerospace, mechanical and nuclear engineering structures which are under thermal loads.