• Title/Summary/Keyword: Microstructural evolution

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Creep Behavior Analysis of High Cr Steel Using the Constitutive Model Based on Microstructure (미세조직기반 구성모델을 이용한 고크롬강의 크리프 거동 해석)

  • 윤승채;서민홍;백경호;김성호;류우석;김형섭
    • Transactions of Materials Processing
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    • v.13 no.2
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    • pp.160-167
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    • 2004
  • In order to theoretically analyze the creep behavior of high Cr steel at $600^{\circ}C$, a unified elasto-viscoplastic constitutive model based on the consideration of dislocation density is proposed. A combination of a kinetic equation describing the mechanical response of a material at a given microstructure in terms of dislocation glide and evolution equations for internal variables characterizing the microstructure provides the constitutive equations of the model. Microstructural features of the material such as the grain size and spacing between second phase particles are directly implemented in the constitutive equations. The internal variables are associated with the total dislocation density in a simple model. The model has a modular structure and can be adjusted to describe a creep behavior using the material parameters obtained from uniaxial tensile tests.

Effects of MgO Addition on Densification and Microstructural Development during Liquid-Phase Sintering of Alumina-Anorthite System (알루미나-anorthite 계의 액상소결에서 MgO의 첨가가 치밀화 및 미세구조에 미치는 영향)

  • 김호양;이정아;김정주
    • Journal of the Korean Ceramic Society
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    • v.36 no.11
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    • pp.1243-1251
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    • 1999
  • Densification behavior and microstructural evolution during the liquid-phase sintering of alumina-anorhite system were investigated as a function of MgO addition. When MgO component was added in either alumina or anorthite glass powder the aspect ratio of alumina grains decreased and concurrently the are of flat interface which was formed as a result of contact solid alumina gains rather increased. Consequently addition of MgO component in the Al2O3-amorthite system brought about suppression of the rearrangement of solid grains during the liquid phase sintering and then densification of specimens was also retarded.

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Ultrasonic Nonlinearity Parameter Due to Precipitate and Dislocation (석출물과 전위에 기인한 초음파 비선형성 파라미터)

  • Kim, Chung-Seok;Park, Ik-Keun
    • Journal of the Korean Society for Precision Engineering
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    • v.25 no.7
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    • pp.131-138
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    • 2008
  • The microstructural effects on the ultrasonic nonlinearity were investigated in isothermally degraded ferritic 2.25Cr-1Mo steel and low cycle fatigued copper. The variation in ultrasonic nonlinearity (${\beta}/{\beta}_0$) was interpreted as resulting from microstructural changes supported by the electron microscopy and X-ray diffraction, in addition to the mechanical test (Victor's hardness and ductile-brittle transition temperature). The ultrasonic nonlinearity of 2.25Cr-1Mo steel increased abruptly in the initial 1,000 h of degradation, and then changed little due to the coarsening of carbide and precipitation of stable $M_6C$ carbide during isothermal degradation. The ultrasonic nonlinearity of copper increased with the fatigue cycles due to the evolution of dislocation cell substructure.

Effect of Carbon Addition and Sintering Temperature on Densification and Microstructural Evolution of Sinter-Hardening Alloys Steels

  • Verma, N.;Anand, S.;Upadhyaya, A.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.557-558
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    • 2006
  • In all conventional sintered PM products, the pores present are of two types, primary and secondary. Primary pores forming during compaction and latter during sintering, due to penetration of formed liquid through the matrix grain boundary. Effect of carbon addition on diffusion of Cu in SH737-2Cu system was investigated. After compaction and transient liquid phase sintering at $1120^{\circ}C$ and $1180^{\circ}C$, samples were characterized for densification, showing rise in sintering density and reduction in swelling on carbon addition. Quantitative microstructural characterization (shape factor and pore size) revealed bimodal distribution for 0% carbon, more rounded pores for 0.9% carbon and higher sintering temperature, and pore coarsening at higher sintering temperature.

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IRRADIATION EFFECTS OF HT-9 MARTENSITIC STEEL

  • Chen, Yiren
    • Nuclear Engineering and Technology
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    • v.45 no.3
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    • pp.311-322
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    • 2013
  • High-Cr martensitic steel HT-9 is one of the candidate materials for advanced nuclear energy systems. Thanks to its excellent thermal conductivity and irradiation resistance, ferritic/martensitic steels such as HT-9 are considered for in-core applications of advanced nuclear reactors. The harsh neutron irradiation environments at the reactor core region pose a unique challenge for structural and cladding materials. Microstructural and microchemical changes resulting from displacement damage are anticipated for structural materials after prolonged neutron exposure. Consequently, various irradiation effects on the service performance of in-core materials need to be understood. In this work, the fundamentals of radiation damage and irradiation effects of the HT-9 martensitic steel are reviewed. The objective of this paper is to provide a background introduction of displacement damage, microstructural evolution, and subsequent effects on mechanical properties of the HT-9 martensitic steel under neutron irradiations. Mechanical test results of the irradiated HT-9 steel obtained from previous fast reactor and fusion programs are summarized along with the information of irradiated microstructure. This review can serve as a starting point for additional investigations on the in-core applications of ferritic/martensitic steels in advanced nuclear reactors.

The Effect of Addition of Ti and Co Elements on Microstructural control and Characteristics of Vacuum-casted Cu-25 wt%Cr Electrical Contact Material (Ti과 Co 첨가가 진공주조법으로 제조된 Cu-25 wt%Cr 난가공성 중고압용 전기접점 소재의 미세구조 제어 및 물성에 미치는 영향)

  • Hye Sung Kim
    • Journal of the Korean Society for Heat Treatment
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    • v.37 no.4
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    • pp.172-181
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    • 2024
  • In this study, the effect of addition of Ti and Co elements on microstructural evolution and characteristics of vacuum-casted Cu-25%Cr electrical contact material was investigated. The coarse and insoluble Cr phases with an average size of 300 ㎛ in commercial Cu-25%Cr alloy were reduced to tens of micrometers in vacuum casted Cu-25%Cr-X(X=Ti, Co) alloy, which can be interpreted as result controlling coarsening and the work-frame structure of the insoluble Cr phase by the formation of intermetallic compounds such as Cr2Ti or Cr0.5Co1.5Ti around the Cr phase As a result, the electrical properties such as weight loss and fusion resistance against the repeated arc generation of the electrical contact material as well as the mechanical properties were greatly improved.

Understanding the Plasticity of Amorphous Alloys Via the Interpretation of Structural Evolution Inside a Shear Band (비정질 합금의 전단띠 내부 구조변화 해석을 통한 소성의 이해)

  • Lee, Chang-Myeon;Park, Kyoung-Won;Lee, Byeong-Joo;Shim, Jae-Hyeok;Lee, Jae-Chul
    • Korean Journal of Materials Research
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    • v.19 no.5
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    • pp.276-280
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    • 2009
  • The effect of the initial packing structure on the plasticity of amorphous alloys was investigated by tracing the structural evolution of the amorphous solid inside a shear band. According to the molecular dynamics simulations, the structural evolution of the amorphous solids inside the shear band was more abrupt in the alloy with a higher initial packing density. Such a difference in the structural evolution within the shear band observed from the amorphous alloys with different initial packing density is believed to cause different degrees of shear localization, providing an answer to the fundamental question of why amorphous alloys show different plasticity. We clarify the structural origin of the plasticity of bulk amorphous alloys by exploring the microstructural aspects in view of the structural disordering, disorder-induced softening, and shear localization using molecular dynamics simulations based on the recently developed MEAM (modified embedded atom method) potential.

Prediction for the Dynamically Recrystallized Grain Size of AISI 304 (AISI 304 스테인리스강의 동적 재결정립 예측)

  • Kim S. I.;Yoo Y. C.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.05a
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    • pp.143-146
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    • 2001
  • The evolution of dynamic recrystallization (DRX) was studied with torsion test for AISI 304 stainless steel in the temperature range of $900-1000^{\circ}C$ and strain rate range of 0.05-5/sec. The evolution of DRX was investigated with microstructural analysis and change of flow stress curve slope. The investigation of serrated grain boundaries using electron back scattered diffraction (EBSD) analysis indicated that the nucleated new DRX grain size was similar to the size of bulging part. Before the steady state, the dynamically recrystallizing grains do not remain a constant size and gradually grow to the size of fully DRX grain at steady state. The calculation of grain size was based on $X_{DRX}$ and the assumption, which the nucleated DRX grains are growing to the steady state, continuously. It was found that the calculated results agreed with the microstructure of the alloy.

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Assessment of Grain Size Distribution in a Hammer-Forged Alloy 718 Disk (해머 단조된 Alloy 718 디스크의 결정립 분포 해석)

  • 염종택;박노광
    • Transactions of Materials Processing
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    • v.6 no.3
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    • pp.250-256
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    • 1997
  • Hammer forging was employed for Alloy 718 disk. The change in grain size during hot forging depends very much on dynamic recrystallization. The final grain size depends especially on the critical strain$($\varepsilon$_C)$/TEX> for dynamic recrystallization and Zener-Holloman parameter(Z). In this study, the critical strain$($\varepsilon$_C)$, the strain for 50 pct. recrystallization$($\varepsilon$_{0.5})$ and fraction of dynamic recrystallization(Xdyn) were measured by compression tests. FE simulation was also carried out ot predict the evolution of microstructure. The strain, strain rate and temperature distribution predicted by forging simulation can be effectively used to predict the distribution of grain sizes in the forged workpiece. The present model predictions showed an excellent agreement with the microstructural evolution of hammer-forged Alloy 718 disks.

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Analysis of Deformation and Microstructural Evolution during ECAP Using a Dislocation Cell Related Microstructure-Based Constitutive Model (전위쎌에 기초한 미세조직 구성모델을 이용한 ECAP 공정 시 변형과 미세조직의 진화 해석)

  • Kim H. S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.10a
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    • pp.207-210
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    • 2004
  • The deformation behavior of copper during equal channel angular pressing (ECAP) was calculated using a three-dimensional version of a constitutive model based on the dislocation density evolution. Finite element simulations of the variation of the dislocation density and the dislocation cell size with the number of ECAP passes are reported. The calculated stress, strain and cell size are compared with the experimental data for Cu deformed by ECAP in a modified Route C regime. The results of FEM analysis were found to be in good agreement with the experiments. After a rapid initial decrease down to about 200 nm in the first ECAP pass, the average cell size was found to change little with further passes. Similarly, the strength increased steeply after the first pass, but tended to saturate with further pressings. The FEM simulations also showed strain non-uniformities and the dependence of the resulting strength on the location within the workpiece.

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