• Title/Summary/Keyword: Microscopic observation

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The Effect of Carburization of the Fatigue of Low Carbon Steel (침탄(浸炭)이 저탄소강(低炭素鋼)의 피로(疲勞)에 미치는 영향(影響))

  • C.S.,Kang;C.M.,Suh
    • Bulletin of the Society of Naval Architects of Korea
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    • v.10 no.2
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    • pp.9-18
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    • 1973
  • The effects of carburization on the fatigue strength and cracks were studied. The fatigue phenomena of the carburized specimens were compared with noncarburized specimens those were either heat-treated or un-treated. The fatigue strength of these specimens were measured by rotating bending fatigue machine. The obtained results indicated that the fatigue strength of carburized specimens were increased ranging from 24-59 % than those of un-treated, and 22-38% than those of heat-treated. The Vickers hardness of carburized were also increased as much as 138-195% than those of un-treated, and 42-125% than those of heat-treated. The microscopic observation of the carburized specimens mostly composed of minute pearlitic structure at hard case exhibited to have more localized slip than those of non-carburized specimens.

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Antimicrobial Activities of Chopi(Zanthoxylum piperitum DC.) Extract (초피추출물의 항균특성)

  • 정순경;정재두;조성환
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.28 no.2
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    • pp.371-377
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    • 1999
  • In order to evaluate the antimicrobial function of natural herb extracts as antimicrobial agent or packaging material for the preservation of foods and greenhouse produce, the water extract of chopi (Zanthoxylum piperitum DC.) was prepared and its antimicobial activity was determined. In the paper disk test its antimicrobial activity was increased in proportion to its concentraion. The growth of microorganisms was completely inhibited above 500ppm of its concentration. It showed wide spectrum of thermal(40 to 180oC) and pH(4 to 10) stabilities. In the electronic microscopic observation(TEM and SEM) of microbial morphological change it showed to decrease the activation of physiological enzymes and to lose the function of cell membranes. Even in the activation test of galactosidase, it seemed to weaken the osmotic function of cell membranes remarkably in comparison with chloroform and its activation corresponded to 40~50% of toluene. Zanthoxylum piperitum DC. extract seemed to be an excellent antimicrobial for the inhibition of food borne microorganisms as well as the pre servation of greenhouse produces.

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The Study on the Material Behavior of Hybrid Composites (Hybrid 열가소성 복합재료의 재료거동에 관한 연구)

  • 조현철;이중희
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2000.11a
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    • pp.67-70
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    • 2000
  • This study was performed to investigate the material behavior of hybrid thermoplastic composites contained glass fiber and calcium carbonate. The composite was prepared with each combination ratio of calcium carbonate, and the content of glass fiber was fixed with 10% by weight. In order to investigate the material behavior for various combination ratio, tension test, flexural test, and impact test were performed. Microscopic observation were conducted to examine the fractured surface of specimen for tension test. And the material behavior of the hybrid thermoplastic composite immersed in salt water with definite time was investigated.

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An Investigation on Mitigation of Crystalization Fouling by Physical Water Treatment using Catalytic Material (촉매물질을 이용한 수처리 기법의 결정화 화울링의 저감에 관한 연구)

  • Kim, Sun-Do;Park, Bock-Choon;Baek, Byung-Joon;Kim, Cheol-Sang
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.1582-1588
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    • 2004
  • The present experimental study aimed to investigate the feasibility of physical water treatment (PWT) devices using catalytic materials to mitigation of crystalization fouling. Two PWT devices having different shape and material were used. The results from microscopic observation and SEM photographs demonstrate that the crystal structure of $CaCO_3$ is Argonite type without water treatment while Calcite type with water treatment, which clearly shows the feasibility of PWT techinque using catalytic materials to mitigate crystalization fouling. For 500 ppm solution, the fouling resistance decreased up to about 23% due to physical water treatment using catalytic materials. The results also reveal that if two more techniques are used simultaneously the additional effects could be expected.

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Formulation of Erythromycin Enteric-coated Pellets (에리스로마이신 장용성 펠렛의 제제 설계)

  • 이승우;박은석;지상철
    • YAKHAK HOEJI
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    • v.39 no.6
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    • pp.593-599
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    • 1995
  • Erythromycin was formulated as enteric-coated pellets in order to reduce degradation in stomach and gastromtestmal irritation, and to maximize the absorption in intestine followmg its oral administration. Core pellets were prepared using fluid-bed granulator with two different methods (powder layering and solvent spraying) and enteric-coated with two different coating polymers (HPMCP and Eudragit E30D). Physical characteristics md dissolution rates of core pellets and enteric-coated pellets were evaluated to optimize the formulation. Powder layering method resulted in shorter initial dissolution time than solvent spraying method, but physicochmical properties of the product were worse than solvent spraying method with respect to hardness, ftiability and density. The dissolution rate of the drug was increased with the addition of surfactants, showing concentration-dependence. The scanning electron microscopic observation of pellets revealed significant differences on the surface appearances prepared with solvent spraying method. The core pellet made with powder layering method had crystals on the surface, which resulted in poor physical properties of the pellets. The dissolution profiles of erythromycin pellets coated with HPMCP or Eudragit L30D were close to that of commercially available erythromycin enteric-coated product.

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Acoustic Emission on Failure Analysis of Rubber-Modified Epoxy Resin

  • Lee Deok-Bo
    • Fibers and Polymers
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    • v.5 no.4
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    • pp.259-263
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    • 2004
  • Rubber-modified epoxy resins have been employed as adhesive and matrix materials for glass and corbon-fiber composites. The behavior of fracture around a crack tip for rubber-modified epoxy resin is investigated through the acoustic emission (AE) analysis of compact tension specimens. Damage zone and rubber particles distributed around a crack tip were observed by a polarized optical microscope and an atomic force microscope (AFM). The damage zone in front of pre-crack tip in rubber-modified specimen $(15wt\%\; rubber)$ began to form at about $13\%$ level of the fracture load and grew in size until $57\%$ load level. After that, the crack propagated in a stick-slip manner. Based on time-frequency analysis of AE signals and microscopic observation of damage zone, it was thought that AE signals with frequency bands of 0.15-0.20 MHz and 0.20­0.30 MHz were generated from cavitation in the damage zone and crack propagation, respectively.

OBSERVATION WITH SCANNING ELECTRON MICROSCOPE ON THE EFFECT OF THREE DENTAL ETCHANTS IN THE ENAMEL SURFACE OF ALBINO RATS (치과용 부식제가 백서 법랑질 표면에 미치는 영향에 대한 주사전자현미경적 관찰)

  • Kwon, Taik-Kyun
    • Restorative Dentistry and Endodontics
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    • v.6 no.1
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    • pp.133-139
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    • 1980
  • In this experiment, etching was performed on the incisor enamel surfaces of 13 Albino rats, weighted about 130gm, with both 30% and 50% concentrations of the phosphoric, citric acids, and EDTA solution for 60 seconds. Immediately after extraction of the animal teeth, laboratory procedures for scanning electron microscopic observations were made and the author derived the following conclusions: 1. On the enamel surface treated with 30% and 50% phosphoric acids, all of the periphery, center of the enamel rods, and the enamel matrices were severely etched. 2. In the etched with 30% citric acid group, only the small part of the enamel rods were etched out. In case of 50% citric acid the periphery, center of enamel rods were partially or entirely etched, and the intermatrix spaces were widened. 3. In the 30% and 50% of the EDTA etched groups, the periphery of the enamel rods explicitely were etched, and the spaces between matrices were widened.

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Study on the Improvement of the Reliability of Al-Cu Connections in Power Distribution Systems(II) (송배전용 Al-Cu 접속금구의 신뢰도 향상에 관한 연구(II) 압축형 및 폭발용접형 접속금구의 내식성 비교)

  • Ha, Yoon-Cheol;Bae, Jeong-Hyo;Ha, Tae-Hyun;Lee, Hyun-Goo;Kim, Dae-Kyeong
    • Proceedings of the KIEE Conference
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    • 2003.11a
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    • pp.370-372
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    • 2003
  • As there expands the usage of Al-Cu connections to interface aluminum and copper in power distribution systems, efforts to mitigate the mechanical, electrical or electro-chemical degradation are widely spreading. The explosive bending technology, in particular, has been thought as a countermeasure for the degradation. In this paper, electrochemical analysis and optical microscopic observation are carried out in order to compare the corrosion resistivities of the commercial compression type bimetallic sleeve and the explosion type bimetallic sleeve. The results show that the explosive bonding technology can prevent the interfacial corrosion caused by the formation of crevices and pits as well as from galvanic potential difference.

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Inactivation of Listeria monocytogenes in Brine and Saline by Alternating High-Voltage Pulsed Current

  • Lee, Mi-Hee;Han, Dong-Wook;Woo, Yeon-I.;Uzawa, Masakazu;Park, Jong-Chul
    • Journal of Microbiology and Biotechnology
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    • v.18 no.7
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    • pp.1274-1277
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    • 2008
  • The inactivating efficiency of alternating high-voltage pulsed (AHVP) current was investigated in brine (20 w/v% NaCl) and saline (0.9 w/v% NaCl) inoculated with $1\times10^7$ cells/ml of Listeria monocytogenes. AHVP current at 12 V with 1 pulse completely inactivated L. monocytogenes in brine within 3 ms, while the bacteria in saline were fully inactivated by 10-pulsed electric treatment at 12 V within the same time. Electron microscopic observation demonstrated substantial structural damage of electrically treated L. monocytogenes in brine. These results suggest that AHVP treatment would be effective for the rapid and complete inactivation of L. monocytogenes in brine or saline solution.

Fault Train Construction Based on Shallow Reasoning Strategy (경험기반추론 전략을 이용한 고장트레인 구축)

  • Bae, Yong-Hwan
    • Journal of the Korean Society of Safety
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    • v.20 no.3 s.71
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    • pp.19-26
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    • 2005
  • There are three reasoning method in fault diagnosis process. The shallow reasoning is based on the experiential knowledge and deep reasoning is based on physical model. Hybrid reasoning is mixing two type reasoning. This study describes about fault train embodiment of screw type air compressor that is used widely in industrial facilities by using various experimental method and shallow reasoning. We investigate macroscopic failure cause of air compressor through naked eye observation and then microscopic failure cause by various experimental method. We composed fault train with fault knowledge based on empirical data and scientific data that is acquired through several experiments. It is possible to analysis system reliability and failure rate with these fault train.