• 제목/요약/키워드: Micrography

검색결과 36건 처리시간 0.031초

Al-Li-Cu-Zr합금의 시효에 따른 인장파괴모드변화에 미치는 미세조직의 영향 (The Influence of Microstructures on the Change of Monotonic Tensile Fracture Mode in Al-Li-Cu-Zr Alloy with Ageing)

  • 정동석;이수진;조현기
    • 열처리공학회지
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    • 제9권3호
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    • pp.212-218
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    • 1996
  • To clarify the influence of precipitation microstructure and inclusion on the monotonic tensile fracture behaviors in 2090 alloy aged at $180^{\circ}C$, the detailed measurement of hardness, tensile strength, elongation and the observation of scanning electron micrography, transmision electron micrography have been carried out. The transgranular shear ductile fracture has been observed in specimen quenched after solution treatment at $500^{\circ}C$ for 45min. While the under-aged specimen was fractured in both transgranular shear ductile and intergranular fracture mode, the fracture mode of peak-aged and over-aged alloy was predominantly intergranular fracture. The fracture behavior of each ageing condition was influenced by the change of precipitation microstructural features. In the case of peak-aged and over-aged alloys, the coarse and heterogeneous slip band caused by both shearable nature of the ${\delta}^{\prime}(Al_3Li)$ precipitates and PFZ along the high angle grain boundary aid the localization of deformation, resulting in low energy intergranular fracture. It was also estimated that the fractured T-type intermetallic phases (inclusion) and the equilibrium ${\delta}$(AlLi) phases which were formed at grain boundaries palyed an important role in promoting intergranular fracture mode.

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연소중 미분탄의 단면관측 (Cross-section micrography of burning pulverized coal particles)

  • 한재현;최상민
    • 대한기계학회논문집
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    • 제13권4호
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    • pp.717-725
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    • 1989
  • 본 연구에서는 미분탄의 연소과정을 파악하기 위하여 메탄-공기 예혼합 화염에서 연소중인 석탄입자를 단계별로 여러 위치에서 순간 냉각에 의해 채취한 후 단면을 관측함으로써 미분탄 연소과정의 해석을 시도하였다. 산소 함유량이 미분탄 연소에 미치는 영향을 고려하기 위하여 반응로에서의 연소 조건을 바꾸어 보았다. 또한 미분탄 연소과정의 이해를 돕기 위해 비분탄을 도가니에 넣어 전기 로에서 가열하여 얻은 챠르와 공기중에서 가열하여 얻은 회(ash)에 대한 단면을 관측하였다. 시험용 미분탄은 국내 발전소 등지에서 대량 소비되는 수입 유연탄을 사용하였다.

건조방법과 한약재 추출물 첨가가 육포의 미세구조에 미치는 영향 (Effects of Drying Method and Medicinal Herb Extract Addition on the Microstructure of Beef Jerky)

  • 박추자;김미림;박찬성
    • 한국식품저장유통학회지
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    • 제16권6호
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    • pp.875-883
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    • 2009
  • 본 연구의 목적은 육포의 제조방법이 품질특성에 미치는 영향을 규명하기 위하여 기본 양념(간장, 물엿, 참기름, 정종, 마늘, 양파, 배즙)에 설탕(A), 감초(B), 3종류의 향신료(정향;C, 회향;D, 청양고추;E) 추출물과 여러 추출물을 혼합 첨가(F)한 6군으로 나누어 쇠고기를 절인후, 열풍건조와 송풍건조하는 육포의 제조과정에서 근육의 미세구조 변화를 주사전자현미경(SEM)과 투과전자현미경(TEM)으로 관찰하였다. 투과전자현미경(TEM)으로 관찰한 결과, 쇠고기는 액틴과 미오신의 근육라인과 근원섬유가 평행으로 발달되어 있었고 세포의 미토콘드리아와 내막을 볼 수 있었으나 절임과정에서 근섬유가 절단되고 근육라인의 분해 및 세포 구조물들의 퇴행이 일어났다. 주사전자현미경(SEM)으로 관찰한 결과, 자연건조한 한약재 추출물 첨가 육포는 근원 섬유와 공간구조가 남아있고 육질이 보존되어 있었으나 열풍건조한 육포는 근원섬유의 배열과 공간구조가 전혀 관찰되지 않았다. 이상의 주사전자현미경과 투과전자현미경으로 육포의 미세구조를 관찰한 결과에서 한약재 추출물은 근섬유의 결을 보존하는데 도움이 되며 송풍건조는 열풍 건조에 비하여 육포의 물성을 좋게 함으로써 품질을 향상시킬 수 있는 건조방법으로 생각된다.

재배양식(栽培樣式)에 따른 벼와 피의 생장(生長) 및 해부형태학적(解剖形態學的) 차이(差異) - III. 재배양식(栽培樣式)에 따른 벼와 피간(間의) 미세구조(微細構造) 차이(差異) (Morphological Characteristics of Growth of Rice and Barnyardgrass under Various Cropping Patterns - III. Difference in Stem Surface and Ultrastructures)

  • 천상욱;구자옥;이영만
    • 한국잡초학회지
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    • 제14권2호
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    • pp.144-155
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    • 1994
  • 재배양식(栽培樣式)을 달리하여 생육하는 벼와 피의 줄기 표면(表面) 및 최외곽(最外廓) 표피세포(表皮細胞)의 미세구조(微細構造) 차이(差異)를 파악하여 제초제(除草劑) 사용원리(使用原理)와 잡초방제요점(雜草防除要點)을 연관지어 밝히고자 주사전자현미경(走査電子顯微鏡)(SEM)과 투사전자현미경(投射電子顯微鏡)(TEM)을 이용(利用)하여 연구(硏究)한 결과(結果)를 요약(要約)하면 다음과 같다. 1. 줄기의 표면구조(表面構造) 차이(差異) 가. 건답조건(乾畓條件)에서는 표면(表面)벼와 토중(土中)벼간에 차이(差異)가 인정되지 않았으나 표면(表面)벼가 토중(土中)벼에 비하여 더 매끄러운 표면(表面)을 형성하였다. 건답직파(乾畓直播)는 최외부층의 납질(蠟質)구조가 아령모양(啞鈴模樣)을 하고 있으며 기공열(氣孔列)과 규산세포열(硅酸細胞列)이 있으나 피는 납질(蠟質)이 실모양이며 모용, 기공열(氣孔列) 및 규산세포열(硅酸細胞列)은 없었다. 나. 담수직파(湛水直播)된 벼 줄기표면(表面)은 미분화(未分化)된 조직(組織)의 상태(狀態)를 나타내며 모용, 규산세포열(硅酸細胞列) 및 기공열(氣孔列)이 발견되지 않았다. 다. 이앙후(移秧後) 8일(日) 및 25일(日)된 묘(苗)의 표면구조(表面構造)는 건답직파(乾沓直播)벼의 구조(構造)보다 기공열(氣孔列), 규산세포열(硅酸細胞列), 납질(蠟質) 및 모용의 발달(發達)이 더 많았다. 2. 최외부(最外部) 세포벽구조(細胞壁構造) 차이(差異) 가. 최외부(最外部) 납질(蠟質)두께는 이앙(移秧)벼가 가장 두꺼웠고 건답(乾沓)벼가 피나 담수(湛水)벼보다 2~6배 두꺼웠다. 나. 벼의 큐티클층(層)은 이앙(移秧)벼와 건답(乾沓)벼보다는 담수(湛水)벼가 두꺼웠으나 반대로 담수(湛水)피보다는 건답(乾沓)피가 두꺼웠고 전반적으로는 피보다 벼가 더 두꺼웠다. 다. 세포벽(細胞壁)은 이앙벼가 가장 두꺼웠고 피보다는 벼가, 건답(乾沓)벼보다 담수(湛水)벼가 그리고 건답(乾沓)피보다 담수(湛水)피가 두꺼웠다.

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닭혈청(血淸)에 의한 면양적혈구(緬羊赤血球)의 용혈(溶血)에 관한 연구(硏究) (Studies on hemolytic reaction of normal chicken serum and sheep erythrocytes)

  • 서익수
    • 대한수의학회지
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    • 제14권1호
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    • pp.77-90
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    • 1974
  • Hemolytic reaction of normal fresh chicken serum on sheep erythrocytes was studied and the following experimental results were obtained and summarized. 1. Chicken sera, 258 (78%) out of 344 samples showed hemolytic activity on sheep erythrocytes. 2. Distribution of a different hemolytic titer of chicken sera was not dependent to sex and age difference of test chicken. 3. Hemolytic activity of serum component obtained from normal fresh chicken was heat inactivated at $56^{\circ}C$. 30 minutes heating. 4. The most enhanced hemolytic activity of chicken serum on sheep erythrocytes was observed at the incubation temperature of $46^{\circ}C$. 5. The most effective pH for the hemolytic reaction of chicken serum on sheep erythrocytes was observed at 7.0, and pH 6.0 or 8.5 resulted less or no hemolysis. 6. Hemolytic reaction of chicken serum and sheep erythrocytes required Mg⧻ and Ca⧻ ions as, co-factor, and the former was required more compared to the latter. 7. Hemolytic activity of chicken serum was observed in ChC 2, 4 fraction but not in ChC 1, 3, ChC 3, 4, ChC 1, 2, 4 and ChC 1, 2, 3 fractions. 8. In electron micrography, morphological changes of sheep erythrocyte membrane by normal chicken serum was similar to that of immune hemolysis: that was, the hemolytic hole was circular and it was surrounded with a white ring. 9. Electron micrography of morphological changes on sheep erythrocyte membrane indicated that the size of hemolytic hole and white ring were functional to the chicken serum concentration used and reaction time.

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공단지역에서 대기중 총 부유분진의 입자크기 분포와 화학적 성분에 관한 분석과 연구 (A Study on the Size Distribution and Chemical Composition of total Suspended Particulates at Industrial Region)

  • 박흥재;이성욱;박원우
    • 한국환경과학회지
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    • 제2권3호
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    • pp.201-206
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    • 1993
  • The concentration of Total Suspended Particulates(T.S.P), size distribution of suspended particulates, and soluble anions of T.S.P in atmosphere of industrial region in Busan were investigated. T.S.P was measured by High-Volume Air Sampler and particle size distribution was measured by Anderson Air Sampler. We analyzed the chemical component of the T.S.P by ion Chromatography and measure4 the shape and size of T.S.P by Scanning Electron Micrography The small size of T.S.P mainly exist in industrial region, but the large size of T.S.P mainly exist in residentail area.

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알루미늄 카바이드 입자로 미세화된 Mg-Al 주조합금의 진동감쇠능 (Damping Capacity of Mg-Al Casting Alloy Refined by Aluminum Carbide Particles)

  • 전중환
    • 열처리공학회지
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    • 제20권6호
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    • pp.293-298
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    • 2007
  • Influences of aluminum carbide ($Al_4C_3$) addition on microstructure and damping capacity of Mg-3%Al casting alloy have been investigated based on experimental results of optical micrography, scanning electron microscopy with energy-dispersive spectrometry analysis and damping capacity measurement at RT. The addition of $Al_4C_3$ particles results in an efficient grain refinement. The damping capacity shows an increasing tendency with an increase in $Al_4C_3$ content. The damping value associated with $Al_4C_3$ particles is linearly dependent on the volume fraction of $Al_4C_3$ particles to the 2/3 power, $f_{2/3}$, which corresponds to the total surface area of the particles.

Microbiologically - Enhanced Crack Remediation (MECR)

  • Bang Sookie S.;Ramakrishnan V.
    • 한국미생물학회:학술대회논문집
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    • 한국미생물학회 2001년도 추계학술대회
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    • pp.26-36
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    • 2001
  • A novel approach of microbiologically-enhanced crack remediation (MECR) has been initiated and evaluated in this report. Under the laboratory conditions, Bacillus pasteurii was used to induce $CaCO_3$ precipitation as the microbial urease hydrolyzes urea to produce ammonia and carbon dioxide. The ammonia released in surroundings subsequently increases pH, leading to accumulation of insoluble $CaCO_3$. Scanning electron micrography (SEM) and x-ray diffraction (XRD) analyses evidenced the direct involvement of microorganisms in $CaCO_3$ precipitation. In biochemical studies, the primary roles of microorganisms and microbial urease were defined. Furthermore, the role of urease in $CaCO_3$ precipitation was characterized utilizing recombinant Escherichia coli that encoded B. pasteurii urease genes in a plasmid. Microorganisms immobilized in polyurethane (PU) polymer were applied to remediate concrete cracks. Although microbiologically- induced calcite precipitation enhanced neither the tensile strength nor the modulus of elasticity of the PU polymer, cement mortar whose crack was remediated with the cemaden polymer showed a significant increase in compressive strength. Through detailed investigation, MECR showed an excellent potential in cementing cracks in granite, concrete, and beyond.

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연소중 미분탄의 발광 분석 및 입자 채집 관찰 (Experimental Investigation of Burning Pulverized Coal Particles: Emission Analysis and Observation of Particle Sample)

  • 김대희;최상민
    • 한국연소학회지
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    • 제15권2호
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    • pp.19-26
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    • 2010
  • Combustion behavior of pulverized coal particles in a post-combustion gas reactor was investigated. Radiation emission from coal particles were analyzed by direct photograph and $CH^*$ radical chemiluminescence intensity. Coal particles were sampled during the combustion and were observed by scanning electron microscopy (SEM) and cross section micrograpy technique. Two coal types(one bituminous and one subbituminous coals typically used in the Korean power plants) were tested at typical combustion environment. Gas flow conditions were controlled to represent temperature and oxygen concentration. Experimental data were discussed along with conceptual descriptions of pulverized coal combustion, where particle heat-up, release and combustion of volatiles, and char combustion were sequentially progressed.

Characterization of Two Urease-Producing and Calcifying Bacillus spp. Isolated from Cement

  • Achal, Varenyam;Mukherjee, Abhijit;Reddy, M. Sudhakara
    • Journal of Microbiology and Biotechnology
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    • 제20권11호
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    • pp.1571-1576
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    • 2010
  • Two bacterial strains designated as CT2 and CT5 were isolated from highly alkaline cement samples using the enrichment culture technique. On the basis of various physiological tests and 16S rRNA sequence analysis, the bacteria were identified as Bacillus species. The urease production was 575.87 U/ml and 670.71 U/ml for CT2 and CT5, respectively. Calcite constituted 27.6% and 31% of the total weight of sand samples plugged by CT2 and CT5, respectively. Scanning electron micrography analysis revealed the direct involvement of these isolates in calcite precipitation. This is the first report of the isolation and identification of Bacillus species from cement. Based on the ability of these bacteria to tolerate the extreme environment of cement, they have potential to be used in remediating the cracks and fissures in various building or concrete structures.