• Title/Summary/Keyword: Micro-structural Property

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Investigation of Structural Change of DLC Coating during Frictional Wear by Raman Spectroscopy (라만 분광법을 활용한 마모 중 DLC 코팅의 구조적 변화 조사)

  • Kim, Song-Hee;Jang, Jae Cheol
    • Journal of Surface Science and Engineering
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    • v.52 no.1
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    • pp.16-22
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    • 2019
  • The structural change of DLC coatings during long-term wear test and dicing test under the low loading condition was investigated. DLC coatings were applied for the precision injection molds of a modified SNCM steel for the extension of life and the micro-diamond blades for the high cutting efficiency and the increase in life. A ball-on-disc wear tests in the mold steel and a dicing tests in the micro-diamond blades were conducted to understand degradation of DLC coatings. The degradation of DLC coatings for the injection mold steel and the micro-diamond blades during the wear and dicing tests were studied with Raman Spectroscopy. Raman peaks were divided two bands(D band and G band) to study the degradation process of DLC structure. By the wear test, polished condition of wear marks were observed to be maintained until 10 hrs of wear test period is given, but small striation marks appeared in 20 hours wear test. It was observed that $I_D/I_G$ ratios changed as the degradation of DLC coatings is proceeded during the wear tests and the dicing tests. It is suggested that the change in $I_D/I_G$ value possibly reflected from the composition of $sp^2$ and $sp^3$ bondings in DLC layers relevant to the change in mechanical and physical property.

Characterization of microstructures and electrical properties of insulating thin films deposited by PECVD and RF magnetron sputtering (화학기상증착 및 마그네트론 스퍼터링 방법으로 증착된 절연박막의 물성 분석 및 전기적 특성)

  • Yun, Sang-Han;Lee, Jae-Yup;Park, Chang-Kyun;Seo, Soo-Hyung;Kim, Yong-Sang;Park, Jin-Seok
    • Proceedings of the KIEE Conference
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    • 1999.07d
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    • pp.1707-1709
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    • 1999
  • Insulating thin films for strain gauge application, such as $SiO_2$ single layers and $SiO_2/Si_3N_4$ multilayers, are deposited by using both PECVD and RF magnetron sputtering techniques. Micro-structural analysis and electrical characterization are carried out on those films. It has been observed that PECVD films have a smoother surface and a denser micro-structure than sputter films. It should be also found out that the electrical insulation property of $SiO_2$ film can be significantly improved by adding the $Si_3N_4$ layer.

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Effects of nano-silica and micro-steel fiber on the engineering properties of ultra-high performance concrete

  • Hakeem, Ibrahim Y.;Amin, Mohamed;Abdelsalam, Bassam Abdelsalam;Tayeh, Bassam A.;Althoey, Fadi;Agwa, Ibrahim Saad
    • Structural Engineering and Mechanics
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    • v.82 no.3
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    • pp.295-312
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    • 2022
  • This study investigates the effects of nano silica (NS) and micro steel fiber on the properties of ultra-high-performance concrete (UHPC). The experimental consists of three groups, each one with five percentages of NS content (0%, 2%, 4%, 6% and 8%) in addition to the 20% silica fume and 20% quartz powder proportioned according to the weight of cement added to the mixtures. In addition, three percentages of micro steel fibers (0%, 1% and 2%) were considered. Different mixtures with varying percentages of NS and micro steel fibers were prepared to set the water-to-binder ratio, such as 0.16% and 1.8% superplasticizer proportioned according the weight of the binder materials. The fresh properties, mechanical properties and elevated temperatures of the mixtures were calculated. Then, the results from the microstructure analyses were compared with that of the reference mixtureand it was found that 6% replacement of cement with NS was optimum replacement level. When the NS content was increased from 0% to 6%, the air content and permeability of the mixture decreased by 35% and 39%, the compressive and tensile strength improved by 21% and 18% and the flexural strength and modulus of elasticity increased by 20% and 11.5%, respectively. However, the effect of micro steel fibres on the compressive strength was inconclusive. The overall results indicate that micro steel fibres have the potential to improve the tensile strength, flexure strength and modulus of elasticity of the UHPC. The use of 6% NS together with 1% micro-steel fiber increased the concrete strength and reduce the cost of concrete mix.

Heating Behavior and Adhesion Property of Epoxy Adhesive with Nano and Micro Sized Fe3O4 Particles (Nano 및 Micro 크기의 Fe3O4 분말이 첨가된 열경화성 에폭시 접착제의 유도가열 및 접착 특성)

  • Hwang, Ji-Won;Im, Tae-Gyu;Choi, Seung-Yong;Lee, Nam-Kyu;Shon, Min-Young
    • Composites Research
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    • v.33 no.2
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    • pp.55-60
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    • 2020
  • A study on the heating behavior and adhesion property of structural epoxy adhesive through induction heating have been conducted. An adhesive for induction heating was manufactured through mixing with nano and micro sized Fe3O4. From the results, it was observed that induction heating is less affected by adherend (GFRP) thickness than oven heating. The heating rate of Fe3O4 embedded epoxy adhesive using induction heating much higher than that of oven curing process and it is more appreciable when the contents of Fe3O4 increased. Furthermore, adhesion strength increased with increase of Fe3O4 particle contents.

Effect of Welding Thermal Cycle on Microstructure and Pitting Corrosion Property of Multi-pass Weldment of Super-duplex Stainless Steel (슈퍼 듀플렉스 스테인리스강 다층용접부의 미세조직 및 공식(Pitting Corrosion)에 미치는 용접열사이클의 영향)

  • Nam, Seong-Kil;Park, Se-Jin;Na, Hye-Sung;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • v.28 no.4
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    • pp.18-25
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    • 2010
  • Super-duplex stainless steels (SDSS) have a good balance of mechanical property and corrosion resistance when they consist of approximately equal amount of austenite and ferrite. The SDSS needs to avoid the detrimental phases such as sigma(${\sigma}$), chi(${\chi}$), secondary austenite(${\gamma}2$), chromium carbide & nitride and to maintain the ratio of ferrite & austenite phase as well known. However, the effects of the subsequent weld thermal cycle were seldom experimentally studied on the micro-structural variation of weldment & pitting corrosion property. Therefore, the present study investigated the effect of the subsequent thermal cycle on the change of weld microstructure and pitting corrosion property at $40^{\circ}C$. The thermal history of root side was measured experimentally and the change of microstructure of weld root & the weight loss by pitting corrosion test were observed as a function of the thermal cycle of each weld layer. The ferrite contents of root weld were reduced with the subsequent weld thermal cycles. The pitting corrosion was occurred in the weld root region in case of the all pitted specimen & in the middle weld layer in some cases. And the weight loss by pitting corrosion was increased in proportional to the time exposed at high temperature of the root weld and also by the decrease of ferrite content. The subsequent weld thermal cycles destroy the phase balance of ferrite & austenite at the root weld. Conclusively, It is thought that as the more subsequent welds were added, the more the phase balance of ferrite & austenite was deviated from equality, therefore the pitting corrosion property was deteriorated by galvanic effect of the two phases and the increase of 2nd phases & grain boundary energy.

Study on the Thermal Characteristics of Concrete Using Micro Form Admixture (마이크로기포제를 사용한 콘크리트의 열적 특성에 관한 연구)

  • Park, Young Shin;Kim, Jung Ho;Jeon, Hyun Kyu;Seo, Chee Ho
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.2
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    • pp.101-109
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    • 2013
  • Recently, it is certain that the increase of heating and cooling energy consumption by radical change in climate condition has caused serious problems related to environmental and energy concerns associated with increase of fossil fuel usage and carbon dioxide production as well as global warming. So, various actions to reduce greenhouse gas exhaustion and energy consumption have been prepared by world developed countries. Our government has also been trying to seek energy control methods for houses and buildings by proclaiming political polices on low-carbon green growth and construction and performance standards for environment-friendly housing. The energy consumption by buildings approximately reaches 25% of total korea energy consumption, and the increasing rate of energy consumption by buildings is stiffer than the rate by the other industries. The greatest part in the buildings of the energy consumption is building facade. While lots of research projects for reducing energy consumption of the facade have been conducted, but a few research projects on concrete comprising more than 70% of outsider of buildings has been tried. This research presents here a study to improve the insulation property of structural concrete formed by micro form admixture (MFA) with experimentally reviewing the physical, mechanical and thermal characteristics of the concrete. As the results of this experiment, in the case of concrete mixed with MFA, slump loss has been improved. As the mixing ratio of MFA increases, the compressive strength is decreased and thermal conductivity is increased. Also it was found that water-cement ratio increases, the compressive strength is decreased and thermal conductivity is increased. but, there was not big influence by the change of fine aggregate ratio.

Motion behavior research of liquid micro-particles filtration at various locations in a rotational flow field

  • Yan, Yan;Lin, Yuanzai;Cheng, Jie;Ni, Zhonghua
    • Structural Engineering and Mechanics
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    • v.62 no.2
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    • pp.163-170
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    • 2017
  • This study presents a particle-wall filtration model for predicting the particle motion behavior in a typical rotational flow field-filtration in blower system of cooker hood. Based on computational fluid dynamics model, air flow and particles has been simulated by Lagrangian-particle/ Eulerian-gas approaches and get verified by experiment data from a manufacturer. Airflow volume, particle diameter and local structure, which are related to the particle filtration has been studied. Results indicates that: (1) there exists an optimal airflow volume of $1243m^3/h$ related to the most appropriate filtration rate; (2) Diameter of particle is the significant property related to the filtration rate. Big size particles can represent the filtration performance of blower; (3) More than 86% grease particles are caught by impeller blades firstly, and then splashed onto the corresponding location of worm box internal wall. These results would help to study the micro-particle motion behavior and evaluate the filtration rate and structure design of blower.

Design of Linear Ultrasonic Motor for Small tong Actuation (렌즈 구동을 위한 선형 초음파 전동기 설계)

  • Kwon Taeseong;Lee Seung-Yop;Kim Sookyung
    • 정보저장시스템학회:학술대회논문집
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    • 2005.10a
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    • pp.190-194
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    • 2005
  • There is a great demand of micro-actuators for mobile information devices such as SFF optical drives and mobile camera phones. However, conventional magnetic coils of electromagnetic motors are a major obstacle for miniaturization because of their complicated structures and large power consumption. In this paper, a linear ultrasonic motor to actuate focusing lens of mobile devices is proposed. The new actuator uses a ring type bimorph piezoelectric material, and $d_{31}$ mode is adopted for applying linear motion. The interaction between inertia force and friction force makes linear motion by high-frequency saw signal input. The saw signal gives steady forces on the one direction by asymmetric inclination property of the signal itself on time domain. A commercial FEM (ANSYS) was used in this investigation for simulating structural analysis, identification of dynamic property, such as resultant displacement and coupled analysis with piezoelectric material. To evaluate the performance of the new design, a prototype was manufactured and experiments were carried out. Experimental results show the actuator motion of 1.52 mm/s at 10 kHz input signal in 5 V.

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Design of a Linear Ultrasonic Actuator for Small Lens Actuation (초소형 렌즈 구동을 위한 선형 초음파 구동기 설계)

  • Kwon, Tae-Seong;Choi, Yo-Han;Lee, Seung-Yop
    • Transactions of the Society of Information Storage Systems
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    • v.2 no.4
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    • pp.251-256
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    • 2006
  • There is a great demand of micro-actuators for mobile information devices such as SFF optical drives and mobile phone cameras. However, the magnetic coils used in conventional electromagnetic motors are a major obstacle for the miniaturization because of their complicated structures and large power consumption. In this paper, a linear ultrasonic motor to actuate focusing lens of mobile devices is proposed. The new actuator uses a ring type bimorph piezoelectric material, and $d_{31}$ mode is adopted for applying linear motion. The interaction between inertia force and friction force makes linear motion by high-frequency saw signal input. The saw signal gives steady forces on the one direction by asymmetric inclination property of the signal itself on time domain. A commercial FEM(ANSYS) was used in this investigation for simulating structural analysis, identification of dynamic property, such as resultant displacement and coupled analysis with piezoelectric material. To evaluate the performance of the new design, a prototype was manufactured and experiments were carried out. Experimental results show the actuator motion of 5.4 mm/s at 10V saw signal of 41 kHz.

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A Study on Thermal and Mechanical Properties of Elastic Epoxy with Water Aging (탄성형 에폭시의 흡습 열화에 따른 열적 및 기계적 특성에 관한 연구)

  • 이관우;민지영;한기만;최용성;박대희
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.53 no.6
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    • pp.293-299
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    • 2004
  • In this paper, thermal and mechanical properties of electric epoxy with water aging were discussed. We made elastic epoxy specimen adding a ratio of 0〔phr〕20〔phr〕, 35〔phr〕 and 53〔phr〕 with modifier to existing epoxy. We studied mechanical property of elastic resin after absorption in water from 0 to 484 hours. As a result, diffusion factor of elastic epoxy showed 20-21${\times}$10$^{-4}$ $\textrm{mm}^2$/s and general epoxy showed 9.5${\times}$10$^{-4}$ $\textrm{mm}^2$/s. Elastic property increased linearly according to addiction and decreased according to water absorption. Tensile strength was reduced according to addition. It was affected by water absorption of micro-void of elastic epoxy. Hardness inclined to decrease after increasing according to absorbed time. In water-absorption state, it was experimented a change of heat flow by temperature of elastic epoxy and change of thermal expansion coefficient. DSC (Differential Scanning Calorimetry) and TMA (Thermomechanical Analysis) equipments were used to measure Tg. A temperature ringe of DSC was from -0($^{\circ}C$) to 200($^{\circ}C$). One of TMA was from -0($^{\circ}C$) to 350($^{\circ}C$). In addition, we investigated structural analysis of water absorbed specimen using SEM (Scanning Electron Microscope).