• Title/Summary/Keyword: Micro Porosity

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WC-Co coating by cold spray deposition (Cold spray를 이용한 WC-Co 코팅)

  • 김형준;황순영;권영각
    • Proceedings of the KWS Conference
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    • 2004.05a
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    • pp.311-313
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    • 2004
  • WC-12-17%Co powders with nano- and micro-structures were deposited by cold spray process using nitrogen and helium gases. The results show that there is no detrimental phase transformation and/or decarburization of WC by cold spray deposition as expected. It is also observed that nano-sized WC in the feedstock powder is maintained in the cold spray deposition. It is demonstrated that it is possible to fabricate the nano-structured WC-Co coating with low porosity and very high hardness (-2050 HV) by cold spray deposition with reasonable powder preheating.

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A Study on Acoustic Emission Characteristics of MCrAlY Coated Material by Vacuum Plasma Spray Process (진공 플라즈마 용사공정에 의한 MCrAlY코팅재의 음향방출 신호 특성 연구)

  • 박진효;이구현;예경환;김정석;강명창
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.921-924
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    • 2004
  • This paper is to investigate a crack for plasma sprayed MCrAlY coated material by acoustic emission method in 4-point bending test. The CoNiCrAlY is coated on Inconel-718 by vacuum plasma spray process. Micro-hardness measurement was conducted by means of Micro Vickers-hardness indentor. The porosity of coating layer was measured using a SEM and Image Analyzer. AE monitoring system is composed of PICO type sensor, a wide band preamplifier(40dB), a PC and AE DSP(16/32 PAC) board. The AE count, Hit and energy of coating specimens is measured according to coating thickness.

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Effective mechanical properties of micro/nano-scale porous materials considering surface effects

  • Jeong, Joonho;Cho, Maenghyo;Choi, Jinbok
    • Interaction and multiscale mechanics
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    • v.4 no.2
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    • pp.107-122
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    • 2011
  • Mechanical behavior in nano-sized structures differs from those in macro sized structures due to surface effect. As the ratio of surface to volume increases, surface effect is not negligible and causes size-dependent mechanical behavior. In order to identify this size effect, atomistic simulations are required; however, it has many limitations because too much computational resource and time are needed. To overcome the restrictions of the atomistic simulations and graft the well-established continuum theories, the continuum model considering surface effect, which is based on the bridging technique between atomistic and continuum simulations, is introduced. Because it reflects the size effect, it is possible to carry out a variety of analysis which is intractable in the atomistic simulations. As a part of the application examples, the homogenization method is applied to micro/nano thin films with porosity and the homogenized elastic coefficients of the nano scale thickness porous films are computed in this paper.

Influence of Activation Temperature on Micro- and Mesoporosity of Synthetic Activated Carbons

  • Park, Soo-Jin;Jung, Woo-Young
    • Carbon letters
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    • v.2 no.2
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    • pp.105-108
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    • 2001
  • In this work, the activated carbons (ACs) with high micropores were synthesized from the polystyrene (PS) with KOH as activating agent. And the influence of activation temperature on porosity of the ACs studied was investigated. The porous structures of ACs were characterized by nitrogen adsorption at 77K using BET and D-R equations, and MP and BJH methods. The weight loss behaviors of the samples impregnated with KOH were also monitored using thermogravimetric analyzer (TGA). As a result, it was found that the samples could be successfully converted into ACs with well-developed micropores. From the results of pore size analysis, it was confirmed that elevated activation temperature does lead to the formation and deepening of microstructures without significant change in mesostructures. A thermogravimetric study showed that KOH could suppress the thermal decomposition of the sample, resulting in the increase of carbon yields.

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Deposition Behavior and Properties of Carbon Nanotube Aluminum Composite Coatings in Kinetic Spraying Process (탄소 나노튜브 알루미늄 복합재료 저온 분사 코팅의 적층 거동 및 특성)

  • Kang, Ki-Cheol;Xiong, Yuming;Lee, Chang-Hee
    • Journal of Welding and Joining
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    • v.26 no.5
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    • pp.36-42
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    • 2008
  • Carbon nanotube (CNT) aluminum composite coatings were built up through kinetic spraying process. Deposition behavior of CNT aluminum composite on an aluminum 1050 alloy substrate was analyzed based on deposition mechanism of kinetic spraying. The microstructure of CNT aluminum composite coating were observed and analyzed. Also, the electrical resistivity, bond strength and micro-hardness of the CNT aluminum composite coatings were measured and compared to kinetic sprayed aluminum coatings. The CNT aluminum composite coatings have a dense structure with low porosity. Compared to kinetic sprayed aluminum coating, the CNT aluminum composite coatings present lower electrical resistivity and higher micro-hardness due to high electrical conductivity and dispersion hardening effects of CNTs.

Size-dependent magneto-electro-elastic vibration analysis of FG saturated porous annular/ circular micro sandwich plates embedded with nano-composite face sheets subjected to multi-physical pre loads

  • Amir, Saeed;Arshid, Ehsan;Arani, Mohammad Reza Ghorbanpour
    • Smart Structures and Systems
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    • v.23 no.5
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    • pp.429-447
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    • 2019
  • The present study analyzed free vibration of the three-layered micro annular/circular plate which its core and face sheets are made of saturated porous materials and FG-CNTRCs, respectively. The structure is subjected to magneto-electric fields and magneto-electro-mechanical pre loads. Mechanical properties of the porous core and also FG-CNTRC face sheets are varied through the thickness direction. Using dynamic Hamilton's principle, the motion equations based on MCS and FSD theories are derived and solved via GDQ as an efficient numerical method. Effect of different parameters such as pores distributions, porosity coefficient, pores compressibility, CNTs distribution, elastic foundation, multi-physical pre loads, small scale parameter and aspect ratio of the plate are investigated. The findings of this study can be useful for designing smart structures such as sensor and actuator.

Development of bone scaffold using HA(Hydroxyapatite) nano powder (HA(Hydroxyapatite) 나노 입자를 이용한 bone scaffold의 개발)

  • Kim J.Y.;Lee S.J.;Lee J.W.;Kim Shin-Yoon;Cho D.W.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.159-160
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    • 2006
  • A novel approach to the manufacture of biocompatible ceramic scaffold for tissue engineering using micro-stereolithography system is introduced. Micro-stereolithography is a newly proposed technology that enables to make a 3D micro structure. The 3D micro structures made by this technology can have accurate and complex shape within a few micron error. Therefore, the application based on this technology can vary greatly in nano-bio fields. Recently, tissue-engineering techniques have been regarded as alternative candidate to treat patients with serious bone defects. So many techniques to design and fabricate 3D scaffolds have been developed. But the imperfection of scaffold such as random pore size and porosity causes a limitation in developing optimum scaffold. So scaffold development with controllable pore size and fully interconnected shape have been needed for a more progress in tissue engineering. In this paper, bone scaffold was developed by applying the micro-stereolithography to the mold technology. The scaffold material used was HA(Hydroxyapatite) nano powder. HA is a type of calcium phosphate ceramic with similar characteristic to human inorganic bone component. The bone scaffold made by HA is expected, in the near future, to be an efficient therapy for bone defect.

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Laboratory tests for studying the performance of grouted micro-fine cement

  • Aflaki, Esmael;Moodi, Faramarz
    • Computers and Concrete
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    • v.20 no.2
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    • pp.145-154
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    • 2017
  • In geological engineering, grouting with Portland cement is a common technique for ground improvement, during which micro-fine cement is applied as a slurry, such that it intrudes into soil voids and decreases soil porosity. To determine the utility and behavior of cements with different Blaine values (index of cement particle fineness) for stabilization of fine sand, non-destructive and destructive tests were employed, such as laser-ray determination of grain size distribution, and sedimentation, permeability, and compressive strength tests. The results of the experimental study demonstrated a suitable mix design for the upper and lower regions of the cement-grading curve that are important for grouting and stabilization. Increasing the fineness of the cement decreased the permeability and increased the compressive strength of grouted sand samples considerably after two weeks. Moreover, relative to finer (higher Blaine value) or coarser (lower Blaine value) cements, cement with a Blaine value of $5,100cm^2/g$ was optimal for void reduction in a grouted soil mass. Overall, study results indicate that cement with an optimum Blaine value can be used to satisfy the designed geotechnical criteria.

Material Nonlinear Behavior and Microstructural Transition of Porous Polyurethane Foam under Uniaxial Compressive Loads (일축 압축하중 하 다공성 폴리우레탄폼의 재료비선형 거동 및 미세구조 변화)

  • Lee, Eun Sun;Goh, Tae Sik;Lee, Chi-Seung
    • Korean Journal of Materials Research
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    • v.27 no.12
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    • pp.688-694
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    • 2017
  • Porous materials such as polymeric foam are widely adopted in engineering and biomedical fields. Porous materials often exhibit complex nonlinear behaviors and are sensitive to material and environmental factors including cell size and shape, amount of porosity, and temperature, which are influenced by the type of base materials, reinforcements, method of fabrication, etc. Hence, the material characteristics of porous materials such as compressive stress-strain behavior and void volume fraction according to aforementioned factors should be precisely identified. In this study, unconfined uniaxial compressive test for two types of closed-cell structure polyurethane foam, namely, 0.16 and $0.32g/cm^3$ of densities were carried out. In addition, the void volume fraction of three different domains, namely, center, surface and buckling regions under various compressive strains (10 %, 30 %, 50 % and 70 %) were quantitatively observed using Micro 3D Computed Tomography(micro-CT) scanning system. Based on the experimental results, the relationship between compressive strain and void volume fraction with respect to cell size, density and boundary condition were investigated.

Modelling of Large Triaxial Test with Rockfill Materials by Distinct Element Method (개별요소법에 의한 락필재료의 대형삼축압축시험 모델링)

  • Jeon, Je-Sung;Kim, Ki-Young;Shin, Dong-Hoon
    • Journal of the Korean Geotechnical Society
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    • v.22 no.10
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    • pp.111-120
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    • 2006
  • In this research, numerical simulations by PFC considering discrete element method are conducted to predict experimental results of large triaxial compression test with rockfill material for dam construction. For generation of compacted assembly with specific grain size distribution and initial material porosity, the clump logic method and expansion of generated particles are adapted. To predict stress-stain behavior of large triaxial test, discrete particle modelling is applied with micro parameters which are chosen by calibration process. It is expected that distinct particle modelling method could be used as a useful tool to investigate micro and macro behavior associated with geotechnical problems and develop a numerical laboratory.