• Journal of Welding and Joining
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• v.28 no.5
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• pp.51-57
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• 2010

Brittle microstructure created in a heat affected zone (HAZ) during the welding of low alloy steel can be eliminated by post-weld heat treatment (PWHT). If the PWHT is not possible during a repair welding, the controlled bead depositions of multi-pass welding should be applied to obtain tempering effect on the HAZ without PWHT. In order to anticipate and control the tempering effect during the temper bead welding, the definition of temperature curve obtained from the analytical solution was suggested in this research. Because the analytical solution for heat flow is expressed as a mathematical equation of weld parameters, it may be effective in anticipating the effect of each weld parameter on the tempering in HAZ during the successive bead depositions. The reheating effect by the successive bead layer on the brittle coarse grained HAZ formed by earlier bead deposition was estimated by comparing the overlapped distance between the temperature curves in the HAZ. Three layered weld specimens of SA508 base metal with A52 filler were prepared by controlling heat input ratio between layers. The tempering effect anticipated by using the overlapped distance between the temperature curves was verified by measuring the micro-hardness distribution in the HAZ of prepared specimens. The temperature curve obtained from analytical solution was expected as a good tool to find optimal temper bead welding conditions.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.41 no.3
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• pp.219-224
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• 2017

A study on dissimilar friction-welded joints was performed for cam shaft applications using solid bar samples, 20mm in diameter, of forging steel(SF45) and carbon steel(SM45C). The main parameters of friction welding such as tensile tests, Vickers hardness surveys of the bond of area, the heat affected zone (HAZ), and the observation of microstructure were investigated to ensure a good quality of friction welding through visual observations. The specimens were tested as-welded and post weld heat treatment(PWHT). This paper deals with optimizing the welding conditions and analyzing various rotary bending fatigue test(RBFT) properties about heat-treated base metal(BM), as-welded and PWHT. Consequently, two materials for friction welding are strongly mixed with a well-combined structure of micro-particles without any molten material, particle growth, or any defect. Moreover, the fatigue limit of BM(SF45) and PWHT for the RBFT were observed as 180MPa and 250MPa, respectively. It was confirmed that the PWHT causes approximately 40％ improvement in the fatigue limit when compared to the BM(SF45).

• Journal of the Korean Society for Nondestructive Testing
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• v.20 no.5
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• pp.390-396
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• 2000

The dynamic elastic constants of the simulated weld HAZ (heat-affected zone) of SA 508 Class 3 reactor pressure vessel (RPV) steel were investigated by resonant ultrasound spectroscopy (RUS). The resonance frequencies of rectangular parallelepiped samples woe calculated from the initial estimates of elastic stiffness $c_{11},\;c_{12}\;and\;c_{44}$ with an assumption of isotropic property, dimension and density. Through the comparison of calculated resonant frequencies with the measured resonant frequencies by RUS, very accurate elastic constants of SA 508 Class 3 steel were determined by iteration and convergence processes. Clear differences of Youngs modulus and shear modulus were shown from samples with different thermal cycles and microstructures. Youngs modulus and shear modulus of samples with fine-grained bainite were higher than those with coarse-grained tempered martensite. This tendency was confirmed from other results such as micro-hardness test.

• Korean Journal of Materials Research
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• v.23 no.5
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• pp.293-298
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• 2013

In this study, an HP-mod. type(KHR-45A), which is used as a heater tube material in the pyrolysis process, was evaluated for its carburizing properties. It was confirmed from the microstructural observation of the tubes that the volume fraction of carbide increased and that the coarsening of Cr-carbide generated as a degree of carburization increased. The depth of the hardened layer, which is similar to the thickness of the carburized region of each specimen, due to carburization is confirmed by measurement of the micro-Vickers hardness of the cross section tube, which thickness is similar to that of the carburized region of each specimen. Two types of chromium carbides were identified from the EBSD (electron back-scattered diffraction) image and the EDS (energy-dispersive spectroscopy) analysis: Cr-rich $M_{23}C_6$ in the outer region and Cr-rich $M_7C_3$ in the inner region of tubes. The EDS analysis revealed a correlation between the ferromagnetic behavior of the tubes and the chromium depletion in the matrix. The chromium depletion in the austenite matrix is the main cause of the magnetization of the carburized tube. The method used currently for the measurement of the carburization of the tubes is confirmed; carburizing evaluation is useful for magnetic flux density measurement. The volume fraction of the carbide increased as the measuring point moved into the carburized side; this was determined from the calculation of the volume fraction in the cross-section image of the tubes. These results are similar to the trends of carburization measurement when those trends were evaluated by measurement of the magnetic flux density.

• Journal of Welding and Joining
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• v.28 no.4
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• pp.73-80
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• 2010

In this work, the effect of welding variables on weldability of gas tungsten arc(GTA) welding was investigated with experimental analysis for a commercial pure(CP) titanium (Grade.1). The GTA welding tests on sheet samples with 0.5mm in thick were carried out at different process variables such as arc length, welding speed and electrode shape. In order to search an optimum arc length with full penetration, bead- on-plate welding before butt-welding were performed with different arc length conditions. From the bead- on-plate welding results, the optimum condition considering arc stability and electrode loss was obtained in the arc length of 0.8mm. Butt-welding tests based on the arc length of 0.8mm were carried out to achieve the optimum conditions of welding speed and electrode shape. Optimum conditions of welding speed and electrode shape were suggested as 10 mm/s and truncated electrode shape, respectively. It was successfully validated by the microstructural observation, tensile tests, micro-hardness tests and formability tests.

• Korean Journal of Materials Research
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• v.25 no.5
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• pp.253-257
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• 2015

The implanting of metal products is performed with numerous surface treatments because of toxicity and adhesion. Recently, the surface modification of metal products has been actively studied by coating the surface of the TiC or TiN film. We prepared a Ti(10%)Ag Target which may be used in dental oral material by, using the AIP(arc ion plating) system TiAgN coating layer that was deposited on Ti g.23. The purpose of this study was to establish the optimal bias voltage conditions of the coated TiAgN layer formed by the AIP process. The TiAgN coatings were prepared with different bias voltage parameters (0V to -500V) to investigate the effect of bias voltage on their mechanical and chemical properties. The SEM(scanning electron microscope), EDS(energy dispersive X-ray spectrometer), XRD(X-ray diffraction), micro-hardness, and potentiodynamic polarization were measured and the surface characteristics of the TiAgN coating layers were evaluated. The TiAgN coating layer had different mechanical characteristics based on the bias voltage, which also showed differences in thickness and composition.

• Korean Journal of Materials Research
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• v.28 no.9
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• pp.499-505
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• 2018

This investigates the microstructure and mechanical properties of Al hybrid material prepared by electromagnetic duo-casting to determine the effect of heat treatment. The hybrid material is composed of an Al-Mg-Si alloy, pure Al and the interface between the Al-Mg-Si alloy and pure Al. It is heat-treated at 373, 573 and 773K for 1h and T6 treated (solution treatment at 773K for 1h and aging at 433K for 5h). As the temperature increases, the grain size of the Al-Mg-Si alloy in the hybrid material increases. The grain size of the T6 treated Al-Mg-Si alloy is similar to that of one heat-treated at 773K for 1h. The interface region where the micro-hardness becomes large from the pure Al to the Al-Mg-Si alloy widens with an increasing heat temperature. The hybrid material with a macro-interface parallel to the tensile direction experiences increased tensile strength, 0.2 % proof stress and the decreased elongation after T6 heat treatment. On the other hand, in the vertical direction to the tensile direction, there is no great difference with heat treatment. The bending strength of the hybrid material with a long macro-interface to the bending direction is higher than that with a short macro-interface, which is improved by heat treatment. The hybrid material with a long macro-interface to the bending direction is fractured by cracking through the eutectic structure in the Al-Mg-Si alloy. However, in the hybrid material with a short macro-interface, the bending deformation is observed only in the limited pure Al.

• Transactions of the Korean Society of Mechanical Engineers
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• v.14 no.3
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• pp.581-593
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• 1990

A semi-solid alloy in which solid and liquid phase are co-existing is obtained by strirring of Al7075 molten metal. A semi-solid alloy is dependent on the corresponding temperature within the solid-liquid range, and the process parameters should be controlled accurately to obtain the homogeneous semi-solid alloy. The possibility o homogeneous fiber-reinforce aluminum alloy by addition of $Al_{2}$O$_{3}$ short fibers with vigorous agitation was investigated. The billet of composite materials was fabricated by squeeze casting, and homogeneous dipersion state of fibers in billet of fabricated metal matrix composites was observed. A slurry of semi-solid short fiber metal matrix composites is used in the direct rolling process, and this process showed the fabrication possibility of metal matrix composite sheets. The fabricated sheet was tested regarding vickers hardness, elongation and micro-structure. It has become clear that mashy state processing and working are very useful to obtain parts of composites material closed to near net shape.

• Restorative Dentistry and Endodontics
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• v.25 no.3
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• pp.482-486
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• 2000

The purpose of the present study was first, to evaluate the relationship between composite surface conversion and surface discoloration, second, to know if there was difference in surface discoloration between celluloid-strip-finished composite surface and polished surface. In addition, the discoloration of composite surface was also evaluated with visual inspection or digital camera with high resolution monitor, Z100, Tetric Ceram, Spectrum, and Aelitfil were used. The composite surfaces were celluloid-strip finished (group 1), polished (group 2), celluloid-strip finished under nitrogen gas purging (group 3) or only light cured without finishing or polishing under nitrogen gas purging (group 4). The microhardness of each samples were also measured in each group. The samples of each group were also divided into 4 subgroup whether they were immediately placed in disclosing solution (0.2% Elythrosin, pH 7.0) (subgroup1), 1 day after light curing(subgroup 2), 3day after light curing(subgroup 3) or 7 day after light curing(subgroup 4). The computer controlled spectrophotometer was used to determine CIELAB coordinates ($L^*$, $a^*$, $b^*$). The amounts of color difference were compared. The results were as follows; 1. There was no difference in discoloration between celluloid strip finished composite surface and polished surface. 2. The samples discolored more when they were placed in disclosing solution immediately after polymerization than other groups. 3. When the samples were light cured under nitrogen gas purging and without polishing process, they discolored more than other groups even though they showed higher micro hardness. 4. With visual inspection or digital camera, only a limited information was available in detecting composite surface discoloration.

• Journal of the Korean Ceramic Society
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• v.25 no.2
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• pp.143-153
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• 1988

In order to synthesize the partially stabilized $\alpha$-Sialon, A1N and Y2O3 were added to synthesized $\alpha$-Si3N4. The phase composition, mechanical properties, micro structure, etc, of the synthesized $\alpha$-Sialon were investigated. Partially stabilized $\alpha$-Sialon ceramics could be synthesized from the composition which was a little deviated from x=0.4, x=0.6 composition along the Si3N4.0.1Y2O3:0.9AlN tie line at 1750-180$0^{\circ}C$ for 2 hrs in N2 atmosphere. It is assumed that A1N is more closely related than Y2O3 to the formation of $\alpha$-Sialon, and that A1N is more easily dissolved into $\alpha$-structure than into $\beta$-structure. In Ya2O3-rich phase mechanical properties were observed to be poor because of formation of mellilite, grain growth, and thermal decomposition of $\alpha$-Sialon. The maximum values of M.O.R, KIC and hardness are 723 MPa, 4.5MN/㎥/2 and 19.3 GPa, respectively, and they were observed for the $\alpha$-Sialon ceramics sintered at 178$0^{\circ}C$.