• Title/Summary/Keyword: Micro Filler

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Effect of Fine Alumina Filler Addition on the Thermal Conductivity of Non-conductive Paste (NCP) for Multi Flip Chip Bonding (멀티 플립칩 본딩용 비전도성 접착제(NCP)의 열전도도에 미치는 미세 알루미나 필러의 첨가 영향)

  • Jung, Da-Hoon;Lim, Da-Eun;Lee, So-Jeong;Ko, Yong-Ho;Kim, Jun-Ki
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.2
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    • pp.11-15
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    • 2017
  • As the heat dissipation problem is increased in 3D multi flip chip packages, an improvement of thermal conductivity in bonding interfaces is required. In this study, the effect of alumina filler addition was investigated in non-conductive paste(NCP). The fine alumina filler having average particles size of 400 nm for the fine pitch interconnection was used. As the alumina filler content was increased from 0 to 60 wt%, the thermal conductivity of the cured product was increased up to 0.654 W/mK at 60 wt%. It was higher value than 0.501 W/mK which was reported for the same amount of silica. It was also found out that the addition of fine sized alumina filler resulted in the smaller decrease in thermal conductivity than the larger sized particles. The viscosity of NCP with alumina addition was increased sharply at the level of 40 wt%. It was due to the increase of the interaction between the filler particles according to the finer particle size. In order to achieve the appropriate viscosity and excellent thermal conductivity with fine alumina fillers, the highly efficient dispersion process was considered to be important.

Evaluation of mechanical Characteristic according to the Filler Metal by GTA welding Process using 7075 Aluminum Alloy (알루미늄 합금 7075의 용가재에 따른 GTA용접공정의 기계적 특성 평가)

  • Son, Yeong-San;Lim, Byung-Chul
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.4
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    • pp.521-526
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    • 2017
  • In the GTA welding process of Al 7075 alloy using different types of filler metals, the tensile test and micro-hardness test were conducted to evaluate the mechanical characteristics. Also, the radiographic test result showed that the weld met the criterion of level 1 in accordance with KS D 0242 for verifying the welding integrity and there were no welding defects. The tensile test result obtained using Al 7075 as a filler metal showed that the material was fractured in the weld zone. The tensile strengths of the materials using Al 7075 and ER 4043 as the filler metal were about 240MPa and 253MPa, their yield strengths were about 132MPa and 120MPa and their elongation percentages were 6.6% and 13%, respectively. The micro-hardness value of the deposited metal zone when using Al 7075 as the filler metal was Hv 132. However, the micro-hardness of the material using ER4043 as the filler metal was about 24% lower than that using Al 7075. When the chemical composition of the filler metal is the same as that of the material itself, fracture can occur in the deposited metal zone. Therefore, it is not desirable to use the same material as the filler metal for the welding of Al 7075 alloy. Moreover, the use of Al-Si based ER 4043 as a filler metal is more desirable than using the same material as a filler metal for welding Al 7075.

Improvement on Surface Properties of Engineering Plastic with Adding Micro-$Al_2O_3$, Nano-$Al(OH)_3$ (Micro-$Al_2O_3$와 Nano-$Al(OH)_3$ 첨가에 따른 엔지니어링 플라스틱의 표면특성 개선)

  • Jung, Eui-Hwan;Lee, Han-Ju;Lim, Kee-Joe;Heo, Jun;Kang, Seong-Hwa
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.03b
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    • pp.29-29
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    • 2010
  • Surface contamination and leakage current have caused operating problems. A flashover in a substation may result in destruction of an insulator or many others electrical equipment. Engineering plastics have good characteristic (light weight, good productivity and little of void) as compare with epoxy or porcelain insulators. Outdoor insulator must have resistance to contamination. However, it isn't suited to outdoor insulator because it is not hydrophobic. RTV(Room temperature vulcanizing) has a good property of hydrophobic and micro-filler. nano-filler have characteristics of obstructing exothermic reaction. In order to reduce the incidence of insulator flashover and damage, the silicon rubber contained with micro, nano-filler coating on surface of engineering plastics. In this paper, it compares tracking resistance, leakage current of the engineering plastic coated RTV with that of non-coated engineering plastic. And filled-composites performed much better than non-filled composites.

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Micro-threads of Cross-linked Hyaluronic Acid Hydrogel using a Microfluidic Chip (미세 유체 칩 기반의 히알루론산 미세 실의 제작)

  • Lee, Yun-Kyung;Lee, Kwang-Ho
    • Journal of Biomedical Engineering Research
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    • v.38 no.1
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    • pp.1-8
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    • 2017
  • The successful synthesis of hyaluronic acid micro-threads is very promising approach for the broad application in tissue engineering such as dermal fillers. Because hyaluronic acid has the excellent biocompatibility and ability to maintain the moisture of up to several hundred times its own weight. In order to generate the hyaluronic acid micro-threads in microfluidic system, we employed two-phase flow microfluidic chip to make a rapid synthesis of the hyaluronic acid hydrogel. Hyaluronic acid was mixed with 0.02N NaOH solution and 1, 4-Butanediol diglycidyl ether (BDDE) solution and then injected into core channel. The ethanol was used for the 3-dimensional micro-thread formation in sheath channel. We manipulated the diameter of HA micro-threads using controlling of flow rates in microfluidic chip, and showed the feasibility of immobilization in HA micro-threads with florescent substances. Also, the generated HA micro-threads were evaluated and showed the suitable properties with tensile strength, bending property, and swelling profiles for dermal fillers. As a result, we suggested an innovative method for microfluidic chip-based HA micro-threads which could safely be applied as dermal filler in tissue engineering.

Brazing Characteristics of Zircaloy-4 Using Rapidly Solidified Amorphous Zr-Be Alloy Filler Metals (급속응고된 비정질 Zr-Be 합금 용가재를 이용한 Zircaloy-4의 브레이징 특성)

  • Kim, Sang-Ho;Go, Jin-Hyeon;Park, Chun-Ho;Kim, Seong-Gyu
    • Korean Journal of Materials Research
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    • v.12 no.2
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    • pp.140-145
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    • 2002
  • This study was conducted to investigate the brazing characteristics between Zircaloy-4 nuclear fuel cladding tubes and bearing pads with filler metals of amorphous $Zr_{1-x}Be_x$(0.3$\leq$x$\leq$0.5) binary alloy, in which they were produced in the ribbon form by the melt-spinning metod. The crystallization behavior, stability, hardness and micro-structure of brazed zone were examined by X-ray diffraction, differential scanning calorimetry, micro-Vickers hardness test, optical microscopy, and transmission electron microscopy. $Zr_{1-x}Be_x$(0.3$\leq$x$\leq$0.4) amorphous alloys were crystallized to $\alpha$-Zr with increasing the temperature, and the rest were transformed to ZrBe$_2$at higher temperatures. On the other hand, $Zr_{1-x}Be_x$(0.4$\leq$x$\leq$0.5) amorphous alloys were crystallized to $\alpha$-Zr and ZrBe$_2$, simultaneously. The thickness of the layer brazed with amorphous alloy was increased with increasing the beryllium content due to the higher diffusion of Be. The morphology of brazed layer with PVD Be filler metal showed dendrite while that brazed with amorphous alloys appeared globular. Micro-Vickers hardness of brazed zone increased as the beryllium content of filler metal was decreased.

Study on Electrical and Mechanical Properties of High Viscosity Solid Epoxy / Silica and Alumina Composite (고점도형 고상에폭시/실리카와 알루미나 콤포지트의 전기적, 기계적 특성연구)

  • Park, Jae-Jun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.67 no.10
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    • pp.1330-1337
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    • 2018
  • In this study, 40, 50, 60, and 70 wt% filler dispersed samples were prepared for the current GIS Spacer or environmentally friendly GIS. In the AC electrical breakdown, EMSC and EMAC decreased with increasing filler content, and EMSC showed better breakdown strength than EMAC. The mechanical properties such as tensile strength and flexural strength of EMSC and EMAC were also increased with increasing filler content. In addition, EMSC results in better mechanical properties than EMAC. The reason for this is considered to be one in which the influence of the interface is important.

AC Electrical and Mechanical Properties of Epoxy-Nano-Microsilica Mixed Composites for Eco-Friendly GIS Spacer (친환경 GIS Spacer용, 에폭시-나노-마이크로실리카 혼합 콤포지트의 교류 전기적, 기계적 특성)

  • Park, Jae-Jun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.67 no.9
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    • pp.1181-1188
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    • 2018
  • In order to develop new insulating materials for GIS Spacer using environmentally friendly insulating gas, three kinds of dispersed liquid nano composites of solid epoxy /nano layered silicate filled material were prepared. And the epoxy/nano/micro silica composite was prepared by mixing epoxy/nano 3 phr dispersion/4 kinds of filler contents(40,50,60, 70wt%). The electrical insulation breakdown strengths of the nano and nano/micro mixed composites were evaluated by using 8 kinds of samples including the original epoxy. The mechanical tensile strength of the epoxy / nano / micro silica composite were evaluated, also. The TEM was measured to evaluate the internal structure of nano/micro composites. As a result, it was confirmed that the layered silicate nano particles was exfoliated through the process of inserting epoxy resin between silicate layers and the layers. In addition, dispersion of nano / micro silica resulted in improvement of electrical insulation breakdown strength with increase of filling amount of dense tissue with nanoparticles inserted between microparticles. In addition, the tensile strength showed a similar tendency, and as the content of microsilica filler increased, the mechanical improvement was further increased.

Extraction of Micro Filler from Bio-waste Material (Bio waste 소재로부터의 마이크로 필러 추출)

  • Nam, Gibeop;Song, Jung-Il
    • Composites Research
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    • v.31 no.5
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    • pp.209-214
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    • 2018
  • This paper explain about the development of environmental friendly, low cost and stable supply material i.e., rice husk and shell were used as micro incorporating bio waste filler. Those were processed by ball mill and analyzed through micro observation by FE-SEM, EDS and particle size distribution. The obtained filler was mixed with epoxy resin for the manufacturing of CFRP composite and study tensile properties. In EDS analysis main contents of rice husk and rice husk ash are C, O and Si. When rice husk was burned C and Si ration were increased. Shell powder has C, O and Ca. It caused $CaCO_3$ from shell. Surface weighted mean of rice husk powder is $6.19{\mu}m$ and volume weighted mean is $14.77{\mu}m$. And it has rod type particles which caused hair and husk structure parts. Surface weighted mean of rice husk ash powder is $1.55{\mu}m$ and volume weighted means is $8.20{\mu}m$. Surface weighted mean of shell powder is $2.53{\mu}m$ and volume weighted mean is $5.79{\mu}m$. The tensile decreased with increasing the content of micro filler in CFRP composites. In case of rice husk, the significant decrement of tensile strength was observed. and in case of shell powder, there is no effect of changes take place in tensile strength.

A Study on the Partial Discharge Resistance Characteristic for Optimizing the Mixing Ratio of Heterogeneous Inorganic Insulated Materials for Environmentally Friendly GIS Spacer (친환경 GIS Spacer용, 이종 무기물 절연소재의 혼합비 최적화를 위한 부분방전 저항성 특성 연구)

  • Park, Jae-Jun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.67 no.9
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    • pp.1189-1196
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    • 2018
  • 7 type composites (40, 45, 50, 55, 60, 65, and 70 wt.%)were prepared for the environmentally friendly GIS Spacer. Five kinds of samples were prepared for optimization of the filler content ratio (MS: MA = 1: 9, 3: 7, 5: 5, 7: 3, 9: 1) of epoxy / microsilica and microalumina. As a result of evaluation of the partial discharge resistance characteristic, surface erosion is generally slowed down as the fill amount of micro silica is increased. Also, partial discharge resistance characteristics for the development of insulating materials with optimal mixing ratios of heterologous showed a higher partial resistance of discharge and a decrease in erosion, as the filler content ratio of micro silica was larger. In the future, various researches such as electrical, mechanical, and thermal studies will be needed to develop insulating materials that can commercialize power devices in environmentally friendly insulating gas.