• Title/Summary/Keyword: Micro Defect

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Crystal Molecular Orbital Calculation of the Lanthanum Nickel Oxide by Means of the Micro-Soft Fortran (마이크로-소프트 포트란을 이용한 복합 산화물 결정의 분자 궤도함수 계산)

  • Koo, Hyun-Joo;Lee, Kwang-Soon;Ahn, Woon-Sun
    • Journal of the Korean Chemical Society
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    • v.39 no.9
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    • pp.685-691
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    • 1995
  • EHMACC and EHPC programs written in VAX version to calculate the tight-binding extended Huckel method is converted into the micro-soft fortran available to PC. The band calculation of LaNiO3 unit cell and extended ($2{\times}2{\times}1$) cell with perovskite structure is made by the PC/386 and PC/486. The calculation is also made for the DOS and the COOP. It is supposed that the electronic property of $LaNiO_3$ is semiconductor along to the ${\Gamma}{\rightarrow}H,\;H{\rightarrow}N,\;and\;N{\rightarrow}{\Gamma}(2D)$ direction with band gap about 0u.35 eV, while metal property in ${\Gamma}{\rightarrow}P\;and\;P{\rightarrow}N(3D)$ direction. The oxygen atom property in $LaNiO_3$ is more effectively affected by oxygen atom position than defect of nickel atom.

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Effect of Alloy Elements on Microstructure of Modified Area via Friction Stir Process in Steel Materials (마찰교반공정을 통한 강재의 개질 영역에서의 미세조직에 미치는 합금원소의 영향)

  • Kim, Sang Hyuk;Lee, Kwang Jin;Woo, Kee Do
    • Korean Journal of Materials Research
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    • v.25 no.8
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    • pp.370-375
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    • 2015
  • In this study, to confirm the effect of alloying elements on the phase transformation and conditions of the friction stir process, we processed two materials, SS400 and SM45C steels, by a friction stir process (FSP) under various conditions. We analyzed the mechanical properties and microstructure of the friction stir processed zone of SS400 and SM45C steels processed under 400RPM - 100mm/min conditions. We detected no macro (tunnel defect) or micro (void, micro crack) defects in the specimens. The grain refinement in the specimens occurred by dynamic recrystallization and stirring. The microstructure at the friction stir processed zone of the SS400 specimen consisted of an ${\alpha}$-phase. On the other hand, the microstructure at the friction stir processed zone of the SM45 specimen consisted of an ${\alpha}$-phase, $Fe_3C$ and martensite due to a high cooling rate and high carbon content. Furthermore, the hardness and impact absorption energy of the friction stir processed zone were higher than those of base metals. The hardness and impact absorption energy of FSPed SM45C were higher than that of FSPed SS400. Our results confirmed the effect of alloying elements on the phase transformation and mechanical properties of the friction stir processed zone.

Fatigue Damage Evaluation of Cr-Mo Steel with In-Situ Ultrasonic Surface Wave Assessment (초음파 시험에 의한 배관용 Cr-Mo강의 피로손상의 비파괴평가)

  • Kim, Sang-Tae;Lee, Hei-Dong;Yang, Hyun-Tae;Choi, Young-Geun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.21 no.1
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    • pp.32-38
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    • 2001
  • Although the ultrasonic method has been developed and used widely in the fields, it has been used only for measuring the defect size and thickness loss. In this study, the relationship between surface wave attenuation through micro-crack growth and variation of velocity under repeated cyclic loading has been investigated. The specimens are adopted from 2.25Cr-1Mo steel, which is used for power plant and pipeline system, and have dimensions of $200{\times}40{\times}4mm$. The results of ultrasonic test with a 5MHz transducer show that surface wave velocity gradually decreases from the point of 60% of fatigue life and the crack length of 2mm with the increasing fatigue cycles. From the results of this study, it is found that the technique using the ultrasonic velocity change is one of very useful methods to evaluate the fatigue life nondestructively.

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Comparative analysis of the in vivo kinetic properties of various bone substitutes filled into a peri-implant canine defect model

  • Jingyang Kang;Masaki Shibasaki;Masahiko Terauchi;Narumi Oshibe;Katsuya Hyodo;Eriko Marukawa
    • Journal of Periodontal and Implant Science
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    • v.54 no.2
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    • pp.96-107
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    • 2024
  • Purpose: Deproteinized bovine bone or synthetic hydroxyapatite are 2 prevalent bone grafting materials used in the clinical treatment of peri-implant bone defects. However, the differences in bone formation among these materials remain unclear. This study evaluated osteogenesis kinetics in peri-implant defects using 2 types of deproteinized bovine bone (Bio-Oss® and Bio-Oss/Collagen®) and 2 types of synthetic hydroxyapatite (Apaceram-AX® and Refit®). We considered factors including newly generated bone volume; bone, osteoid, and material occupancy; and bone-to-implant contact. Methods: A beagle model with a mandibular defect was created by extracting the bilateral mandibular third and fourth premolars. Simultaneously, an implant was inserted into the defect, and the space between the implant and the surrounding bone walls was filled with Bio-Oss, Bio-Oss/Collagen, Apaceram-AX, Refit, or autologous bone. Micro-computed tomography and histological analyses were conducted at 3 and 6 months postoperatively (Refit and autologous bone were not included at the 6-month time point due to their rapid absorption). Results: All materials demonstrated excellent biocompatibility and osteoconductivity. At 3 months, Bio-Oss and Apaceram-AX exhibited significantly greater volumes of formation than the other materials, with Bio-Oss having a marginally higher amount. However, this outcome was reversed at 6 months, with no significant difference between the 2 materials at either time point. Apaceram-AX displayed notably slower bioresorption and the largest quantity of residual material at both time points. In contrast, Refit had significantly greater bioresorption, with complete resorption and rapid maturation involving cortical bone formation at the crest at 3 months, Refit demonstrated the highest mineralized tissue and osteoid occupancy after 3 months, albeit without statistical significance. Conclusions: Overall, the materials demonstrated varying post-implantation behaviors in vivo. Thus, in a clinical setting, both the properties of these materials and the specific conditions of the defects needing reinforcement should be considered to identify the most suitable material.

Development of A-ABR system for identifying difficulty in hearing (난청 감별을 위한 자동청성뇌간반응검사(A-ABR) 측정기 개발)

  • No, Hyung-Wook;Kim, Soo-Chan;Cha, Eun-Jong;Kim, Deok-Won
    • Proceedings of the KIEE Conference
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    • 2008.04a
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    • pp.141-142
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    • 2008
  • Hearing loss is the most common birth defect among infants. Yet most hearing-impaired children are not identified until 1 to 3 years of age - which is well beyond the critical period(6 month) for healthy speech and language development. However, if a hearing-impairment is identified and treated in its early stages, child's speech and language skills will be comparable to his or her normal- hearing peers. For these reasons, hearing screening at birth and routinely throughout childhood is extremely important. Auditory brain-stem response(ABR) is nowadays one of the most reliable diagnostic tools in the early detection of hard of hearing. In this study, we developed the system that detects auditory evoked potential using micro-processor. Furthermore, it is required to develop a portable system to measure in not only soundproof room but also nursery for infants.

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Color Enhancement of the Type II and Type I aB Brown Diamonds into Colorless by HPHT Process (고온고압법에 의한 Type II, Type I aB 갈색 다이아몬드의 색향상)

  • Song, Jeong-Ho;Song, Oh-Sung
    • Journal of the Korean Ceramic Society
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    • v.49 no.3
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    • pp.221-225
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    • 2012
  • It is possible to enhance the color of the natural diamond with a high pressure high temperature(HPHT) process. We employed a pyrophyllite tube cell and cubic press apparatus for HPHT treatment on the brown colored Type II (5.6 GPa/ $1700^{\circ}C$/ 52 min), and Type I aB(5.6 GPa/ $1650^{\circ}C$/ 30 min) diamond samples. We investigated the microstructure, Types, fluorescence, properties of the diamonds with an optical microscopy, FT-IR, photoluminescence(PL) spectroscopy, Diamond-View, and micro-Raman spectroscopy. Two tinted brown diamonds changed into colorless just after the HPHT process. Optical microscopy showed that no crack and significant inclusion evolution occurred during the HPHT process except the small graphite spot appeared in Type I aB sample. FTIR spectrum confirmed that no Type, amber center, and platelet defect change with the HPHT treatment. Diamond-View could not distinguish the HPHT treated diamonds from the naturals. PL spectroscopy showed that N3 and H3 color centers remained even after HPHT process. Consequently, we successfully changed the color of diamonds into colorless by 5.6 GPa HPHT process.

Wafer-level Fabrication of Ball Lens by Cross-cut and Reflow of Wafer-bonded Glass on Silicon

  • Lee, Dong-Whan;Oh, Jin-Kyung;Choi, Jun-Seok;Lee, Hyung-Jong;Chung, Woo-Nam
    • Journal of the Optical Society of Korea
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    • v.14 no.2
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    • pp.163-169
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    • 2010
  • Novel wafer-level fabrication of a glass ball-lens is realized for optoelectronic applications. A Pyrex wafer is bonded to a silicon wafer and cross-cut into a square-tile pattern, followed by wet-etching of the underlying silicon. Cubes of Pyrex on the undercut silicon are then turned into ball shapes by thermal reflow, and separated from the wafer by further etching of the silicon support. Radial variation and surface roughness are measured to be less than ${\pm}3\;{\mu}m$ and ${\pm}1\;nm$, respectively, for ball diameter of about $500\;{\mu}m$. A surface defect on the ball that is due to the silicon support is shown to be healed by using a silicon-optical-bench. Optical power-relay of the ball lens showed the maximum efficiency of 65% between two single-mode fibers on the silicon-optical-bench.

Study about material properties of Al particles and deformation of Al alloy substrate by cold gas dynamic spray (초음속 저온분사법에 의한 알루미늄 합금 모재의 변형과 적층된 알루미늄 층의 물성에 대한 연구)

  • Lee, J.C.;Ahn, S.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2006.05a
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    • pp.145-148
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    • 2006
  • Cold gas dynamic spray is a relatively new coating process by which coatings can be produced without significant heating during the process. Cold gas dynamic spray is conducted by powder sprayed by supersonic gas jet, and generally called the kinetic spray or cold-spray. Cold-spray was developed in Russia in the early 1980s to overcome the defect of thermal spray method. Its low process temperature can minimize thermal stress and also reduce the deformation of the substrate. Most researches on cold-spray have focused on micro scale coating, but our research team tried to apply this method to macro scale deposition. The macro scale deposition causes deformation of a thin substrate which is usually convex to the deposited side. In this research, the main cause of the deformation was investigated using 6061-T6 aluminum alloy and properties of deposited aluminum layer such as coefficient of thermal expansion, Elastic modulus, hardness, electric conductivity were measured. From the result of the analysis, it was concluded that compressive residual stress was the main reason of substrate deformation while CTE had little effect.

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Time-Frequency Analysis of Lamb wave mode (램파모드의 시간-주파수 해석)

  • 박익근;안형근
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.10 no.1
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    • pp.133-140
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    • 2001
  • Recently, to assure the integrity of a structural components such as piping pressure vessels and thinning structure, Lamb wave inspection technique has been used in material evaluation. It is very important to select the optimal Lamb wave mode and to analyze the signal accurately because of its unique dispersion properties grnerating several modes within the speci-men. It this study, the feasibility of material evaluation applications using wavelet analysis of Lamb wave has been veir-fied experimentally. These results show as follows; 1)dispersion characteristic of each mode in dispersion curve is demon-strated that A0 mode propagating material surface is useful mode having the lest energy loss and not sensitive to surface condition. 2) it can be detected even the micro defect ($1\times2mm$) fabricated in ultrasonic probe flaw distance (290mm) to axis direction. 3) the wavelet transform which is called "time-frequency analysis" shows the Lamb wave propagation due to the change of materials characterization can be evaluated at each frequency and experimental group velocity of Lamb wave agrees quite well with that of simulated dispersion curve.ion curve.

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A Study on the Solidification Structure of Al-Si Alloy by the Continuous Casting with the Heated Mold (가열주형식 연속주조법에 의한 Al-Si합금의 응고조직에 관한 연구)

  • Kim, Won-Tae;Moon, Jeong-Tak;Kim, Myung-Han;Jo, Hyung-Ho
    • Journal of Korea Foundry Society
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    • v.14 no.5
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    • pp.464-470
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    • 1994
  • The horizontal continuous casting method with the heated mold was applied to study the solidification structures of the pure Al and Al-0.5wt%Si and Al-1.0wt%Si alloy rods. The results could be summarized as follows: 1. The S/L interface structures of pure Al represented the hexagonal cells at the casting speed of 590 and 350mm/min, respectively. However, the hexagonal cells became irregular as the casting speed and(or) Si amount increased. 2. The striation increased as the Si amount and casting speed increased and was found to result from the occurrence of growth twin crystals by XRD analysis. 3. The striation did not affect the mechanical and electrical property of the drawn wire from the casted rod. This means the striation is not a serious defect which has to consider in the production of micro-sized fine wire in the drawing process.

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