• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.516-521
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• 2002

A study was carried out to grow an understanding of the microstructural development of friction stir welds on an AZ91D magnesium alloy, and to evaluate the mechanical properties of the welds. AZ91D plates with the thickness of 4mm were used, and the microstructural development of the weld zone was investigated using optical and scanning electron microscopes. Square butt welding joint with good quality was obtained at the conditions of under 187mm/min of travel speed with 1100 to 1250 rpm of tool rotation speed. The microstructure within the weld region consisted of fine equiaxed grains with no evidence of the original dendritic structure. The hardness tests showed slightly increased harness in the weld region, and the minimum hardness measured is in that of the parent material. Tensile strength of the weld zone was remarkably improved due to very fine recrystallized structure. XRD pattern of weld zone revealed the removal of $\beta$ intermetallic compounds, $Mg_{17}$Al$_{12}$, which had been distributed in the base metal.l.

• 한국마린엔지니어링학회:학술대회논문집
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• 한국마린엔지니어링학회 2006년도 전기학술대회논문집
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• pp.265-266
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• 2006

The chemical conversion coating formed on magnesium alloy investigated for low cost and harmless in environment by using the colloidal silica as the main component. The film formed in 298 K is thick, the film, which was thought combination of Si-O, was formed. The film formed in 313 K is thinner than that in 298 K. The quantity of film formed at high temperature such as 333 K and 353 K is smaller than dissolved quantity. At the anodic polarization experiment, corrosion resistance in sealing by hot water after chemical conversion treatment in basic solution condition get worse than that in comparison with basic solution condition. In salt spray test, the ratio of black rust on specimen that did not conducted chemical conversion treatment was five times or more compared with those of chemical conversion treated specimen. The film thickness of chemical conversion coating produced by alkali treatment process is thinner than in comparison with that of specimen produced in basic chemical conversion treatment solution condition. It is thought, however, that it showed good corrosion resistance during salt spray test because the area of microcracks is small.

• 소성∙가공
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• 제27권3호
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• pp.145-153
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• 2018

Magnesium material could be widely used in the automotive industry because of its high strength to weight ratio, but the electric resistance spot welding process of magnesium sheets is difficult because of its low electric resistance and high thermal conduction and thermal expansion. For this reason, an electric resistance surface friction spot welding process using rotating dies is suggested for the spot welding of magnesium metal sheets. This welding method can be characterized by three heating methods: (1) electric resistance heating on contacted surface, (2) surface friction heating by rotating dies, and (3) thermal conduction heating from heated steel electrodes, for the fusion of metal at the interfacial zone between the two magnesium sheets. This welding process also has variables to explore, such as welding currents, diameters of the steel electrode, and rotating dies. It was found that the welding strength could reach industrial requirements by applying a welding current of 11.0kA, with steel electrodes of 12mm diameter, with rotating dies of 4.4 mm diameter, under the condition of a revolution speed of 1200rpm of rotating dies, for the surface friction spot welding process of AZ31 magnesium alloy sheets of 1.4mm thickness.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2010년도 춘계학술발표대회 초록집
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• pp.93-93
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• 2010

환경 규제 및 배출가스 규제에 의하여 차량 경량화를 위해 점차적으로 Al합금의 차체 및 부품적용 비율이 점차 확대되고 있다. 이에 따라 알루미늄의 레이저 용접 시 출력, 초점거리, 용접 속도 등 공정 변수의 상관관계와 용접 결함 현상에 의한 관심이 집중된 연구가 많이 발표되었으며, 알루미늄 5000계열의 경우 박판 용접 시 기공, 균열 등 과 같은 결함 현상을 방지하기 위하여, Twin spot laser, Laser-TIG hybrid 등과 같은 공법 적용을 제안되었다. 본 연구에서는 Yb:YAG laser welding 시 Mg 함량이 높은 AA5J32을 소재를 이용하여 박판 겹치기 용접 시 Back side spiking 결함 방지를 위한 레이저 빔 출력 파형을 설계하여 실험을 수행하였다. 또한 파형의 특성에 따라 나타나는 겹치기 용접부의 기계적 특성과 기공에 대해 알아 보고자 하였다.

• 한국재료학회지
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• 제9권7호
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• pp.715-723
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• 1999

마그네슘은 20여년간 자동차 산업에서 휠소재로 사용되어 왔다. 마그네슘 휠은 무게가 알루미늄 휠보다 25% 가벼워서 주행성이 우수하다. 이 연구의 목적은 사형주조 및 영구금형주조 공정에 의한 AZ91D 합금제 췰을 개발하는 것이다 보호개스$(SF_6+CO_2)$를 사용하는 비플럭스 용해기술을 적용하여 용탕의 산화와 불순물의 유입을 배제하였다 마그네슘 용탕은 가압식 펌프시스템을 사용하여 가열된 파이프를 통하여 모울드에 자동으로 공급된다. 열처리 및 인고트의 조성에 따른 AZ91B 합금제 휠의 기계적 특성을 조사하였다.

• 한국표면공학회지
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• 제23권1호
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• pp.34-43
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• 1990

Al-Si piston alloys such as AlS10CuMg have been anodized to examine apossibility of forming a hard film aat relatively higher temperatures compard with those in conventional sulfuric acid processes. Three types of electrolytes have been employed in this study ; electrolyte A(15% H2SO4, $0^{\circ}C$), electrolyte B(12% H2SO4, 1% oxalic, $10^{\circ}C$), electrolyte C(tartaric acid 125g/L+oxalic 75g/L+aluminum sulfate 225g/L, $25^{\circ}C$). Hard anodisine process in electrolyte B at a current density of 1.54A/dm2 produced a harder film of VHN 396 at a relatibely low film forming voltage compared with those obtained in other electrolyte at equivalent current density. A liner relationship between hardness and abrasion resistance exists for Al-Si piston alloys. The hardness of anodized film decreasees with increasing silicon content in Al-Si alloys and also with bath temperature. The film hardeness of Na-modified alloy os higher than that of P-modified alloy due to its finer microstructre. The film on the silicon phase in Al-Si alloys is observed to be formed by lateral growth of oxide film nucleated at surroundings.

• 소성∙가공
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• 제26권4호
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• pp.222-227
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• 2017

In order to respond to environmental regulations and increased demand for fuel economy, the demand for lightweight car bodies has grown. Hydroforming of aluminum is one possible solution as it eliminates the need for additional welding to develop closed cross-sectional parts. However, the low formability of aluminum is a limitation of its application. On the other hand, the ductility of materials can be improved at higher temperatures, and hot metal gas forming has been widely applied in the production of lightweight vehicle parts. In this study, aluminum alloy for pipe extrusion was developed by controlling the Mg:Cr:Mn ratio based on AA5083. Mechanical properties of the developed material were examined by tensile test and were applied to a forming simulation. Cold forming simulation for preforming and non-isothermal hot forming simulation for hot metal gas forming were carried out to validate process conditions. A prototype of the sidemember was manufactured under the given process condition. Finally, thickness distribution was compared with finite element analysis results.

• 한국재료학회지
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• 제25권5호
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• pp.221-225
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• 2015

In-situ neutron diffraction has been employed to examine the effect of strain path on lattice strain evolution during monotonic and cyclic tension in an extruded Mg-8.5wt.%Al alloy. In the cyclic tension test, the maximum applied stress increased with cycle number. Lattice strain data were acquired for three grain orientations, characterized by the plane normal to the stress axis. The lattice strain in the hard {10.0} orientation, which is unfavorably oriented for both basal slip and {10.2} extension twinning, evolved linearly throughout both tests during loading and unloading. The {00.2} orientation exhibited significant relaxation associated with {10.2} extension twinning. Coupled with a linear lattice strain unloading behavior, this relaxation led to increasingly compressive residual strains in the {00.2} orientation with increasing cycle number. The {10.1} orientation is favorably oriented for basal slip, and thus showed a soft grain behavior. Microyielding occurred in the monotonic tension test and in all cycles of the cyclic test at an applied stress of ~50 MPa, indicating that strain hardening in this orientation was not completely stable from one cycle to the next. The lattice strain unloading behavior was linear in the {10.1} orientation, leading to a compressive residual strain after every cycle, which, however, did not increase systematically from one cycle to the next as in the {00.2} orientation.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2012년도 추계총회 및 학술대회 논문집
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• pp.179-180
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• 2012

Aluminum alloys are widely known as non-ferrous metal with light weight and high strength. Consequently, these materials take center stage in the aircraft and automobile industry. The Al7075 aluminum alloy is based on the Al-Zn-Mg-Cu and one of the strongest wrought aluminum alloys. Aluminum nitride has ten times higher thermal conductivity($319W/m{\cdot}K$) than Al2O3 and also has outstanding electric insulation($1{\times}1014{\Omega}{\cdot}cm$). Furthermore, it has high mechanical property (430 MPa) even though its co-efficient of thermal expansion is less than alumina For these reasons, it has great possibilities to be used for not only the field which needs high strength lightweight but also electronic material field because of its suitability to be applied to the insulator film of PCB or wafer of ceramic with high heat conduction. This paper investigates the mechanical properties and corrosion behavior of aluminum alloy Al7075 deposited with aluminum nitride thin films To improve the surface properties of Al7075 with respect to hardness, and resistance to corrosion, aluminum nitride thin films have been deposited by pulsed DC reactive magnetron sputtering. The pulsed DC power provides arc-free deposition of insulating films.

• 한국전기전자재료학회논문지
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• 제13권8호
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• pp.711-717
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• 2000

Effect of alloying element additions to Ag on thermal conductivity electrical conductivity and mechanical properties of sheath materials for BSCCO tapes has been characterized. The thermal conductivity at low temperature range(10~300K) of Ag alloys were evaluated by both direct and indirect measurement techniques and compared with each other. It was observed that thermal conductivity decreased with increasing the content of alloying elements such as Au, Pd and Mg. Thermal conductivity of pure Ag at 30 K was measured to be 994.0 W/m.K on the other hand the corresponding values of A $g_{0.9995}$/M $g_{0.0005}$, A $g_{0.974}$/A $u_{0.025}$/M $g_{0.001}$, A $g_{0.973}$/Au.0.025//M $g_{0.002}$, and A $g_{0.92}$/P $d_{0.06}$/M $g_{0.02}$ were 342.6, 62.1, 59.2, 28.9 W/m.K respectively indicating 3 to 30 times lower than that of pure Ag. In addition alloying element additions to Ag improved mechanical strength while reduced elongation probably due to the strengthening mechanisms by the presence of additive atoms.s.