• Title/Summary/Keyword: Mg particles

Search Result 736, Processing Time 0.022 seconds

Microstructure and Mechanical Properties of Very-high-speed Extruded Mg-Bi-Al-Mn Alloy (Mg-Bi-Al-Mn 초고속 마그네슘 압출재의 미세조직 및 기계적 특성)

  • Cha, J.W.;Jin, S.C.;Park, S.H.
    • Transactions of Materials Processing
    • /
    • v.31 no.2
    • /
    • pp.73-80
    • /
    • 2022
  • In this study, a developed Mg-5Bi-2Al-0.4Mn (BAM520, wt%) alloy was successfully extruded at an extremely high speed of 70 m/min. Microstructural evolution during extrusion and the microstructural characteristics and tensile properties of the very-high-speed extruded BAM520 alloy were then investigated. The homogenized BAM520 billet contained only thermally stable Mg3Bi2 phase particles without any Mg17Al12 phase with a low melting temperature. Therefore, the BAM520 alloy exhibited excellent extrudability. The very-high-speed extruded BAM520 alloy had a completely recrystallized grain structure and a typical basal fiber texture. Despite the extremely high extrusion speed of 70 m/min, the extruded BAM520 alloy had a high ultimate tensile strength of 280 MPa due to combined strengthening effects of a small grain size, numerous fine Mg3Bi2 particles, and strong basal texture.

Fabrication of $Al_2O_{3p}/Al$ composites by in-situ Reaction Process of Molten Al (In-situ 반응에 의한 $Al_2O_{3p}/Al$기 복합재료의 제조)

  • 김재동;정해용;고성위
    • Composites Research
    • /
    • v.12 no.3
    • /
    • pp.36-44
    • /
    • 1999
  • The fabrication process of $Al_2O_{3p}/Al$ composite by in-situ process was investigated. The effects of processing variables such as addition type and content of Mg, processing temperature and time on the infiltration behavior of molten Al, microstructure and hardness were investigated. When the pure Al was infiltrated into mixtures of Mg and $Al_2O_3l$ powder, processing temperature required to spontaneous infiltration was decreased, and the content of Mg was the most powerful variable for infiltration of molten Al. But when the Al-Mg alloy was infiltrated into $Al_2O_3l$ particles, infiltration ratio indicated nearly same value regardless of Mg content in alloy and processing temperature, and critical processing temperature required to spontaneous infiltration was $800^{\circ}C$. The $Al_2O_{3p}/Al$ composites which were fabricated by mixtures of Mg and $Al_2O_3l$ powders resulted in high hardness value, but hardness values were scattered due to non uniform dispersion of $Al_2O_3l$ particles by excessive reaction of Mg.

  • PDF

Experiment on Settling Behaviour of Fine Mineral Particles (광물성 미립자의 침전거동에 관한 실험)

  • Kim, Jong-Woo
    • Journal of the Korean Society of Hazard Mitigation
    • /
    • v.5 no.1 s.16
    • /
    • pp.13-21
    • /
    • 2005
  • Experiments on settling behaviour of fine-grained particles without destroying the large fragile aggregates were carried out in still water with a CCD (Charged Coupled Device)-Camera. The experiments dealt with the measuring of the vertical concentration profile of cohesive particles with a CCD-Camera and the physico-chemical influences (NaCl, density, temperature and pH value) on the vertical distribution of the concentration. The vertical concentration profile of fine suspended particles (alumina and quartz) was possible up to $20,000\;mg/{\ell}$ with a CCD-Camera. The vertical concentration profile of cohesive sediments was on the decrease because of the increasing initial concentration, temperature and salinity. The vertical concentration profile of alumina was on the decrease quicker than quartz with increasing salinity. Furthermore, the pH value affects the settling behaviour of alumina. At a PH value of 4.2 the settling rate of the particles was very low and on the increase until pH 8.9 because of the aggregation behaviour of particles. From the PH value of 9 the average settling velocity was on the decrease.

Studies on Inactivation and Reactivation of Isolated Photosystem II Complexes in Spinach (시금치에서 분리한 광계 2 복합체의 불활성화와 재활성화에 대한 연구)

  • 전현식
    • Journal of Plant Biology
    • /
    • v.33 no.4
    • /
    • pp.277-283
    • /
    • 1990
  • Inactivation and reactivation of photosynthetic oxygen evolving complex were studied with isolated spinach (Spinacia oleraceda. L.) photosystem II particles by the activity of oxygen evolution and chlorophyll fluorescence. When the particles were treated with Tris and urea, the oxygen evolution was inactivated and three polypeptides having molecular weights of 33 kDa, 24 kDa and 18 kDa were simultaneously released. But in NaCl-treated particles, two polypeptides of 24 kDa and 18 kDa were removed from PS II particles. The oxygen evolution activities of Tris and urea-treated particles were not restored by adding cation ions (Mg2+, Mn2+ and Ca2+), but the NaCl-treated particles were restored by exogenously added Ca2+. The removal of these extrinsic polypeptides, especially 33 kDa, markedly showed the decrease of the variable fluorescence (Fv). These results are likely to be due to dissipate thermal energy by antenna of photosystem II complexes.

  • PDF

Effects of P2O5-doped on the Surface of MgO Particles for Hydrolysis, Water Repellency, and Insulation Behavior (MgO입자 표면에 도핑된 P2O5가 가수분해, 발수성, 그리고 절연거동에 미치는 영향)

  • Choi, Jin Sam
    • Applied Chemistry for Engineering
    • /
    • v.33 no.6
    • /
    • pp.588-593
    • /
    • 2022
  • The effects of P2O5-doped on the surface of MgO particles on hydrolysis, water repellency, and insulation behavior were investigated. P2O5-doped MgO has exhibited a unique electrical property, which is significant insulation behavior due to both the suppression of the hydrolysis reaction by P2O5 and water repellency. Therefore, the insulation behavior was inversely proportional to the hydrophilicity and the Mg(OH)2 and OH-charge transfer ratio by the surface hydration reaction of MgO. The insulation of MgO according to aging was strongly influenced by the surface hydration reaction, the band gap of the added dopant species, and the hydrophilicity and hydrophobicity of the dopant. Finally, it was to show electrical insulation by inhibiting the surface hydration reaction of the hydrophilic MgO, which has a great potential for use in heat transfer medium applications.

Magnetic Properties of Spherocarb Supported Nickel Particles (탄소에 분산된 니켈 입자의 자기 특성)

  • Kwan Kim
    • Journal of the Korean Chemical Society
    • /
    • v.27 no.5
    • /
    • pp.376-381
    • /
    • 1983
  • Dispersed nickel particles on Spherocarb were prepared at 540$^{\circ}C$ in various reaction atmosphere. Magnetic properties of these samples were determined, and results were compared with those of unsupported and MgO supported nickel particles. It was shown that nickel react primarily with carbon regardless of reducing atmosphere. In addition, apparent possibility of nickel-carbon interaction was discussed.

  • PDF

Preparation process of functional particles: III. Preparation of composite particles by rapid expansion of supercritical fluid solutions and release behavior (기능성 미분말의 제조공정에 관한 연구 : III. 초임계 분출법에 의한 복합분체의 합성과 용출특성)

  • ;;;Eiichi Abe
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.9 no.1
    • /
    • pp.55-59
    • /
    • 1999
  • The Rapid Expansion of Supercritical fluid Solutions (RESS) process was applied to particles coating. Microcapsules prepared by spray drying were used as the core particles, and two kinds of paraffin were used as the coating materials. Supercritical $CO_{2}$ solutions of paraffin were expanded through the short nozzle into the bed that was fluidized by air. Extraction temperature and pressure were varied at $50~120^{\circ}C$, $150~200\;kg/\textrm{cm}^2$, respectively. The thickness of theoritical coating layer ws measured, and precipitate coating layer on surface was analyzed by using SEM, FT-IR. The release behaviors of $Mg^{2+}$ ions were inspected by atomic absorbance spectrophtometer.

  • PDF

Synthesis of $Pb(Mg_{1/3}Nb_{2/3})O_3$ by $Li_2SO_4-Na_2SO_4$ Molten Salts ($Li_2SO_4-Na_2SO_4$ 용융염에 의한 $Pb(Mg_{1/3}Nb_{2/3})O_3$의 합성)

  • 윤기현;조용수;남윤우;강동헌
    • Journal of the Korean Ceramic Society
    • /
    • v.30 no.7
    • /
    • pp.543-548
    • /
    • 1993
  • Stability and formation of Pb(Mg1/3Nb2/3)O3 (PMN) phase synthesized in Li2SO4-Na2SO4 molten salts have been investigated. And powder characteristics of PMN have been studied with a variation of processing parameters such as temperature, time, amount of the salts, and excess PbO. More ratio of Li2SO4 to Na2SO4 influences the percentage of perovskite phase due to the difference of the eutectic point of the salts, but does not influence the powder characteristics. The shape of PMN particles shows faceted morphology with bimodal distribution consisting with large and submicron parts. Particle size of PMN increased greatly with increasing soaking time or amount of salts rather than temperature. The addition of excess PbO resulted in round PMN crystallites without submicron particles. These results are discussed by XRD, SEM and thermal analyses.

  • PDF

Fabrication of Ultra Fine MgO Particles Added BSCCO 2223 Tapes with Different Precursor Phase Constituent

  • Ko, Jae-Woong;Yoo, Jai-Moo;Kim, Hai-Doo;Chung, Hyung-Sik
    • Progress in Superconductivity
    • /
    • v.1 no.1
    • /
    • pp.56-60
    • /
    • 1999
  • Ultra fine MgO particles added BSCCO tapes were fabricated by tape casting using Doctor Blade Method and enclosed by silver foil for different starting compositions (that is, 2223 major, 2212 major). In order to obtain optimum microstructure, thermomechanical treatment was done. Microstructure and phase were analyzed by XRD, SEM and DTA. The critical current density was measured under magnetic field at 77K. The tapes fabricated from the precursor powder with BSCCO-2223 phase (>90%) result in a microstructure with a larger grain size and higher transport critical current density value under magnetic field at given thermomechanical treatment conditions.

  • PDF

Studies on the Chemical Compositions and Distributions of Ambient Sumicron Aerosols (Submicron 부유분진의 화학적 조성 및 분포에 관한 연구)

  • 황인조;김동술
    • Journal of Korean Society for Atmospheric Environment
    • /
    • v.14 no.1
    • /
    • pp.11-23
    • /
    • 1998
  • The purpose of this study was to survey chemical distribution of inorganic elements and ions in the submicron particles, to characterize qualitatively emitting sources by factor analysis, and finally to reveal existing patterns in terms of chemical compounds by a stepwise multiple regression analysis. Total of 141 samples were collected by a cascade impactor from 1989 to1996. Fifteen chemical species (Al, Ba, Cd, K, Pb, Cu, Fe, Ni, $Cl^-, NO_3^-, SO_4^{2-}, K^+, Mg^{2+}, Ca^{2+}, and Na^+$) were characterized by AAS and IC. The study showed that average seasonal levels of submicron particulate matters $(d_p<0.43 \mum)$ were 18.7 $\mug/m^3$ in spring, 15.5 $\mug/m^3$ in summer, 15.7 $\mug/m^3$ in fall, and 24.5 $\mug/m^3$ in winter, respectively. All of the anion concentrations in the particle were highest in the winter season. By applying a factor analysis, 5 source patterns were qualitatively obtained, such as sulfate related source, nitrate related source, oil burning source, calcium related source, and coal combustion source. Finally, when applying a stepwise multiple regression analysis, the results clearly showed that $Na^+ and Ca^{2+}, K^+ and Ca^{2+}, NO_3^-$ and relative humidity, $Cl^-$ and ambient temperature, $Ca^{2+} and Cl^-, Mg^{2+} and SO_4^{2-}, Na^+ and NO_3^-, and Ca^{2+} and NO_3^-$, respectively, are negatively contributed to each other. As a result of those statistical analysis, we could suggest that some chemical compounds in the submicron particles such as$NaNO_3, MgSO_4, Ca(NO_3)_2, and CaCl_2$ may not exist on the filter as final composing products; however, other compounds may possibly exist in the form of $Mg(NO_3)_2, CaSO_4, Na_2SO_4, K_2SO_4, MgCl_2, NaCl, and KCl$. Thus, it must be necessary to identify differences between the results of above statistical analysis and of the real world by laboratory experiments.

  • PDF