• Proceedings of the KWS Conference
• /
• 2002.10a
• /
• pp.516-521
• /
• 2002

A study was carried out to grow an understanding of the microstructural development of friction stir welds on an AZ91D magnesium alloy, and to evaluate the mechanical properties of the welds. AZ91D plates with the thickness of 4mm were used, and the microstructural development of the weld zone was investigated using optical and scanning electron microscopes. Square butt welding joint with good quality was obtained at the conditions of under 187mm/min of travel speed with 1100 to 1250 rpm of tool rotation speed. The microstructure within the weld region consisted of fine equiaxed grains with no evidence of the original dendritic structure. The hardness tests showed slightly increased harness in the weld region, and the minimum hardness measured is in that of the parent material. Tensile strength of the weld zone was remarkably improved due to very fine recrystallized structure. XRD pattern of weld zone revealed the removal of $\beta$ intermetallic compounds, $Mg_{17}$Al$_{12}$, which had been distributed in the base metal.l.

• Proceedings of the Korean Society of Marine Engineers Conference
• /
• 2006.06a
• /
• pp.265-266
• /
• 2006

The chemical conversion coating formed on magnesium alloy investigated for low cost and harmless in environment by using the colloidal silica as the main component. The film formed in 298 K is thick, the film, which was thought combination of Si-O, was formed. The film formed in 313 K is thinner than that in 298 K. The quantity of film formed at high temperature such as 333 K and 353 K is smaller than dissolved quantity. At the anodic polarization experiment, corrosion resistance in sealing by hot water after chemical conversion treatment in basic solution condition get worse than that in comparison with basic solution condition. In salt spray test, the ratio of black rust on specimen that did not conducted chemical conversion treatment was five times or more compared with those of chemical conversion treated specimen. The film thickness of chemical conversion coating produced by alkali treatment process is thinner than in comparison with that of specimen produced in basic chemical conversion treatment solution condition. It is thought, however, that it showed good corrosion resistance during salt spray test because the area of microcracks is small.

• Applied Microscopy
• /
• v.43 no.3
• /
• pp.122-126
• /
• 2013

The heterogeneous nucleation of the ${\Theta}^{\prime}$ phase on nanoscale precipitates has been investigated using a combination of three-dimensional atom probe tomography and high-resolution transmission electron microscopy. Two types of ${\Theta}^{\prime}$ phases were observed, namely small (~2 nm thick) cylindrical precipitates and larger (~100 nm) globular precipitates and both appear to be heterogeneously nucleated on the nanoscale precipitates. The composition and crystal structure of precipitates were directly analyzed by combination of two advanced characterization techniques.

• Journal of Korea Foundry Society
• /
• v.14 no.5
• /
• pp.471-479
• /
• 1994

Al-2%Si-2%Mg alloy containing SiC particle in 20, $70{\mu}m$ were prepared by mean of squeeze casting with various pressure 50, 100, 150 and 220MPa respectively. The specimens were made by casting into $50{\Phi}{\times}100{\ell}$ mold under various squeeze conditions(pressures, pressurizing temperature, particle sizes). Mechanical properties(hardness, tensile strength, elongation and wear characteristics) were evaluated at room temperature with those various fabrication factors. It became feasible to make favorable Al-SiCp composite free from casting defects by the injection of Ar gas during melting and 100MPa pressure squeeze casting. However, pressure of 50MPa was not sufficient to avoid completely porosity formation as a result of precessing and shrinkage during solidification. As the particle size is smaller and the squeeze pressure is higher, the hardness and tensile strength at room temperature are higher. Cell size became smaller gradually with increase of squeeze pressure. With increase of squeeze pressure(MPa), wear behaviors of those composites were changed from adhesive into abrasive wear, and the tendency of above behavior became outstanding with increasing sliding speed. The chemical reaction(4Al＋3SiC${\rightarrow}$$Al_4C_3+3Si$) is more accelerated at interface between SiCp and matrix with increase of squeeze pressure. Therefore $Al_4C_3$ intercompound and Si peak intensity is increased at interface.

• Proceedings of the KWS Conference
• /
• 2009.11a
• /
• pp.8-8
• /
• 2009

알루미늄 합금 Al 6082-T6는 최근에 개발되어 북유럽 등의 선진국에서는 그 뛰어난 해양 내식성과 우수한 강도로 인하여 해양구조물의 헬리데크(Helideck), 타워 갱웨이(Tower gangway), 알루미늄 피팅류(Aluminium fitting)등의 해양구조물과 플랫폼(Flatform), 알루미늄 래더(Aluminium ladder)등의 선박부품, 차량, 기계부품 분야에서 전 세계적으로 널리 사용되기 시작하였다. 그러나 전통적으로 용접금속의 기공은 결함으로 분류 되고, Rakesh Kumar 등의 논문에 따르면 용접 시 용접금속 내에 발생되어진 미세기공이 기계적 성질에 악영향을 미치는 것으로 보고되어졌다. 따라서 용접금속내의 발생하는 기공을 방지하는 용접공정의 개발이 반드시 필요하다. 본 연구의 목적은 Al 6082-T6 고속 MIG용접에서 기공방지를 위한 용접공정을 개발하는 것이다. Al 6082-T6의 7t 플레이트에 Al 5356의 와이어를 사용하여 아크길이 변경 및 용접속도를 60cpm과 120cpm으로 변경하여 실험하였고, 용접속도 120cpm의 고속 MIG용접에서 토치 진행각을 변경하여 실험을 진행하였다. 용접공정 파라메터 변경에 따른 기공율 측정은 이미지 분석 소프트웨어를 사용하여 정량적으로 분석하였다.

• Journal of the Korean institute of surface engineering
• /
• v.53 no.6
• /
• pp.322-329
• /
• 2020

The utilization of aluminum scrap is a subject of great importance in terms of reducing energy consumption and environmental protection. However, aluminum scrap contains impurities, which can degrade the properties of aluminum alloy, especially corrosion resistance. This study examines the effect of scrap charge rate of aluminum alloys about microstructures and corrosion characteristics. According to the metallographic examinations, Mg2Si tended to become coarser and its uniformity was decreased by increasing aluminum scrap charge rate. The immersion test exhibited corrosion progressed through the eutectic areas due to micro-galvanic interactions. Electrochemical measurements revealed that excess aluminum scrap could reduce the intergranular corrosion resistance of aluminum alloys. Results showed that the scrap charge rate is important factor in the design of corrosion resistance of aluminum die casting alloys.

• Journal of Powder Materials
• /
• v.14 no.2 s.61
• /
• pp.116-122
• /
• 2007

It is well known that thermal plasma process has lots of advantages such as high temperature and good quality for synthesis of nano particles. In this research, we attempt the synthesis of nano unitary and composite powder (Ag, Mg-Al, Zr-V-Fe) using transferred thermal plasma. Nano particles of metal alloy, ranging from 20 nm to 150 nm, have been synthesized by this process.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 1999.03b
• /
• pp.165-168
• /
• 1999

The coil design of induction heating systems and their optimization are of paramount importance for semi-solid processing(SSP) The authors of this paper present the coil design and optimization of a 60 Hz induction heating system for ALTHIX 86S (Al-6%_Si-3%Cu-0.3%Mg) alloy. An objective function on the basis of the optimization process for the coil design is proposed by introducing an optimization technique. Finally the results of the optimal coil design are also applied to the induction heating process to obtain a fine globular microstructure. The proposed new objective function based on the computational techniques would contribute to obtaining the thixoformed components with good mechanical properties and reducing lead time.

• Proceedings of the KWS Conference
• /
• 2002.10a
• /
• pp.505-510
• /
• 2002

The Friction Stir Welding (FSW) is a new joining method that was developed at The Welding Institute (TWI) in England in 1991. It applied heating by the rotational friction and material plastic flow. It was developed as a new joining method to solve the problems of epochally in the welding of Al alloys. In the study, 6000series of Alloy composed of AI-Mg-Si, one of the Al alloys that are utilized for shipbuilding and construction, is selected as a specimen and the numerical is executed against the welded zone of FSW. The material used in this study had the unique properties of strength and anti-corrosion, but since the welded joint of this material is easily softened by the welding heat, FSW is executed and the numerical analysis is carried out around the joint. To examine the mechanical behaviors and properties, F.E.M analysis is executed and the developed thermal-elastic-plastic [mite analysis are used.

• Journal of the Korean Ceramic Society
• /
• v.43 no.10 s.293
• /
• pp.646-652
• /
• 2006

Several oxynitride glasses were fabricated by means of adding $Si_3N_4$ powders as nitrogen source to Ca-Al-Si-O-N (CAS) and Mg-Al-Si-O-N (MAS) glass powders, and heat-treated in graphite crucible at 1600$^{\circ}C$ for 1 h. The physical and mechanical properties as well as impact resistance were generally increased and compared with each other. The impact resistance properties of those manufactured glasses were evaluated by DOP (depth of penetration) method which is a way to analyze armor materials. There were two means to be used herein; the copper jet impacted at hyper velocity by exploding K2l5 warhead and tungsten heavy alloy (WHA) impact bar at high velocity by firing in 30 mm solid propellent gun. The impact resistance properties against copper jet were increased and then decreased with increasing nitrogen content, while those against WHA bar were not changed apparently with nitrogen content.