• The Transactions of the Korean Institute of Electrical Engineers A
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• v.55 no.1
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• pp.7-12
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• 2006

This paper proposes the new voltage event detection method using the weight factor of neural network and describes control system design for the DVR(Dynamic Voltage Restorer) consisted of a rectifier and series inverter applied to 22.9kV distribution system. As this method can express the fault level of each phase, we expect the proposed method can make up for disadvantage of synchronous detection method. Also, in this paper, the control system was designed using double deadbeat controller, As it has an inner current control loop and an outer voltage control loop, we can easily limit the current level during the transient intervals by using the current control loop. Simulation and experiment are performed to prove the analysis of the voltage event detection method and double deadbeat controller.

• Economic and Environmental Geology
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• v.29 no.1
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• pp.21-24
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• 1996

Inductively coupled plasma atomic emission spectrophotometer (ICP/AES) is a versatile modern instruments for the multi-element analysis, but quantitative analysis using ICP/AES with normal pneumatic nebulizer is not applicable for the measurement of elemental concentrations in water down to the drinkining water standard level except a few elements because of poor detection limits. However, the detection limit can be lowered enough to measure drinking water standard, if ultrasonic nebulizer and/or hydride vapor generator is attached. This method is tested with groundwater samples from Tajeon area. It is confirmed that the elemental concentrations in these samples are within the limit of drinking water standard for the most elements. However, uranium concentration is very high in some samples compared with the concentrations suggested by Environmental Protection Agency of U.S.A. There is no standard concentration level to this element in Korea and it should be prepared immediately.

• The Journal of Engineering Geology
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• v.24 no.2
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• pp.191-199
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• 2014

We describe a method for detecting slope instability in flume tests using pore pressure and water content data in conjunction with a statistical control chart analysis. Specifically, we conducted univariate statistical analysis on x-MR control chart data (pore pressure and water content) collected at several points along the flume slope, which we separated into three parts: upper, middle, and lower. To assess our results in the context of landslide forecasting and warning systems, we applied control limit lines at $1{\sigma}$, $2{\sigma}$, and $3{\sigma}$ levels of uncertainty. In doing so, we observed that dispersion time varies depending on the control limit line used. Moreover, the detection of instabilities is highly dependent on the position and type of sensor. Our findings indicate that different characteristics of the data on various factors predict slope failure differently and these characteristics can be identified by univariate statistical analysis. Therefore, we suggest that a univariate statistical approach is an effective method for the early detection of slope instability.

• Korean Journal of Veterinary Research
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• v.48 no.1
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• pp.9-16
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• 2008

A method for the quantification of eugenol in the medicinal herb Clove was developed and validated. For preparation of sample solutions clove was dried at $60^{\circ}C$ for 2h and ground by mixer and extracted with 95% ethanol for shaking extraction. The elutes were analyzed by HPLC system included a reversed phase column, a isocratic mobile phase of 60% methanol and PDA detector set at 280 nm. Calibration graphs were linear with very good correlation coefficients ($r^2>0.9999$) from $0.0125~1{\mu}g/ml$. The limit of detection per sample injection ($20{\mu}l$) was $0.81ng/{\mu}l$ and limit of quantification was $2.47ng/{\mu}l$. The method showed good intra-day precision (%RSD 0.08 ~ 0.27%) and inter-day precision (%RSD 0.32 ~ 1.19%).

• Analytical Science and Technology
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• v.8 no.3
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• pp.237-248
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• 1995

The simultaneous analysis of 16 organic pesticides, which are listed as a part of 129 priority pollutants by EPA(Environmental Protection Agency), was performed by GC-ECD(electron capture detector) and GC/MS-SIM(selected ion monitoring). Two extraction procedures from SW-846, sonication extraction and Soxhlet extraction, were somewhat modified and compared as an extraction and concentration method for the analysis of priority pollutants in soil. Accuracy and precision of the methods were reported from the calculation of mean recovery, mean relative standard deviation, and method detection limit.

• YAKHAK HOEJI
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• v.42 no.2
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• pp.149-152
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• 1998

A high performance liquid chromatographic method was developed for the determination of DA-6034 in biological fluids using internal standard. Plasma containing DA-6034 and inter nal standard was extracted by liquid-liquid extraction at an acidic pH. After evaporation of the organic layer, the drug and internal standard were reconstituted with mobile phase and injected into the column. They were separated by high performance liquid chromatography on inertsil ODS II column at 334 nm. The detection limit of DA-6034 in plasma was 0.02 ${\mu}$g/ml. In this method, the range of recovery and coefficients of variation were 96-110% and 0.40-3.78%, respectively. There was no interference from endogenous substances. Urine and bile were analysed using the deproteinization method and the detection limit of DA-6034 was 1${\mu}$g/l.

• Journal of the Korean Chemical Society
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• v.57 no.5
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• pp.568-573
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• 2013

A selective and sensitive method for simultaneous determination of copper in blood by adsorptive differential pulse cathodic stripping voltammetry is presented. The procedure involves an adsorptive accumulation of Cu(II)-ETSC (4- ethyl-3-thiosemicarbazide) on a hanging mercury drop electrode, followed by a stripping voltammetry measurement of reduction current of adsorbed complex at about -715 mV. The optimum conditions for the analysis of copper (II) ion are : pH 10.3, concentration of 4-ethyl-3-thiosemicarbazide $3.25{\times}10^{-6}$ M and an accumulation potential of -100 mV. The peak current is proportional to the concentration of copper over the range 0.003-125 ng/mL with a detection limit of 0.001 ng/mL and an accumulation time of 60 s. Moreover, with the use of the proposed method, there is a considerable improvement in the detection limit, the linear dynamic range and the deposition time, compared with the methods of adsorptive stripping voltammetry for the determination of copper. The developed method was validated by analysis of whole blood certified reference materials.

• The Korea Journal of Herbology
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• v.23 no.4
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• pp.171-177
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• 2008

Objectives: This study presents a reversed-phase high-performance liquid chromatography- pulsed amperometric detection(RP-HPLC-PAD) method for the determination of puerarin and daidzin in Puerariae Radix extract and Chinese medicinal preparations. Methods: Chromatographic separation was performed using a 10% acetonitrile with a reversed-phase column(Unison UK-C18, $100mm{\times}2.0mm$ I.D.; $3{\mu}m$). The analyses were detected by pulsed amperometric detector(PAD) in alkaline conditions by combining with post-column NaOH solution. Geniposide was used as an internal standard. Results: The limit of detection(S/N=3) and the limit of quantification(S/N=10) were 0.025 ng, 0.075 ng for puerarin, and 0.05 ng, 0.15 ng for daidzin, respectively. The intra- and inter-day precisions(RSDs) were less than 6.5% and average recoveries of puerarin were 99.7-101.3% and those of daidzin were 101.0-102.8%. Conclusions: According to above results, we developed a determination method for puerarin and daidzin in Puerariae Radix with high sensitivity and selectivitely.

• The Journal of the Institute of Internet, Broadcasting and Communication
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• v.15 no.6
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• pp.291-296
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• 2015

The tire damage classification method is researched on the periodicity detection of ramdomness ultrasonic signals to occur at the driving vehicle tire. Setting method of adaptive threshold is proposed in order to valid pulse detection by tire damage in ultrasonic noise on the road and used low pass filter for decrease signal ramdomness as preprocessing. Time interval of detected pulse is setted the density function depend on the vehicle's speed and the method of tire damage detection is proposed that measuring the first peak's time of time density function.The result of time density function in case of one damage material, the first peak's time is measured within the error limit of tire's rotation period, 169.8ms and 97.9ms and 81.8ms, about the speed of 50km/h and 80km/h and 100km/h. In case of more than one damage material, the sum of each peak's time is measured within the error limit of tire's rotation period about the speed.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1998.10a
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• pp.60-65
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• 1998

Recently, It is gradually raised necessity that thickness of thin film is measured accuracy and managed in industrial circles and medical world. Ultrasonic Signal processing method is likely to become a very powerful method for NDE method of detection of microdefects and thickness measurement of thin film below the limit of Ultrasonic distance resolution in the opaque materials, provides useful information that cannot be obtained by a conventional measuring system. In the present research, considering a thin film below the limit of Ultrasonic distance resolution sandwiched between three substances as acoustical analysis model, demonstrated the usefulness of ultrasonic Signal processing technique using information of ultrasonic frequency for NDE of measurements of thin film thickness, sound velocity, and step height, regardless of interference phenomenon