• Journal of Korea Foundry Society
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• v.11 no.4
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• pp.323-330
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• 1991

The relationships between the microstructure changes, retained austenite volume and elevated temperature tensile properties of Mo-Ni-Cu ADI corresponding to various austempering temperatures and time were investigated, After the $250^{\circ}C$ tensile test for the test piece austempered at $270^{\circ}C$ the accicular bainite structure was observed blunted under room temperature microscope. In the case of $370^{\circ}C$ austempering, the feathery bainite lath spacing was observed broadened. But after the $450^{\circ}C$ tensile test, bainitic features could not be observed. As the testing temperature increased, retained austenite volume tested at room temperature decreased. Especially, after the $450^{\circ}C$ tensile test retained austenite volume approached nearly to zero. A little higher tensile properties appeared at $250^{\circ}C$ testing than those at room temperature.

• Applied Microscopy
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• v.16 no.2
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• pp.14-24
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• 1986

The interrelation of secondary defects, intermediate S' phase and aging condition in Al-2.0 wt% Cu-1.1 wt% Mg alloy is studied by transmission electron microscope. The results obtained in this study are as follows. 1. High density of dislocation loops, helices and stacking faults are observed in this specimen with aging treatment. 2. The number of dislocation loops and the width of loop free zone (LFZ) are increased with aging time. 3. The intermediate S' phase precipitates and grows on the dislocations and secondary defects. 4. The misfit dislocations are formed around intermediate S' phase. 5. It is thought that the helices appear to be produced by the climb of screw dislocations, while the dislocation loops appear to be formed both by condensation of vacancies into collapsed discs and by interaction of helices with screw of opposite sign.

• Applied Microscopy
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• v.43 no.3
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• pp.122-126
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• 2013

The heterogeneous nucleation of the ${\Theta}^{\prime}$ phase on nanoscale precipitates has been investigated using a combination of three-dimensional atom probe tomography and high-resolution transmission electron microscopy. Two types of ${\Theta}^{\prime}$ phases were observed, namely small (~2 nm thick) cylindrical precipitates and larger (~100 nm) globular precipitates and both appear to be heterogeneously nucleated on the nanoscale precipitates. The composition and crystal structure of precipitates were directly analyzed by combination of two advanced characterization techniques.

• Korean Journal of Materials Research
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• v.13 no.11
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• pp.756-760
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• 2003

Two dimensional computer simulations were conducted on percolative structure in which second phases with various short diameter were arranged in matrix phase. In case of prohibiting the overlap among the second phases, the maximum area fraction of second phase arranged in matrix was increased with higher short diameter. In case of allowing the overlap among the second phases, the critical area fraction was increased with higher short diameter and the total number of distributed second phase was decreased. This results represented that thickness variation of short diameter by grain growth on the production processes affect significantly forming the completion path.

• Journal of Korea Foundry Society
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• v.8 no.4
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• pp.459-466
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• 1988

This study was carried out in the austempering temperature and time after Ni, Mo addition in purpose of modification of impact toughness of austempered ductile irons. Addition of alloy element and austempering treatment of $900^{\circ}C$ 60 minutes followed by $300^{\circ}C$, $350^{\circ}C$ and $400^{\circ}C$ for 60 minutes, in this case impact value was increased by ideal mixed structure. But impact value was decreased when holing time is 120minutes, this is attributed to segregation and carbide precipitation from high carbon austenite. Highest impact value was obtained by $350^{\circ}C$ (Mo-addition) and $400^{\circ}C$ (Ni-addition). This phenomena was caused by presence of remained austenite. At all austempering temperature,, Ni-added specimen showed higher impact values than that of Mo-added specimen. And hardness property was affected by austempering temperature and holding time rather than amounts of alloying element.

• Journal of Korea Foundry Society
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• v.14 no.5
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• pp.429-437
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• 1994

Influence of interfacial structure between matrix and particle in A356/coated SiC composite fabricated by squeeze casting method was studied. Experimental variables are types of coated metallic film on SiC particles such as Cu, Ni-P, and applied pressure for squeeze casting. It was found that coating treatment on SiC particles improves the wetting of liquid A356 alloy on SiC particles. SiC particle distribution is very homogeneous in A356 matrix alloy which is fabricated by squeeze casting. Analysing the surface morphology of fractured A356/coated SiC, it was concluded that metallic thin film by coating treatment on SiC particle improves the interfacial bonding between particle and matrix, and so does on mechanical properties such as tensile strength. However, there was on significant difference in hardness between those composite made of as-received SiC particle and coated SiC particle.

• Journal of Korea Foundry Society
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• v.23 no.2
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• pp.63-68
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• 2003

Al-Ti-C grain refiner form a relatively new alternative to the existing class of Al-Ti-B type grain refiners for achieving fine equiaxed structures in aluminum alloys during casting and solidification. The present study was carried out to investigate the influence of Al-Ti-C master alloys on the grain structure of Al-7Si alloys. The present study also investigates the relationship between grain refining efficiency and concentrations of Fe and Si in hypo-eutectic Al-Si alloys using Al-3Ti-0.13C master alloys. It is found that several parameters affect significantly the grain refining performance in silumin alloys. The present study reports the influence of various parameters such as alloy content, master alloy addition level, melt holding time and superheat on the grain refining efficiency in Al-7Si alloys.

• Journal of the Korean institute of surface engineering
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• v.39 no.5
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• pp.223-228
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• 2006

The current efficiency of copper anode containing impurities in copper sulfate solution for electrorefining was studied at various current type such as direct current, variable current and periodic reverse current. The passivity behavior was investigated by galvanostatic technique. The results obtained were that current efficiency of variable current was higher than those of direct current and periodic reverse current. The increased current efficiency could be explained by the formation of slime structure with lower average resistance due to variable current. The frequency of various factors in variable current condition has a greatest effect on current efficiency. It appeared that frequency increased current efficiency when increased from 1 to 4, but further increases did not have an effect.

• Proceedings of the KIEE Conference
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• 2001.07d
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• pp.2544-2545
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• 2001

In industry and engineering, the tensile measurement of single crystal metal material such as the uniform change, surface structure and the tensile torque of the material is not easy to obtain by current the tensile measurement methods. In this paper, we have implemented a tensile system which can acquire tensile information in real time.

• Korean Journal of Materials Research
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• v.4 no.7
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• pp.741-749
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• 1994

The planar solid oxide fuel cell(SOFC) contains several ceramic materials depending on its structure and has rdfractory metal parts for manifolds, shrouds and current leads. Among ceramic materials for planar SOFC, joining of lanthanum chromite separator and yttria stabilized zirconia(YSZ) electoyte in planar SOFC stack to give strong gas tight seals is necessary for satisfactory operation and high performance. Nevertheless, for planar SOFC/sub s/, how to seal the cell stack and gas manifold remains as one of the unsolved problems. Therefore, in this study. we investigated the joining of sintered lanthanum chromite and YSZ pellets using unsintered lanthanum chromite green films as sealent. Scanning electron microscopy(SEM) and energy dispersive X-ray analysis(EDX) revealed that Ca in the sealing material diffused and dissolved into YSZ and sintered lanthanum chromite, and unsintered lanthanum chromite green films reacted with YSZ to from a new phase at the interface. Also, the densification of unsintered lanthanum chromite green films was inpeded by the Ca migration.