• Journal of Powder Materials
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• v.10 no.5
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• pp.310-317
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• 2003

Two-component ceramic (alumina-zirconia) composites were fabricated by a soft-solution process in which polyethylene glycol (PEG) was used as a polymeric carrier. Metal salts and PEG were dissolved in ethyl alcohol without any precipitation in 1:1 volume ratio of alumina and zirconia. In the non-aqueous system, the flammable solvent made explosive, exothermic reaction during drying process. The reaction resulted in formation of volume expanded, porous precursor powders by a vigorous decomposition of organic components in the precursor sol. The PEG content affected the grain size of sintered composites as well as the morphology of precursor powders. The difference of microstructure in sintered composite was attribute to the solubility and homogeneity of metal cations in precursor sol. At the optimum amount of the PEG polymer, the metal ions were dispersed effectively in solution and a homogeneous polymeric network was formed. It made less agglomerated particles in the precursor sol and affected on uniform grain size in sintered composite.

• Journal of Korea Foundry Society
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• v.25 no.2
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• pp.80-87
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• 2005

The microstructure and mechanical property of the Ni and Ni-Cr porous metal reinforced AC4C matrix composites fabricated by squeeze casting were investigated. In this study Ni, Ni-Cr porous metals which are estimated to be easy to fabricate by squeeze casting are used as strengtheners for composite materials. As a matrix material, Al-7wt.%Si-0.3wt.%Mg(AC4C) has been used. In case of Ni/AC4C and Ni-Cr/AC4C composite, $750^{\circ}C$ melt temperature and minimum 25MPa squeezing pressure are needed to produce sound composite materials. The observation of interfacial reaction zone at various heat treatment condition shows that atsolutionizing temperature of above $520^{\circ}C$, the interfacial reaction zone increases proportionally with heat treatment time and the reaction products formed by interfacial reactions are mainly composed by $Al_{3}Ni$ and $Al_{3}Ni_{2}$ phases.

• Journal of the Korean Society for Heat Treatment
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• v.7 no.3
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• pp.160-168
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• 1994

This was studied about mechanical characteristic of AC4A/SiCw 10-30% reinforced composites. Tensile strength of pressed base metal(base metal) with SiCw preform was higher than without pressed base metal(AC4A). If SiCw whisker volume fraction was increased, tensile strength at room temperature was increased. And tensile strength of SiCw 30% was about $35kg/mm^2$. Tensile strength of SiCw 30 % $400^{\circ}C$ at same time aging was the most excellence, about $40kg/mm^2$. The fracture energy value of composite material at three point bending test was higher than AC4A. Dislocation at matrix of composite material was evenly distributed. But dislocation around whisker of composite material was more existed than matrix. The reasom was thought of pile-up around whisker.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.11a
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• pp.183-186
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• 2000

A new textile metal matrix composite fur electronic packaging was developed and characterized. The thermal management materials consist of a plain woven carbon fabric as reinforcement and pure aluminum as matrix. The finite element method has been utilized in the analysis of thermal stress between the constituent components of packaging. The prototype part was manufactured by the liquid pressurizing method. The composite has CTE values of 4 to $5{\times}10^{-6}\;^{\circ}C^{-1}$10 in the range of $25^{\circ}C$ ~ 175$^{\circ}C$, resulting in good agreement with electronic materials such as Si and GaAs.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2001.05a
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• pp.38-41
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• 2001

A new 2-D braided textile metal matrix composite was developed and characterized. The constituent materials consist of PAN type carbon fiber as reinforcements and pure aluminum as matrices. The braided preforms of different braider yarn angles were fabricated. For a fixed bundle size of 12K, three braider yarn angles was selected: $30^{\circ}$, $45^{\circ}$, and $60^{\circ}$. The braided preforms were infiltrated with pure Al by vacuum assisted squeeze casting. Through the investigation of melt pressing methods and the effects of process parameters such as applied pressure, and pouring temperature, the optimal process conditions were identified as follows: applied pressure of 60MPa, pouring temperature of $800^{\circ}C$. Using the measured geometric parameters, 3-D engineering constants of metal matrix composites have been determined from the elastic model, which utilizes the coordinate transformation and the averaging of stiffened and compliance constants based upon the volume of each reinforcement and matrix material.

• Journal of Welding and Joining
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• v.20 no.3
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• pp.54-59
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• 2002

Overlays is a treatment of the surface and near-surface regions of a material to allow the surface to perform functions that are distinct from those frictions demanded far the bulk of the material. Welding, thermal spray, quenching, carburizing and nitration have been used as the surface treatment. Especially, weld overlay is a relatively thick layer of filler metal applied to a carbon or low-alloy steel base metal for the purpose of providing a wear resistant surface. In this study, weld overlay was performed by MAG welding on the base metal(SS400) with filler metal which contain composite powders($Cr_3C_2+Mn+Mo+NbC$) and solid wire(JIS-YGW11). Characteristics of hardness and wear resistance on overlays were analyzed by EDS, EPMA, XRD and microstructures. Carbide formations were $M(Cr, Fe)_7C_3$ and NbC phases. And carbide volume fraction, hardness and specific wear resistance of overlays were increased with increasing powder feed rate and decreasing wire fred rate. Hardness and wear resistance were almost proportioned to carbide volume fraction of overlay.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1999.05a
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• pp.548-551
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• 1999

The cure characteristics of metal particle filled DGEBA/MDA/SN/ zeolite epoxy resin composite system for EMI shielding were investigated by dynamic DSC run method and FT-lR spectroscopy. As the heating rate increased, the peak temperature on dynamic DSC curve increased because of the rapid cure reaction. From the straight line of the Kissinger plot, the curing reaction activation energy and pre-exponential factor could be obtained. As the post-curing time at 15$0^{\circ}C$ increased, the glass increased the glass transition temperature or the thermal stability increased. When the post curing time is too long, the system filled with metallic Al particle can be thermally oxidized by the catalytic reaction of metal filler and the thermal stability of the composite for the EMI shielding application may be decreased.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2002.08a
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• pp.80-83
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• 2002

In this study, a single phase driven piezoelectric motor design is presented for linear motion-metal/ ceramics composite structure. Using ANSYS finite element analysis software, mode shape of free motor was obtained to clarify the working principle of this motor. And characteristics of the motor was measured. The motor is composed of a piezoelectric ceramic, a metal ring which has 4 arms, and a guider. The motor with 25.0[mm] diameter was studied by finite element analysis and experimentation too. As a result, the motor was expressed the best speed in resonance frequency. And according as voltage of the motor increase, the speed increased by ratio.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.11a
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• pp.45-48
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• 2005

In manufacturing process of composite cylinders with metal liner, the autofrettage process which induces compressive residual stress on liner to improve cycling life can be applied. In this study, finite element analysis technique is presented, which can predict accurately the compressive residual stress on liner induced by autofrettage and stress behavior after. Material and geometry non-linearity is considered in finite element analysis, and the Von-Mises stress of a liner is introduced as a key parameter that determines pressure cycling life of composite cylinders. Presented methodology is verified through fatigue test of liner material and pressure cycling test of composite cylinders.

• Journal of Mechanical Science and Technology
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• v.17 no.2
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• pp.171-180
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• 2003

One of the most significant problems in the processing of composite materials is residual stress. The high residual stress may cause cracking in the matrix without external loads and degrade the integrity of composite structures. In this study, thermo-viscoelastic residual stresses occurred in an aluminum liner-inserted polymer composite cylinder are investigated. This type of the structure is used for rocket fuselage due to the convenience to attach payloads and equipment to the metal liner by machining. The time and degree of cure dependent thermo-viscoelastic constitutive equations are developed and coupled with a thermo-chemical process model. These equations are solved with the finite element method to predict the residual stresses in the composite cylinder and also in the interface between the liner and the composite during cure.