• 제목/요약/키워드: Melting treatment

검색결과 357건 처리시간 0.025초

ZnS 미립자 분산 붕규산엽계 유리에서의 분상 및 미립자 석출 특성 (Phase Separation and Precipitation Characteristics in ZnS doped Borosilicate Glasses)

  • 이승환;류봉기
    • 한국세라믹학회지
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    • 제35권12호
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    • pp.1337-1342
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    • 1998
  • To investigate an effect of phase separation on precipitation characteristics of ZnS microcrystals in ma-trix glass ZnS doped borosilicate glasses for nonlinear optical applications were prepared by melting and pre-cipitation process. ZnS dopant contributed to phase separation promotion which increased the phase separa-tion of the matrix glass within immiscibility region. It was also found that ZnS as phase separation promoter showed a similar contribution for some selected glass compositions in miscibility region. The precipitation of ZnS microcrystals occurred in thephase separable glass compoitions. The radius of ZnS microcrystals in-creased with increasing the heat treatment temperature and Na2O contents of matrix glass composition. The ZnS particle sizes estimated by effective mass approximation ranged from about 30 to 80${\AA}$ It was suf-ficiently small to show quantum confinement effect.

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Polyester Film Laminating Technology for Chip Condenser

  • Lee, Yun Dai;Son, Yang Soo;Ahn, Joong Geol
    • Corrosion Science and Technology
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    • 제3권4호
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    • pp.172-177
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    • 2004
  • Biaxially oriented polyethylene terephthalate copolymer(BO - PET)film laminated aluminiums have been applied for chip condenser case. The BO PET film is characterized by high molecular which gives high corrosion resistance, good adhesion and high heat resistance. The higher orientation lowers formability of the film. So, optimum orientation has to be controlled during the laminating process. And to confirm the adhesion between BO PET and aluminium and to guarantee the formability of PET laminated aluminums, we have controlled the chromium oxides weight on the aluminium and laminating condition ( laminating temperature, soaking temperature and lag time after nip roll and quenching conditions) This paper discusses the effect of the laminating conditions on the formability of laminated aluminums. As results, it is clear that the orientation of the BO PET film decreased with an increase in the strip temperature. When the film temperature is over the melting point of the film, its orientation drastically decreased.

A Comparative Study on Corrosion Behavior of Ti-35Nb-5Ta-7Zr, Ti-6Al-4V and CP-Ti in 0.9 wt% NaCl

  • Saji, Viswanathan S.;Jeong, Yong Hoon;Choe, Han Cheol
    • Corrosion Science and Technology
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    • 제8권4호
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    • pp.139-142
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    • 2009
  • Recently, quaternary titanium alloys of the system Ti-Nb-Ta-Zr received considerable research interest as potential implant materials because of their excellent mechanical properties and biocompatibility. However, only few reported works were available on the corrosion behavior of such alloys. Hence, in the present work, electrochemical corrosion of Ti-35Nb-5Ta-7Zr alloy, which has been fabricated by arc melting and heat treatment, was studied in 0.9 wt% NaCl at $37\pm1^{\circ}C$, along with biomedical grade Ti-6Al-4V and CP-Ti. The phase and microstructure of the alloys were investigated employing XRD and SEM. The results of electrochemical studies indicated that the corrosion resistance of the quaternary alloy was inferior to that of Ti-6Al-4V and CP Ti.

열간압축성형으로 제조한 Co1-xNixSb3의 열전특성 (Thermoelectric Properties of Co1-xNixSb3 Prepared by Hot Pressing)

  • 김미정;어순철;김일호
    • 한국재료학회지
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    • 제16권6호
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    • pp.382-385
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    • 2006
  • Ni-doped $CoSb_3$ was prepared by the hot pressing, and its doping effects on the thermoelectric properties were investigated. Single phase ${\delta}-CoSb_3$ was successfully obtained by encapsulated induction melting and the subsequent heat treatment at 773 K for 24 hrs, followed by the hot pressing under 60 MPa at 773 K for 2 hrs. Nickel atoms acted as electron donors by substituting cobalt atoms. Thermoelectric properties were remarkably improved by the Ni doping.

LC 직렬공진에 의한 전기 수술기 개발 (Development of electric surgical machine by LC series resonance)

  • 이오걸;김태우;송호신
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2002년도 학술대회 논문집 전문대학교육위원
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    • pp.153-157
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    • 2002
  • Electricity living body formation operation appliance is using most imports until present. And, because electricity living body formation operation appliance is too expensive, it becomes burden to buy in small scale hospital. Also, problem that economical damage by income is added follows, Therefore, this treatise developed electricity living body formation operation appliance by home production, Ultra high frequency eruption circuit used LC circuit, and output frequency is possible to 8 [MHz], and output voltage amplified maximum 800 [V]. This operation appliance could display size of fixed current. This developed product could microscopic operation fewer than 1 [mm]. This development technology is considered by do metallic surface heat treatment, melting, welding, induction heating device and that can apply to domestic animals surgical operation and so on.

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Nb이 첨가된 Ti합금의 미세 조직 및 산화 거동 (Effects of Nb Addition on Microstructure and Oxidation Behavior of Ti Alloy)

  • 이도재;이광민;이경구;박범수;김수학;전충극;윤계림
    • 한국표면공학회지
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    • 제37권1호
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    • pp.58-63
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    • 2004
  • The oxidation behavior of Ti-Nb alloys was studied in dry atmosphere. After vacuum arc melting and hot rolling treatment, Ti-Nb alloys were oxidized at $450^{\circ}C$$750^{\circ}C$. The oxidation behaviors between matrix and oxide scale were analyzed by SEM, XPS and XRD. Ti-Nb alloys had higher oxidation resistance than pure Ti at $750^{\circ}C$. XPS analysis of oxide film revealed that $TiO_2$ oxide was formed on the top of surface. The weight gains during the oxidation increase rapidly at temperature above $600^{\circ}C$ which obey the parabolic law.

직렬공진에 의한 피부 수술기 개발 (Development of skin surgical machine by series resonance method)

  • 이오걸;김상주
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 춘계합동학술대회 논문집
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    • pp.127-132
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    • 2002
  • Electricity living body formation operation appliance is using most imports until present. And, because electricity living body formation operation appliance is too expensive, it becomes burden to buy in small scale hospital. Also, problem that economical damage by income is added follows. Therefore, this treatise developed electricity living body formation operation appliance by home production. Ultra high frequency eruption circuit used LC circuit. and output frequency is possible to 8 [MHz], and output voltage amplified maximum 800 [V]. This operation appliance could display size of fixed current. This developed product could microscopic operation fewer than 1 [mm]. This development technology is considered by do metallic surface heat treatment, melting, welding, induction heating device and that can apply to domestic animals surgical operation and so on.

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Surface Characteristics of Anodized Ti-30Nb-xTa Alloys with Ta Content

  • Kim, Eun-Sil;Ko, Yeong-Mu;Choe, Han-Cheol
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2012년도 춘계학술발표회 논문집
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    • pp.254-254
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    • 2012
  • The purposed of this work was to determine surface charateristics of anodized Ti-30Nb-xTa alloys with Ta content. Samples were prepared by arc melting, followed by followed by homogenization for 12 hr at $1000^{\circ}C$ in argon atmosphere. The electrolyte for anodization treatment was prepared by mixing 465ml $H_2O$ with 35M $H_3PO_4$ and anodized at 180V to 220V. The microstructures of the alloys were examined by X-ray diffractometer (XRD) and optical microscopy (OM). Surface characteristics of anodized Ti-30Nb-xTa alloys was investigated by potentiodynamic test and potentiostatic in 0.9% Nacl solution at $36.5{\pm}1^{\circ}C$. It was observed that the changed ${\alpha}$ phase to ${\beta}$ phase with Ta content.

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Formation of Particles in the Laser Melted Zone of Alloy 600

  • Lim, Yun-Soo;Cho, Hai-Dong;Kuk, Il-Hiun;Kim, Joung-Soo
    • 한국원자력학회:학술대회논문집
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    • 한국원자력학회 1997년도 춘계학술발표회논문집(2)
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    • pp.80-85
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    • 1997
  • Studies on particles formed in the laser melted zone (LMZ) of sensitized Ni base Alloy 600 have been carried out using microscopic equipments. Most of them were identified as TiN type and MgS type particles were also found in the cell boundaries. All of the particles were located in the cellular solidification region, but no particle was formed in the plane front solidification regions of the LMZ. Cr carbides which had formed during sensitization treatment were completely melted during laser surface melting and hardly re-precipitated during the matrix solidification.

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디젤 엔진용 캠축 소재의 금속적 특성 및 선삭 가공 특성에 관한 연구 (Turning and Metalic Characterization for CAM Shaft Materials of Diessel Engine)

  • 채왕석;김경우;김동현
    • 한국정밀공학회지
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    • 제14권7호
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    • pp.22-28
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    • 1997
  • In this paper, We have studied internal quality incluiding chemical compositions, microscopic structure and nonmetalic inclusion of test material. We have analyzed dynamic characteristics of cutting resistence and compared chip treatment of the test material. In analyzing internal quality, all of the test material have typical ferrite+pearlite structure. But, nonmetallic inclusion has oxide and sulfide inclusion has oxide and sulfide inclusion in medium carbon steel, mainly sulfide inclusion is existed in S-free cutting steel. In Ca+S-free cutting steel, calcium aluminate and sulfide complex inclusion, had low-melting point, as deformation of sulfide and oxide inclusion is existed. Machining characteristics, cutting resistence is maximum in medium carbon steel. Chip treatement are excellent in S-free cutting steel, similar to the Ca+S free cutting steel and medium carbon steel.

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