• 한국재료학회지
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• 제16권6호
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• pp.377-381
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• 2006

Skutterudite $CoSb_3$ doped with nickel was prepared by encapsulated induction melting, and its doping effects on thermoelectric properties were investigated. Single phase ${\delta}-CoSb_3$ was successfully obtained by encapsulated induction melting and subsequent heat treatment at 773 K for 24 h. Nickel atoms acted as electron donors by substituting cobalt atoms. Thermoelectric properties were remarkably improved by appropriate heat treatment and doping, and they were closely related to phase transitions and dopant activation. The maximum ZT(dimensionless figure of merit) was achieved as 0.2 at 600 K for the $Co_{0.93}Ni_{0.07}Sb_3$ specimen.

• 대한치과보철학회지
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• 제59권2호
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• pp.248-260
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• 2021

코발트-크롬 합금은 다양한 치과보철물 제작에 이용되고 있고, 다른 합금에 비해 저렴한 가격과 우수한 기계적 특성이 장점이다. 최근, 기존 제작 방식의 단점을 극복하기 위해 적층제조 방식인 선택적 레이저 용융 방법이 보철물 제작에 이용되고 있다. 선택적 레이저 용융 방법의 공정 중 급속 가열과 냉각 과정은 제작된 합금의 미세구조와 결정립을 미세화하고, 기포를 감소시켜 기존 제작 방식에 의한 합금에 비해 기계적 특성을 향상시킨다. 반면, 적층과 급속 가열 및 냉각은 다량의 잔류응력 축적을 초래하는데, 추후 기계적 특성에 악영향을 미칠 수 있다. 따라서, 잔류응력을 제거하기 위해 주로 열처리를 시행하고, 회복과 재결정화에 의한 잔류응력의 감소뿐만 아니라 상변태, 석출물 및 미세구조의 균질화가 동반되어 기계적 특성의 복잡한 변화가 나타난다. 본 문헌고찰에서 코발트-크롬 합금의 제작 방식 비교 및 선택적 레이저 용융 방법으로 제작된 합금의 특징에 대해 알아보고자 한다.

• 전기학회논문지
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• 제65권1호
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• pp.73-80
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• 2016

The preliminary test for the dual mode plasma torch system was carried out to explore the operation properties in advance. The dual mode plasma torch system that is able to operate in transferred, non-transferred, or dual mode is very adequate for melting the mixed wastes including nonconductive materials such as concrete, asbestos, etc. since it exploits both the high efficiency of heat transfer to the melt in transferred mode and stable operation in non-transferred mode. Also, system operation including restarting is reliable and very easy. A stationary melter with a refractory structure was designed and manufactured considering the melting behavior of slags to minimize the refractory erosion. The power supply for the dual mode plasma torch system built with high power insulated gate bipolar transistor (IGBT) modules has functions for both current control and voltage control and is sufficient to suppress the harmonics during the operation of the plasma torch. The power supply provides two different voltages for transferred operation and non-transferred. It is confirmed that the operation voltage in transferred is always higher than non-transferred. The dual mode plasma torch system was successfully developed and is under operation for a melting experiment to optimize operation data.

• 한국재료학회지
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• 제32권6호
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• pp.287-292
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• 2022

Magnesium-antimonide is a well-known zintl phase thermoelectric material with low band gap energy, earth-abundance and characteristic electron-crystal phonon-glass properties. The nominal composition Mg_3.8-xZn_xSb₂ (0.00 ≤ x ≤ 0.02) was synthesized by controlled melting and subsequent vacuum hot pressing method. To investigate phase development and surface morphology during the process, X-ray diffraction (XRD) and scanning electron microscopy (SEM) were carried out. It should be noted that an additional 16 at. % Mg must be added to the system to compensate for Mg loss during the melting process. This study evaluated the thermoelectric properties of the material in terms of Seebeck coefficient, electrical conductivity and thermal conductivity from the low to high temperature regime. The results demonstrated that substituting Zn at Mg sites increased electrical conductivity without significantly affecting the Seebeck coefficient. The maximal dimensionless figure of merit achieved was 0.30 for x = 0.01 at 855 K which is 30% greater than the intrinsic value. Electronic flow properties were also evaluated and discussed to explain the carrier transport mechanism involved in the thermoelectric properties of this alloy system.

• 전기학회논문지
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• 제58권9호
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• pp.1775-1777
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• 2009

BiSrCaCuO films were prepared on MgO single substerate at $885^{\circ}C$ by melt process. The films showed superconductivity above liquid nitrogen temperature (Tc= 96K). To investigate the effect of a melting temperature on the forming of the surface texturing, the samples were prepared under various temperature. The used powder was of high Tc phase. It is implies that the origin of the properties due to the heat treatment.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2020년도 가을 학술논문 발표대회
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• pp.102-103
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• 2020

In this study, the effect of the change in the cement contents on the basic properties of the concrete and the estimation of the cement contents of hardened concretes using the hydrochloric acid melting heat. As a result of the study, as the cement contents increased, the fluidity and compressive strength increased, and there was no significant difference in the air contents and the unit volume mass. In addition, it showed a high correlation when compared with the estimated cement contents derived using the hydrochloric acid melting and the cement contents at the time of mixing. Therefore, it is considered that the hydrochloric acid melting is possible as a method of estimating the cement contents of concrete.

• 한국염색가공학회지
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• 제25권1호
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• pp.47-55
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• 2013

Physical properties of the composite yarn using low-melting(LM) polyester/Tencel were investigated with air-jet texturing conditions such as temperature, take-up overfeed, yarn speed and air pressure. Surface morphology, microstructure, tensile property, glossiness were evaluated. Surface morphology of a composite yarn had more damaged and loosened structure according to increase of take-up overfeed, yarn speed and air pressure. Crystallinity was affected by parameters such as temperature, yarn speed, take-up overfeed and air pressure and especially, yarn speed was most effective for increase of crystallinity. Also, it was found that temperature and air pressure had significantly affected tensile properties of a composite yarn. The glossiness of yarn increased with increase of temperature, yarn speed and air pressure.

• 열처리공학회지
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• 제8권4호
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• pp.245-254
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• 1995

The purpose of this study was to examine the effects of low melting point phase(LMPP) on mechanical properties in the Al-Cu-Li-X(In, Be) alloys. This study was performed by the differential scanning calorimetry(DSC), the transmission electron microscope(TEM), hardness test, tensile test and notch tensile test. The shape of LMPP in the specimens homogenized at $570^{\circ}C$ was film type due to remelting at grain boundary during homogenization. Low melting point phases had no effects on mechanical properties in the aging treated materials, because the density of LMPPs was low. Mechanical properties of the aging treated materials were affected by the density of matrix precipitation phases and grain sizes. For the In or In, Be added Al-Cu-Li alloys, the optimum solution treatment temperature was $550^{\circ}C$. The strength of Al-Cu-Li-In-Be $T_6$ treated alloy was higher than that of 2090-$T_8$ alloy.

• 한국전기전자재료학회논문지
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• 제17권8호
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• pp.893-897
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• 2004

In this paper, we studied the mechanical and thermal properties on slice XLPE sheet from 22 kV and 154 kV power cables. Interface structures are XLPE/semiconductor and XLPE/water/semiconductor. We evaluated mechanical property, thermal analysis, moisture analysis. Based on mechanical and thermal properties of the 22 kV XLPE sheet, elongation, mechanical strength, and melting point were evaluated to be 485.48 %, 1.74 kgf/$\textrm{mm}^2$ and $102.48^{\circ}C$, respectively. It was also evaluated from the mechanical and thermal properties of 154 kV XLPE sheet that elongation, mechanical strength, and melting point are 507.81 %, 1.8 kgf/$\textrm{mm}^2$, $106.9^{\circ}C$, respectively. A region shows a rapid increase in tension strength, and B region only shows increase in elongation under 1.0 kgf/$\textrm{mm}^2$, C region shows increase in both elongation and tension strength. Difference of melting point came from the chain of XLPE polymer and the difference of crystallization. Moisture density of semiconductor showed 800 ∼ 1200 ppm before extrude, 14000 ∼24000 ppm after extrude. These values were higher than the moisture density of XLPE (300∼560) ppm.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.686-687
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• 2006

The encapsulated induction melting and hot pressing were employed to prepare Fe-doped $CoSb_3$ skutterudites and their thermoelectric properties were investigated. Single phase $\delta-CoSb_3$ was successfully obtained by the subsequent heat treatment at 773K for 24 hours. Iron atoms acted as electron acceptors by substituting cobalt atoms. Thermoelectric properties were remarkably improved by the appropriate doping. $Co_{0.7}Fe_{0.3}Sb_3$ was found as an optimum composition for best thermoelectric properties in this work.