• Korean Journal of Plant Resources
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• v.24 no.3
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• pp.309-313
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• 2011

Houttuynia cordata is used as a raw material of oriental medicine to acquire antioxidant and anti cancer effect and to cure a heart disease. Mechanochemical technology not only reduces the size of the object but also changes the chemical properties of the object. Extraction of functional materials from the Houttuynia cordata after grinding as a pretreatment using the mechanochemical technology was conducted in this study to investigate the effect of grinding on the yields and antioxidant activities of the extract. Houttuynia cordata was ground by the planetary ball mill and the morphology was analyzed by SEM. Yields of functional materials were increased from 6.2 g in the sample without grinding to 7.0, 7.8, 8.8 g after grinding of 30 minutes, 1 hour and 2 hours, respectively. Nitrite scavenging abilities were increased from 57-77% to 69-86% as a result of mechanochemical pretreatment. Also, DPPH scavenging abilities for the methanol extraction were increased from 10.01-40.29% to 11.01-49.29% as a result of mechanochemical grinding.

• Journal of the Korean Recycled Construction Resources Institute
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• v.9 no.3
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• pp.367-374
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• 2021

In this study, the applicability of mechanochemical process for the manufacture of self-healing admixtures and the effect of mechanochemical process on the self-healing performance were evaluated. The self-healing admixtures were adopted as a highly reactive materials(expansive agent, swelling material and crystal growth agent) for mechanochemical processes. The self-healing admixtures for the mechanochemical process application were evaluated by X-Ray Diffraction and Fourier Transform Infrared Spectroscopy analysis, water permeability performance was used to evaluate self-healing performance of mortar. As a result of the evaluation, the self-healing performance of the WM(With-Mortar)3 sample to which mechanochemical process increased by 4.1% compared to the WM1 sample that was not treated, and the average healing index was 94.3%.

• Journal of the Korean Ceramic Society
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• v.38 no.12
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• pp.1110-1114
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• 2001

We report the mechanochemical effect of an Fe(NO$_3$)$_3$$.$9H$_2$O-Al(OH)$_3$sample as catalytic precursor mixed-ground by mixer mill on the growth of carbon nanotubes using thermal chemical vapor deposition method. From and TEM observations, carbon products grown on a ground catalyst were more uniform than those grown on an unground catalyst and most of them were identified as carbon nanobubes. Also, it was observed that field emission properties of products on ground catalyst were superior to those of unground catalyst.

• Journal of the Semiconductor & Display Technology
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• v.3 no.1
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• pp.9-13
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• 2004

Carbon nanofibers (CNFs) with uniform diameter and controlled size were prepared from catalytic decomposition of $\textrm{C}_{2}\textrm{H}_{2}$ with Ni-MgO catalyst treated by mechanochemical (MC) process. The properties of Ni catalyst, such as size, distribution and morphology, can be governed by tuning grinding time in MC process. As a result, size and structure of CNFs can be tailored. The effect of grinding time to the as-grown CNFs was studied. CNFs with diameter from 10-70 nm were synthesized. CNFs with bundle formation sharing one tip and twisted CNFs were also synthesized with catalyst treated by MC process.

• Korean Journal of Plant Resources
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• v.24 no.3
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• pp.314-318
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• 2011

Saururus chinensis is used as a raw material of an anti-rheumatic, poultice, sedative and stomachic. The tea of dried Saururus chinensis leaves has a function of relaxing pains in back and breast and of treating stomach ailments. The plant has the functions of anti-inflammatory, depurative, diuretic, febrifuge and refrigerant. The extraction of functional material is carried out by methanol and ethanol solvents. Mechanochemical grinding is applied as a pretreatment process before extraction to enhance the extraction efficiency by increasing the surface area of the materials while changing the chemical properties of the materials. Extraction of functional materials from the Saururus chinensis after grinding as a pretreatment using the mechanochemical technology was accomplished in this study to investigate the effect of grinding on the antioxidant activities of the extract. Saururus chinensis was ground by the planetary ball mill and the morphology was analyzed by SEM. Mechanochemical pretreatment increased the yields of functional materials from 5.9 g to 6.4, 7.0, and 8.1 g after grinding of 30 minutes, 1 hour and 2 hours, respectively. Nitrite scavenging ability increased from 53.0-71.0% to 61.0-79.0% for the methanol extraction in the solution of pH 1.2. Also, Electron donating abilities were increased from 7.90-33.51% to 11.97-38.51% for the methanol extraction. The extract concentration for the half inhibition of DPPH radicals was reduced from $278{\mu}g/mL$ in the original sample to $263{\mu}g/mL$ in the sample after grinding for the methanol extraction.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.171-171
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• 2003

• Proceedings of the Materials Research Society of Korea Conference
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• 2001.05a
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• pp.164-164
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• 2001

• Proceedings of the Korean Ceranic Society Conference
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• 2000.10a
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• pp.34.1-34
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• 2000

• Bulletin of the Korean Chemical Society
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• v.25 no.5
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• pp.617-619
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• 2004

As an pretreatment, a Fe$(NO_3)_3{\cdot}9H_2O-Al(OH)_3$mixture was ground by a high energy mill and used as a supported catalyst for the growth of carbon nanotubes by a thermal CVD. The crystal structure of the catalyst disordered by the grinding influenced significantly the synthesis of carbon nanotubes in a thermal CVD.

• Journal of the Korean Society for Precision Engineering
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• v.13 no.6
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• pp.45-51
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• 1996

Silicon wafers are required to be finished under the roughness of nanometer order for the subsequent chip fabrication processes. Recently, the finish grinding techniques have been researched for the improvement of accuracy and surface roughness simultaneously. Among them, the grinding technique using fine abrasive has been known as an easily accessible method. However, the manufacture of the fine grit grinding wheel has been very difficult because of the coherence of the grits. In this paper, the development of the ultrafine grit silica($SiO_2$) grinding wheel by the combination of the binder coating and the vacuum forming techniques is reported. And, the mechanochemical removal effects of the grinding conditions are discussed. Finally, a successful result of Ra O.4nm. Rmax 4nm in the ground surface roughness of a 6 inch silicon wafer was achieved.