• Title/Summary/Keyword: Measurement Standards

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Development of a Nutritional Supplement Certified Reference Material for Elemental Analysis

  • Lee, Jong Wha;Heo, Sung Woo;Kim, Hwijin;Lim, Youngran;Lee, Kyoung-Seok;Yim, Yong-Hyeon
    • Mass Spectrometry Letters
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    • 제9권4호
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    • pp.105-109
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    • 2018
  • A certified reference material (CRM) for the analysis of inorganic nutrients in nutritional supplements has been developed. Accurate mass fractions of chromium (Cr), iron (Fe), copper (Cu), and zinc (Zn) were determined by isotope dilution inductively coupled plasma mass spectrometry (ID ICP/MS). The measurement results were used to assign certified values for the CRM, which were metrologically traceable to the definitions of the measurement units in the International System of Units (SI). Production of a candidate reference material (RM) and the certification processes are summarized. Each nutrient in the CRM showed good homogeneity, which was estimated using relative standard deviations of the measurement results of twelve bottles in a batch. This CRM is expected to be an important reference to improve reliability and comparability of nutrient analyses in nutritional supplements and related samples in analytical laboratories.

초공진기를 이용한 노란색 레이저의 선폭 축소 및 초공진기의 예리도 측정 (Linewidth Reduction of a Yellow Laser by a Super-cavity and the Measurement of the Cavity Finesse)

  • 이원규;박창용;박상언;유한영;유대혁;문종철;서호성
    • 한국광학회지
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    • 제21권3호
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    • pp.123-128
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    • 2010
  • 이터븀 광격자 시계의 검색 레이저로 쓰기 위하여, WG-PPLN를 사용하여 1319 nm 파장의 Nd:YAG 레이저와 1030 nm 파장의 Yb 도핑된 광섬유 레이저의 합주파수 (578.4 nm)를 발생시켰다. 이터븀 광격자에서 시계 전이선을 분광하기 위해서는 1 Hz 수준의 선폭을 가지는 검색 레이저가 필요하기 때문에, 합주파수로 발생된 노란색 레이저의 주파수를 초공진기에 안정화하여 선폭을 축소하였다. 초공진기는 선팽창 계수가 낮은 ULE로 제작되었고, 진동으로 인한 영향이 작은 받침점에서 능동형 제진대 위에 설치되었다. 공기 굴절률의 영향을 제거하기 위하여 이 초공진기를 진공 체임버 내부에 설치하고, 온도를 1 mK 수준에서 안정화 하였다. 또한, 이 장치들을 방음 체임버 안에 설치하여, 소리로 인한 잡음을 막아 주었다. 실험에 사용된 초공진기의 광자 수명시간으로부터, 그 예리도가 380 000으로 측정되었다.

교류저항 표준기 제작과 그 특성 (Development and Its Properties of Resistance Standards for Using Alternative Current)

  • 김한준;이상화;강전홍;유광민;한상옥
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 하계학술대회 논문집
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    • pp.267-268
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    • 2009
  • Resistance standards from 1 ${\Omega}$ to 100 $k{\Omega}$, with calculable frequency dependencies of up to 1 MHz, have been developed for the calibration of commercial inductance-capacitance-resistance (LCR) meters and impedance analyzers. The resistors are designed on the basis of single bifilar loops. The typical resistance change from dc to 1 MHz is from 200 to $800\;{\mu}{\Omega}/{\Omega}$. According to the measurement results, the frequency dependencies of the resistors are severaltimes lower than the measurement uncertainty of commercial LCR meters.

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Measurement Uncertainties for Vacuum Standards from a Low to an Ultra-high Vacuum

  • Hong, S.S.;Shin, Y.H.;Lim, J.Y.
    • Applied Science and Convergence Technology
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    • 제23권3호
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    • pp.103-112
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    • 2014
  • The Korea Research Institute of Standards and Science (KRISS) has three major vacuum systems: an ultrasonic interferometer manometer (UIM; Section II, Figs. 1 and 2) for a low vacuum, a static expansion system (SES; Section III, Figs. 3 and 4) for a medium vacuum, and an orifice-type dynamic expansion system (DES, Section IV, Figs. 5 and 6) for high and ultra-high vacuum systems. For each system, explicit measurement model equations with multiple variables are given. According to ISO standards, all of these system variable errors were used to calculate the expanded uncertainty (U). For each system, the expanded uncertainties (k = 1, confidence level = 95%) and relative expanded uncertainty (expanded uncertainty/generated pressure) levels are summarized in Table 4. Within the uncertainty limits, our bilateral and key comparisons [CCM.P-K4 (10 Pa to 1 kPa)] are extensive and in good agreement with those of other nations (Fig. 8 and Table 5).

교류-직류 변환오차 자동 측정시스템 (An Automatic AC-DC Transfer Error Measurement System)

  • 권성원;조용명;김규태;강전홍;박영태
    • 센서학회지
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    • 제7권6호
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    • pp.401-408
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    • 1998
  • 교류전압표준기인 열전형 전압변환기의 교류-직류 변환오차를 비교평가하기 위하여 이중채널방식 자동측정시스템을 개발하였다. 비교측정되는 2대의 변환기출력을 동시에 측정하여 드리프트의 영향을 감소시켰고, 또 저열기전력 이중채널 스캐너를 사용하여 변환기 출력을 순방향-역방향으로 측정하여 그 평균값을 취함으로서 전압측정기의 ���V전압이 제거되도록 하였다. 정격전압이 동일한 4 V인 변환기끼리 비교 측정한 결과, 주파수 $40\;Hz{\sim}100\;kHz$에서는 외국표준기관에서의 측정값과 약 ${\pm}2\;ppm$ 이내에서 일치하였으며, $200\;kHz{\sim}1\;MHz$ 범위에서는 약 ${\pm}4\;ppm$ 이내에서 일치하였다. 본 시스템의 개발로 변환기의 교류-직류 변환오차의 측정능력을 기존수동방식의 약 ${\pm}15\;ppm$에서 ${\pm}\;3ppm$(100 kHz 이하)로 크게 향상시켰으며, 표준유지 및 산업체 지원의 효율을 크게 높일 수 있게 되었다.

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대규모 건물의 기밀성능 측정기준 수립에 관한 연구 (Study on the Establishment of Large Building Airtightness Measurement Standards)

  • 이동석;지경환;조재훈
    • 한국태양에너지학회 논문집
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    • 제34권1호
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    • pp.117-124
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    • 2014
  • Airtightness standards using fan pressurization method are normally used for measuring small buildings, detached houses, and apartment units. And, it is easy to conduct airtightness measurement through this fan pressurization method. However, it can be difficult to achieve accurate measurement results for the large buildings as the height and volume of the buildings have been increased. In this paper, we studied the principle of airtightness method by fan pressurization. And, we reviewed the measurement process described in ISO 9972, EN 13829, ASTM E779, ATTMA TS 1, CAN/CGSB 149.15, and JIS A 2201. Then, we categorized the methods' items according by air flow rate (Q) and pressure difference(${\Delta}P$). As a result, we made a comparison analysis on the measurement methods appeared in each standards. And, we achieved 5 test conditions about air flow rate and pressure difference to state requirements for large buildings airtightness measurement.

전기수술기 성능시험용 True RMS 측정에 관한 연구 (A Study on the True RMS Measurement of Electrical Unit for Performance Test)

  • 고한우;배문섭;최덕희
    • 대한의용생체공학회:의공학회지
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    • 제12권4호
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    • pp.309-314
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    • 1991
  • This paper describes the results of study on the measurement method of TRMS (true root mean square value) In electrosurgical unit. We used three type (direct computing type, indirect computing type, thermal converting type) in the measurement of TRMS. Three types of measurement method were compared with respect to power level, frequencey and crest factor in addition to environmental temperature. In three of them, the thermal converting type was the best for th electrosurgical unit analyzer

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자유공간 물질상수 측정법을 이용한 W-Band 유전율 측정 (W-Band Permittivity Measurements Using a Free-Space Material Measurement Technique)

  • 강진섭;김정환;조치현;김대찬
    • 한국전자파학회논문지
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    • 제24권3호
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    • pp.253-258
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    • 2013
  • 본 논문에서는 W-band(75~110 GHz) 자유공간 물질상수 측정법을 논의하였다. 우선 자유공간에서 주위 환경에 영향을 덜 받으면서 피측정물(MUT: Material Under Test)에 의한 산란계수를 정확하게 측정하기 위한 W-band quasi-optical 기술 기반 자유공간 물질상수 측정시스템을 논의하고, 관련 측정시스템의 GRL(Gated Reflect Line) 교정법을 기술하였다. 그리고 공기를 피측정물로 하여 제안된 측정법의 타당성을 보이고, 두께가 1.1 mm, 2 mm, 2.75 mm, 5 mm인 arystal 평판에 대한 측정 결과를 제시하였다.

Development of a Model System of Uncertainty Evaluations for Multiple Measurements by Isotope Dilution Mass Spectrometry: Determination of Folic Acid in Infant Formula

  • Kim, Byung-Joo;Hwang, Eui-Jin;So, Hun-Young;Son, Eun-Kyung;Kim, Yong-Seong
    • Bulletin of the Korean Chemical Society
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    • 제31권11호
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    • pp.3139-3144
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    • 2010
  • A model system has been established for the evaluation of the uncertainty of the value from measurements of multiple subsamples by isotope dilution mass spectrometry (IDMS). In this report, we apply this model system for the evaluation of measurement uncertainty in determination of folic acid in infant formula. Five subsamples were analyzed by IDMS. The mean of the measurement results of the five subsamples was assigned as the final measurement value. The standard deviation (s) of the results from five subsamples was attributable to repeatability of the measurement. The uncertainty components in the IDMS measurement methods were categorized into two groups. Group I includes uncertainty components which give common systematic effects to all subsamples and do not contribute to the variation among multiple measurements (repeatability). Group II includes uncertainty components that give random effects on the measurement results, and are related with the measurement repeatability. These random effects are attributed to s. Therefore, the uncertainty of the final value was calculated by combining the standard deviation of the mean of multiple measurements, $s/{\surd}n$ (where n = 5), and the measurement uncertainty associated with the uncertainty components that give systematic effects.